Some thermal studies of polysilanes and polycarbosilanes
Тип публикации: Journal Article
Дата публикации: 2004-12-01
scimago Q2
wos Q2
БС2
SJR: 0.64
CiteScore: 6.2
Impact factor: 3.5
ISSN: 00406031, 1872762X
Physical and Theoretical Chemistry
Condensed Matter Physics
Instrumentation
Краткое описание
Some thermal (TGA and DSC) studies of polysilanes viz., polydimethylsilane (PDMS), copolymer of polydimethyl-methylphenylsilane (PDMMPS), polydimethyl-methylsilane (PDMMS), polydimethyl-methylvinylsilane (PDMMVS) and polycarbosilanes (PCS) synthesized using PDMS have been carried out. PDMS and PDMMPS found more suitable for synthesizing meltable and soluble polycarbosilanes and gave better char yield compared to PDMMVS and PDMMS. The polydimethyl-methylvinylsilane (PDMMVS) did not show any melting behavior and cured at ∼166 °C as an endotherm was noticed in DSC. The PCS-N (mp ∼124 °C) on heating up to 450 °C become non-meltable but remain soluble in common organic solvents, which on further heating up to ∼650 °C become non-meltable and non-soluble. The thermal recycling of the PCS-N at ∼350 °C minimized the exotherms as observed in the DSC. The XRD studies revealed that the α-SiC and β-SiC formation took place at ∼930 and 1250 °C, respectively as reported earlier too.
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Shukla S. K. et al. Some thermal studies of polysilanes and polycarbosilanes // Thermochimica Acta. 2004. Vol. 424. No. 1-2. pp. 209-217.
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Shukla S. K., Tiwari R. K., Ranjan A., Saxena A. K., Mathur G. Some thermal studies of polysilanes and polycarbosilanes // Thermochimica Acta. 2004. Vol. 424. No. 1-2. pp. 209-217.
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TY - JOUR
DO - 10.1016/j.tca.2004.06.003
UR - https://doi.org/10.1016/j.tca.2004.06.003
TI - Some thermal studies of polysilanes and polycarbosilanes
T2 - Thermochimica Acta
AU - Shukla, Sanjeev K.
AU - Tiwari, R. K.
AU - Ranjan, Ashok
AU - Saxena, A. K.
AU - Mathur, G.N.
PY - 2004
DA - 2004/12/01
PB - Elsevier
SP - 209-217
IS - 1-2
VL - 424
SN - 0040-6031
SN - 1872-762X
ER -
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@article{2004_Shukla,
author = {Sanjeev K. Shukla and R. K. Tiwari and Ashok Ranjan and A. K. Saxena and G.N. Mathur},
title = {Some thermal studies of polysilanes and polycarbosilanes},
journal = {Thermochimica Acta},
year = {2004},
volume = {424},
publisher = {Elsevier},
month = {dec},
url = {https://doi.org/10.1016/j.tca.2004.06.003},
number = {1-2},
pages = {209--217},
doi = {10.1016/j.tca.2004.06.003}
}
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MLA
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Shukla, Sanjeev K., et al. “Some thermal studies of polysilanes and polycarbosilanes.” Thermochimica Acta, vol. 424, no. 1-2, Dec. 2004, pp. 209-217. https://doi.org/10.1016/j.tca.2004.06.003.