Polymer

, volume 52 , issue 3 , pages 622-628

Poly (acrylonitrile – co -1-vinylimidazole): A new melt processable carbon fiber precursor

Wenjin Deng ¹

Alexander Lobovsky ²

Scott T. Iacono ^{1, 3}

Tianyu Wu ⁴

Neetu Tomar ¹

Stephen M. Budy ¹

Timothy Long ⁴

Wesley P. Hoffman ^{5, 6}

Dennis G. Smith ^{1, 7}

Hide authors affiliations Show authors affiliations: 7 affiliations

CLEMSON UNIVERSITY |

Advanced Fiber Engineering, LLC

United States Air Force Academy

⁴

Virginia Polytechnic Inst & State Univ. |

⁵

Air Force Research Laboratory

⁶

university of Arizona |

⁷

University Of Texas At Dallas |

Publication type: Journal Article

Publication date: 2011-02-03

Elsevier

Polymer

scimago Q1

wos Q2

SJR: 0.843

CiteScore: 7.7

Impact factor: 4.5

ISSN: 00323861, 18732291

DOI: 10.1016/j.polymer.2010.11.054

Copy DOI

Materials Chemistry

Organic Chemistry

Polymers and Plastics

Abstract

Acrylonitrile/1-vinylimidazole (AN/VIM) copolymers containing various mol% of VIM were synthesized by free radical solution polymerization. The copolymers were characterized by Attenuated Total Reflectance-Fourier Transform Infrared (ATR-FTIR) spectroscopy, 1 H NMR spectroscopy, gel permeation chromatography (GPC) and differential scanning calorimetry (DSC). Char yields of the copolymers were 40–48% as determined by thermogravimetric analysis (TGA) while gel fractions were found to be 90–99% depending upon the composition, temperature and time. The complex viscosity of the precursor copolymers was measured as a function of composition and temperature. 82/18 mol% of AN/VIM copolymer based carbon fiber precursor was successfully processed by solvent-free melt spinning at 192 °C and the melt-spun fiber was characterized by DSC, ATR-IR, and X-ray Diffraction (XRD).

Found

3 citations

Prokopov N

34 publications, 263 citations

h-index: 11

MIREA — Russian Technological University

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GOST |

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GOST Copy

Deng W. et al. Poly (acrylonitrile – co -1-vinylimidazole): A new melt processable carbon fiber precursor // Polymer. 2011. Vol. 52. No. 3. pp. 622-628.

GOST all authors (up to 50) Copy

Deng W., Lobovsky A., Iacono S. T., Wu T., Tomar N., Budy S. M., Long T., Hoffman W. P., Smith D. G. Poly (acrylonitrile – co -1-vinylimidazole): A new melt processable carbon fiber precursor // Polymer. 2011. Vol. 52. No. 3. pp. 622-628.

RIS |

Cite this

RIS Copy

TY - JOUR

DO - 10.1016/j.polymer.2010.11.054

UR - https://doi.org/10.1016/j.polymer.2010.11.054

TI - Poly (acrylonitrile – co -1-vinylimidazole): A new melt processable carbon fiber precursor

T2 - Polymer

AU - Deng, Wenjin

AU - Lobovsky, Alexander

AU - Iacono, Scott T.

AU - Wu, Tianyu

AU - Tomar, Neetu

AU - Budy, Stephen M.

AU - Long, Timothy

AU - Hoffman, Wesley P.

AU - Smith, Dennis G.

PY - 2011

DA - 2011/02/03

PB - Elsevier

SP - 622-628

IS - 3

VL - 52

SN - 0032-3861

SN - 1873-2291

ER -

BibTex |

Cite this

BibTex (up to 50 authors) Copy

@article{2011_Deng,

author = {Wenjin Deng and Alexander Lobovsky and Scott T. Iacono and Tianyu Wu and Neetu Tomar and Stephen M. Budy and Timothy Long and Wesley P. Hoffman and Dennis G. Smith},

title = {Poly (acrylonitrile – co -1-vinylimidazole): A new melt processable carbon fiber precursor},

journal = {Polymer},

year = {2011},

volume = {52},

publisher = {Elsevier},

month = {feb},

url = {https://doi.org/10.1016/j.polymer.2010.11.054},

number = {3},

pages = {622--628},

doi = {10.1016/j.polymer.2010.11.054}

}

MLA

Cite this

MLA Copy

Deng, Wenjin, et al. “Poly (acrylonitrile – co -1-vinylimidazole): A new melt processable carbon fiber precursor.” Polymer, vol. 52, no. 3, Feb. 2011, pp. 622-628. https://doi.org/10.1016/j.polymer.2010.11.054.

Publisher

Elsevier

Journal

Polymer

scimago Q1

wos Q2

SJR

0.843

CiteScore

7.7

Impact factor

4.5

ISSN

00323861 (Print)

18732291