Polyhedron, volume 177, pages 114279
Metal complexes based on polyfluorosalicylic acids and their antimycotic and antimicrobial activity
I V Shchur
1
,
E.V. Shchegol’kov
2, 3
,
Ya. V. Burgart
2, 3
,
A N Kozitsina
4
,
Alla Ivanova
4
,
I S Alyamovskaya
4
,
N P Evstigneeva
5
,
N A Gerasimova
5
,
I N Ganebnykh
1
,
N V Zilberberg
5
,
N V Kungurov
5
,
V. I. Saloutin
2, 3
,
O. N. Chupakhin
2, 3
5
Ural Research Institute for Dermatology, Venereology and Immunopathology, Shcherbakova St. 8, Ekaterinburg 620076, Russia
|
Publication type: Journal Article
Publication date: 2020-02-01
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
To study acidity of polyfluorosalicylic acids, their ionization constants (pKa) were determined. A series of metal salts and heteroligand complexes was obtained from polyfluorosalicylic acids containing biogenic metal ions and coligands, such as triphenylphosphine, pyridine, 2,2′-bipyridine and 1,10-phenanthroline. The structures of synthesized salts and complexes were determined by elemental analysis, HRMS and IR spectroscopy. X-Ray diffraction analysis was used to confirm the structure of the heteroligand metal complexes based on polyfluorosalicyic acids and bipyridine-type coligands. In the heteroligand complexes, it was possible to achieve different ratios of polyfluorosalicylate and coligand, depending on the metal cation. The antimycotic and antibacterial activities of polyfluorosalicylic acids were studied and their metal complexes were investigated. The metal heteroligand complexes were found to exhibit high anti-gonorrhea activity. In addition, cobalt(II) 2,3,4,5-tetrafluorosalicylato-κ2O-bis(2,2′-bipyridine-κ2N) dihydrate was found to show a pronounced activity against Trichophyton rubrum, T. interdigitale, Epidermophyton floccosum strains.
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Shchur I. V. et al. Metal complexes based on polyfluorosalicylic acids and their antimycotic and antimicrobial activity // Polyhedron. 2020. Vol. 177. p. 114279.
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Shchur I. V., Shchegol’kov E., Burgart Y. V., Kozitsina A. N., Ivanova A., Alyamovskaya I. S., Evstigneeva N. P., Gerasimova N. A., Ganebnykh I. N., Zilberberg N. V., Kungurov N. V., Saloutin V. I., Chupakhin O. N. Metal complexes based on polyfluorosalicylic acids and their antimycotic and antimicrobial activity // Polyhedron. 2020. Vol. 177. p. 114279.
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TY - JOUR
DO - 10.1016/j.poly.2019.114279
UR - https://doi.org/10.1016/j.poly.2019.114279
TI - Metal complexes based on polyfluorosalicylic acids and their antimycotic and antimicrobial activity
T2 - Polyhedron
AU - Shchur, I V
AU - Shchegol’kov, E.V.
AU - Burgart, Ya. V.
AU - Kozitsina, A N
AU - Ivanova, Alla
AU - Alyamovskaya, I S
AU - Evstigneeva, N P
AU - Gerasimova, N A
AU - Ganebnykh, I N
AU - Zilberberg, N V
AU - Kungurov, N V
AU - Saloutin, V. I.
AU - Chupakhin, O. N.
PY - 2020
DA - 2020/02/01 00:00:00
PB - Elsevier
SP - 114279
VL - 177
SN - 0277-5387
ER -
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@article{2020_Shchur,
author = {I V Shchur and E.V. Shchegol’kov and Ya. V. Burgart and A N Kozitsina and Alla Ivanova and I S Alyamovskaya and N P Evstigneeva and N A Gerasimova and I N Ganebnykh and N V Zilberberg and N V Kungurov and V. I. Saloutin and O. N. Chupakhin},
title = {Metal complexes based on polyfluorosalicylic acids and their antimycotic and antimicrobial activity},
journal = {Polyhedron},
year = {2020},
volume = {177},
publisher = {Elsevier},
month = {feb},
url = {https://doi.org/10.1016/j.poly.2019.114279},
pages = {114279},
doi = {10.1016/j.poly.2019.114279}
}