Synthesis, crystal structure, thermal properties of copper(II) acrylate complex with 4′-phenyl-2,2′:6′,2′′-terpyridine and its use in nanomaterials science
Igor E Uflyand
1
,
Valerii V Tkachev
2
,
Ekaterina G. Drogan
3
,
Victoria E. Burlakova
3
,
Mikhail E Sokolov
4
,
Victor T Panyushkin
5
,
Publication type: Journal Article
Publication date: 2022-02-01
scimago Q2
wos Q2
SJR: 0.628
CiteScore: 8.0
Impact factor: 4.7
ISSN: 00222860, 18728014
Organic Chemistry
Inorganic Chemistry
Spectroscopy
Analytical Chemistry
Abstract
The reaction between copper(II) acrylate and 4′-phenyl-2,2′:6′,2″-terpyridine resulted in a new metal-containing monomer 1, which was characterized by elemental analysis, FTIR spectroscopy, and single-crystal X-ray diffraction analysis. Complex 1 crystallizes in triclinic form with space group P-1. The chelate node of complex 1 is close to an ideal tetragonal pyramidal structure and includes three nitrogen atoms of the terpyridine ligand and two oxygen atoms of acrylate fragments. Medium-strong hydrogen bond interactions lead to infinite 1D chains. The kinetic and thermodynamic parameters of the thermolysis process of complex 1 were studied. As a result of thermolysis process, nanomaterials of the [email protected] core-shell type were obtained. The resulting nanomaterials are effective antiwear and antifriction additives for lubricating oils.
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Uflyand I. E. et al. Synthesis, crystal structure, thermal properties of copper(II) acrylate complex with 4′-phenyl-2,2′:6′,2′′-terpyridine and its use in nanomaterials science // Journal of Molecular Structure. 2022. Vol. 1250. p. 131909.
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Uflyand I. E., Tkachev V. V., Zhinzhilo V. A., Drogan E. G., Burlakova V. E., Sokolov M. E., Panyushkin V. T., Baimuratova R. K., Dzhardimalieva G. I. Synthesis, crystal structure, thermal properties of copper(II) acrylate complex with 4′-phenyl-2,2′:6′,2′′-terpyridine and its use in nanomaterials science // Journal of Molecular Structure. 2022. Vol. 1250. p. 131909.
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TY - JOUR
DO - 10.1016/j.molstruc.2021.131909
UR - https://doi.org/10.1016/j.molstruc.2021.131909
TI - Synthesis, crystal structure, thermal properties of copper(II) acrylate complex with 4′-phenyl-2,2′:6′,2′′-terpyridine and its use in nanomaterials science
T2 - Journal of Molecular Structure
AU - Uflyand, Igor E
AU - Tkachev, Valerii V
AU - Zhinzhilo, Vladimir A.
AU - Drogan, Ekaterina G.
AU - Burlakova, Victoria E.
AU - Sokolov, Mikhail E
AU - Panyushkin, Victor T
AU - Baimuratova, Rosa K.
AU - Dzhardimalieva, Gulzhian I.
PY - 2022
DA - 2022/02/01
PB - Elsevier
SP - 131909
VL - 1250
SN - 0022-2860
SN - 1872-8014
ER -
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@article{2022_Uflyand,
author = {Igor E Uflyand and Valerii V Tkachev and Vladimir A. Zhinzhilo and Ekaterina G. Drogan and Victoria E. Burlakova and Mikhail E Sokolov and Victor T Panyushkin and Rosa K. Baimuratova and Gulzhian I. Dzhardimalieva},
title = {Synthesis, crystal structure, thermal properties of copper(II) acrylate complex with 4′-phenyl-2,2′:6′,2′′-terpyridine and its use in nanomaterials science},
journal = {Journal of Molecular Structure},
year = {2022},
volume = {1250},
publisher = {Elsevier},
month = {feb},
url = {https://doi.org/10.1016/j.molstruc.2021.131909},
pages = {131909},
doi = {10.1016/j.molstruc.2021.131909}
}