Open Access
Incorporation of 3d-metal ions in the hexagonal channels of the Sr5(PO4)3OH apatite
Publication type: Journal Article
Publication date: 2007-01-17
scimago Q2
wos Q1
SJR: 0.609
CiteScore: 5.4
Impact factor: 3.3
ISSN: 12932558, 18733085
General Chemistry
Condensed Matter Physics
General Materials Science
Abstract
Strontium phosphate apatites with compositions Sr 5 (PO 4 ) 3 Zn 0.15 O 0.3 (OH) 0.7 , Sr 5 (PO 4 ) 3 Ni 0.2 O 0.4 (OH) 0.6 , and Sr 5 (PO 4 ) 3 Co 0.2 O 0.5 (OH) 0.4 were synthesized by solid state reaction at 1400 °C in air. The samples were characterized by powder X-ray diffraction, EDX analysis, magnetic measurements and IR spectroscopy. The crystal structures were refined by the Rietveld method in the space group P 6 3 / m with lattice constants a = 9.7499(1), 9.7722(1), 9.7507(1) A and c = 7.3066(1), 7.2962(1), 7.2988(1) A, respectively. The 3d-metal atoms were found randomly distributed in the hexagonal channels formally substituting hydrogen in the initial hydroxyapatite. Zn and Ni atoms were twofold coordinated by oxygen atoms such that the linear O–M–O groups formed in the channel separated by the OH groups. Co atom was shifted from the channel center giving the O–Co–O fragment distorted from a linear geometry probably due to the additional coordination by the oxygen atoms of the phosphate groups.
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Kazin P. E. et al. Incorporation of 3d-metal ions in the hexagonal channels of the Sr5(PO4)3OH apatite // Solid State Sciences. 2007. Vol. 9. No. 1. pp. 82-87.
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Kazin P. E., Gazizova O. R., Karpov A. S., Jansen M., Tretyakov Y. D. Incorporation of 3d-metal ions in the hexagonal channels of the Sr5(PO4)3OH apatite // Solid State Sciences. 2007. Vol. 9. No. 1. pp. 82-87.
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TY - JOUR
DO - 10.1016/j.solidstatesciences.2006.11.005
UR - https://doi.org/10.1016/j.solidstatesciences.2006.11.005
TI - Incorporation of 3d-metal ions in the hexagonal channels of the Sr5(PO4)3OH apatite
T2 - Solid State Sciences
AU - Kazin, P. E.
AU - Gazizova, Olga R
AU - Karpov, Andrey S.
AU - Jansen, Martin
AU - Tretyakov, Yuri D.
PY - 2007
DA - 2007/01/17
PB - Elsevier
SP - 82-87
IS - 1
VL - 9
SN - 1293-2558
SN - 1873-3085
ER -
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BibTex (up to 50 authors)
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@article{2007_Kazin,
author = {P. E. Kazin and Olga R Gazizova and Andrey S. Karpov and Martin Jansen and Yuri D. Tretyakov},
title = {Incorporation of 3d-metal ions in the hexagonal channels of the Sr5(PO4)3OH apatite},
journal = {Solid State Sciences},
year = {2007},
volume = {9},
publisher = {Elsevier},
month = {jan},
url = {https://doi.org/10.1016/j.solidstatesciences.2006.11.005},
number = {1},
pages = {82--87},
doi = {10.1016/j.solidstatesciences.2006.11.005}
}
Cite this
MLA
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Kazin, P. E., et al. “Incorporation of 3d-metal ions in the hexagonal channels of the Sr5(PO4)3OH apatite.” Solid State Sciences, vol. 9, no. 1, Jan. 2007, pp. 82-87. https://doi.org/10.1016/j.solidstatesciences.2006.11.005.