Influence of preparation procedure on catalytic activity of PdBEA zeolites in aqueous phase hydrodechlorination of 1,1,2-trichloroethene
Publication type: Journal Article
Publication date: 2017-01-01
scimago Q1
wos Q2
SJR: 1.003
CiteScore: 11.0
Impact factor: 4.7
ISSN: 13871811, 18733093
General Chemistry
Condensed Matter Physics
General Materials Science
Mechanics of Materials
Abstract
Pd-loaded BEA zeolites containing 1 wt % of Pd were prepared by a two-step postsynthesis method (PdSiBEA and PdSiAlBEA) and a conventional wet impregnation (PdHAlBEA). Modification of BEA zeolite resulted in the introduction of Pd ions into zeolite framework as pseudo-tetrahedral Pd(II) and extra-framework octahedral Pd(II) evidenced by XRD, DR UV–vis and TPR measurements. Calcination of as prepared zeolites in air at 773 K for 3 h and then reduction in 10% H2/Ar flow at 873 K for 3 h led to obtain red-C-PdSiBEA, red-C-PdSiAlBEA and red-C-PdHAlBEA zeolites with different Pd nanoparticles size distributions showed by TEM. These zeolite materials were found to be active catalysts in aqueous-phase hydrodechlorination of 1,1,2-trichloroethene (TCE). The conducted catalytic reactions have demonstrated that the rate and course of TCE hydrodechlorination depend on the catalysts preparation method and Pd nanoparticles size.
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Kamińska I. et al. Influence of preparation procedure on catalytic activity of PdBEA zeolites in aqueous phase hydrodechlorination of 1,1,2-trichloroethene // Microporous and Mesoporous Materials. 2017. Vol. 237. pp. 65-73.
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Kamińska I., Lisovytskiy D., Casale S., Śrębowata A., Dzwigaj S. Influence of preparation procedure on catalytic activity of PdBEA zeolites in aqueous phase hydrodechlorination of 1,1,2-trichloroethene // Microporous and Mesoporous Materials. 2017. Vol. 237. pp. 65-73.
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TY - JOUR
DO - 10.1016/j.micromeso.2016.09.023
UR - https://doi.org/10.1016/j.micromeso.2016.09.023
TI - Influence of preparation procedure on catalytic activity of PdBEA zeolites in aqueous phase hydrodechlorination of 1,1,2-trichloroethene
T2 - Microporous and Mesoporous Materials
AU - Kamińska, Inez
AU - Lisovytskiy, D.
AU - Casale, Sandra
AU - Śrębowata, A.
AU - Dzwigaj, Stanislaw
PY - 2017
DA - 2017/01/01
PB - Elsevier
SP - 65-73
VL - 237
SN - 1387-1811
SN - 1873-3093
ER -
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@article{2017_Kamińska,
author = {Inez Kamińska and D. Lisovytskiy and Sandra Casale and A. Śrębowata and Stanislaw Dzwigaj},
title = {Influence of preparation procedure on catalytic activity of PdBEA zeolites in aqueous phase hydrodechlorination of 1,1,2-trichloroethene},
journal = {Microporous and Mesoporous Materials},
year = {2017},
volume = {237},
publisher = {Elsevier},
month = {jan},
url = {https://doi.org/10.1016/j.micromeso.2016.09.023},
pages = {65--73},
doi = {10.1016/j.micromeso.2016.09.023}
}