Synthesis and structural determination of 3,5-bis(2-fluorobenzylidene)-4-piperidone analogs of curcumin
Тип публикации: Journal Article
Дата публикации: 2009-11-01
scimago Q2
wos Q2
БС1
SJR: 0.628
CiteScore: 8.0
Impact factor: 4.7
ISSN: 00222860, 18728014
Organic Chemistry
Inorganic Chemistry
Spectroscopy
Analytical Chemistry
Краткое описание
Analogs of cytotoxic compound 3,5-bis(2-fluorobenzylidene)-4-piperidone (1) were synthesized and their molecular structures were characterized by 1H, 13C NMR, ESI–MS, IR spectra and X-ray crystallography. The central ring of the piperidin-4-one ring assumes a sofa conformation with two benzylidene rings connected through E,E oriented groups. The compound 1 crystallized in triclinic space group P 1 ¯ . In order to obtain potentially more efficacious compounds, three dimers of 3,5-bis(2-fluorobenzylidene)-4-piperidone were synthesized. The two molecules of 1 were conjugated together via N oxalyl N (3), N fumaryl N (4) or N DTPA N (5) linkers. Compound 3 crystallized in monoclinic space group P21/n.
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Lagisetty P., Powell D. R., Awasthi V. Synthesis and structural determination of 3,5-bis(2-fluorobenzylidene)-4-piperidone analogs of curcumin // Journal of Molecular Structure. 2009. Vol. 936. No. 1-3. pp. 23-28.
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Lagisetty P., Powell D. R., Awasthi V. Synthesis and structural determination of 3,5-bis(2-fluorobenzylidene)-4-piperidone analogs of curcumin // Journal of Molecular Structure. 2009. Vol. 936. No. 1-3. pp. 23-28.
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TY - JOUR
DO - 10.1016/j.molstruc.2009.07.016
UR - https://doi.org/10.1016/j.molstruc.2009.07.016
TI - Synthesis and structural determination of 3,5-bis(2-fluorobenzylidene)-4-piperidone analogs of curcumin
T2 - Journal of Molecular Structure
AU - Lagisetty, Pallavi
AU - Powell, Douglas R.
AU - Awasthi, Vibhudutta
PY - 2009
DA - 2009/11/01
PB - Elsevier
SP - 23-28
IS - 1-3
VL - 936
SN - 0022-2860
SN - 1872-8014
ER -
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@article{2009_Lagisetty,
author = {Pallavi Lagisetty and Douglas R. Powell and Vibhudutta Awasthi},
title = {Synthesis and structural determination of 3,5-bis(2-fluorobenzylidene)-4-piperidone analogs of curcumin},
journal = {Journal of Molecular Structure},
year = {2009},
volume = {936},
publisher = {Elsevier},
month = {nov},
url = {https://doi.org/10.1016/j.molstruc.2009.07.016},
number = {1-3},
pages = {23--28},
doi = {10.1016/j.molstruc.2009.07.016}
}
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Lagisetty, Pallavi, et al. “Synthesis and structural determination of 3,5-bis(2-fluorobenzylidene)-4-piperidone analogs of curcumin.” Journal of Molecular Structure, vol. 936, no. 1-3, Nov. 2009, pp. 23-28. https://doi.org/10.1016/j.molstruc.2009.07.016.