Solid State Ionics, volume 182, issue 1, pages 53-58
Crystal structure and phase transitions of the lithium ionic conductor Li3PS4
Kenji Homma
1
,
Masao Yonemura
2
,
Takeshi KOBAYASHI
1
,
Miki Nagao
1
,
Masaaki Hirayama
1
,
Ryoji Kanno
1
Publication type: Journal Article
Publication date: 2011-02-03
General Chemistry
Condensed Matter Physics
General Materials Science
Abstract
The crystal structures of and phase transitions in the lithium ionic conductor, Li3PS4, which is part of the thio-LISICON (LIthium Super Ionic CONductor) family, were studied using high-temperature synchrotron X-ray diffraction measurements and thermal analysis. There are three transitions among the α, β and γ-phases of this material as a function of temperature. The low-temperature γ-phase transformed to the medium-temperature β-phase at 573 K, which then transformed to the high-temperature α-phase at 746 K. The γ-phase is iso-structural with β-Li3PO4 (SG: Pmn21) with an orthorhombic cell with a = 7.70829(11), b = 6.53521(10), and c = 6.1365(7) A at 297 K. The β-phase has an orthorhombic cell with a = 12.8190(5), b = 8.2195(4), and c = 6.1236(2) A at 637 K. The apexes of the PS4 tetrahedron are ordered in the same direction in the γ-phase, while in the β-phase, they are ordered in a zig-zag arrangement. The γ-phase showed an ionic conductivity of 3.0 × 10− 7 S cm− 1 with an activation energy of 21.3 kJ mol− 1 at room temperature. The β-phase showed an ionic conductivity of 3.0 × 10− 2 S cm− 1 at 500 K with an activation energy of 15.5 kJ mol− 1.
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Homma K. et al. Crystal structure and phase transitions of the lithium ionic conductor Li3PS4 // Solid State Ionics. 2011. Vol. 182. No. 1. pp. 53-58.
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Homma K., Yonemura M., KOBAYASHI T., Nagao M., Hirayama M., Kanno R. Crystal structure and phase transitions of the lithium ionic conductor Li3PS4 // Solid State Ionics. 2011. Vol. 182. No. 1. pp. 53-58.
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TY - JOUR
DO - 10.1016/j.ssi.2010.10.001
UR - https://doi.org/10.1016/j.ssi.2010.10.001
TI - Crystal structure and phase transitions of the lithium ionic conductor Li3PS4
T2 - Solid State Ionics
AU - Homma, Kenji
AU - Yonemura, Masao
AU - KOBAYASHI, Takeshi
AU - Nagao, Miki
AU - Hirayama, Masaaki
AU - Kanno, Ryoji
PY - 2011
DA - 2011/02/03 00:00:00
PB - Elsevier
SP - 53-58
IS - 1
VL - 182
SN - 0167-2738
ER -
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@article{2011_Homma,
author = {Kenji Homma and Masao Yonemura and Takeshi KOBAYASHI and Miki Nagao and Masaaki Hirayama and Ryoji Kanno},
title = {Crystal structure and phase transitions of the lithium ionic conductor Li3PS4},
journal = {Solid State Ionics},
year = {2011},
volume = {182},
publisher = {Elsevier},
month = {feb},
url = {https://doi.org/10.1016/j.ssi.2010.10.001},
number = {1},
pages = {53--58},
doi = {10.1016/j.ssi.2010.10.001}
}
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Homma, Kenji, et al. “Crystal structure and phase transitions of the lithium ionic conductor Li3PS4.” Solid State Ionics, vol. 182, no. 1, Feb. 2011, pp. 53-58. https://doi.org/10.1016/j.ssi.2010.10.001.