An efficient method for the preparation of silyl esters of diphosphoric, phosphoric, and phosphorous acid
Publication type: Journal Article
Publication date: 2014-03-01
scimago Q3
wos Q2
SJR: 0.396
CiteScore: 4.9
Impact factor: 2.6
ISSN: 02775387, 18733719
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Tetrakis(trialkylsilyl) diphosphate (alkyl = Me, Et, iPr, tBu) can be obtained in quantitative yield by reacting commercial disodium dihydrogen diphosphate with the respective trialkyl chlorosilane in a triphasic system with formamide. The alkylsilane residues of the diphosphate silyl esters can be either partially or completely hydrolyzed without concurrent cleavage of the P–O–P bond of the diphosphate moiety. The method can be expanded to efficiently produce other persilylated or partially silylated phosphates and phosphites.
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Wessjohann L. A., Dessoy M. A. An efficient method for the preparation of silyl esters of diphosphoric, phosphoric, and phosphorous acid // Polyhedron. 2014. Vol. 70. pp. 133-137.
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Wessjohann L. A., Dessoy M. A. An efficient method for the preparation of silyl esters of diphosphoric, phosphoric, and phosphorous acid // Polyhedron. 2014. Vol. 70. pp. 133-137.
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TY - JOUR
DO - 10.1016/j.poly.2013.12.024
UR - https://doi.org/10.1016/j.poly.2013.12.024
TI - An efficient method for the preparation of silyl esters of diphosphoric, phosphoric, and phosphorous acid
T2 - Polyhedron
AU - Wessjohann, Ludger A.
AU - Dessoy, Marco A
PY - 2014
DA - 2014/03/01
PB - Elsevier
SP - 133-137
VL - 70
SN - 0277-5387
SN - 1873-3719
ER -
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@article{2014_Wessjohann,
author = {Ludger A. Wessjohann and Marco A Dessoy},
title = {An efficient method for the preparation of silyl esters of diphosphoric, phosphoric, and phosphorous acid},
journal = {Polyhedron},
year = {2014},
volume = {70},
publisher = {Elsevier},
month = {mar},
url = {https://doi.org/10.1016/j.poly.2013.12.024},
pages = {133--137},
doi = {10.1016/j.poly.2013.12.024}
}