Unambiguous structure elucidation of the reaction products of 3-acyl-4-methoxy-1-methylquinolinones with hydroxylamine via NMR spectroscopy
Тип публикации: Journal Article
Дата публикации: 2007-11-01
scimago Q3
wos Q2
БС2
SJR: 0.426
CiteScore: 4.1
Impact factor: 2.2
ISSN: 00404020, 14645416
Organic Chemistry
Drug Discovery
Biochemistry
Краткое описание
Reaction of 3-acyl-4-methoxy-1-methylquinolinones 2a,b with hydroxylamine has been investigated under different experimental conditions. Whereas compound 2a gives rise selectively and exclusively to the regioisomeric isoxazolo[4,5-c]- or isoxazolo[4,3-c]quinolin-4(5H)one (compound 3a or 4a, respectively), reaction of 2b always led to a mixture of the required isoxazole together with the oxazole derivative. Structural elucidation of all products has been independently achieved by multinuclear (13C and 15N) magnetic resonance spectroscopy.
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Chimichi S., Boccalini M., Matteucci A. Unambiguous structure elucidation of the reaction products of 3-acyl-4-methoxy-1-methylquinolinones with hydroxylamine via NMR spectroscopy // Tetrahedron. 2007. Vol. 63. No. 47. pp. 11656-11660.
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Chimichi S., Boccalini M., Matteucci A. Unambiguous structure elucidation of the reaction products of 3-acyl-4-methoxy-1-methylquinolinones with hydroxylamine via NMR spectroscopy // Tetrahedron. 2007. Vol. 63. No. 47. pp. 11656-11660.
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TY - JOUR
DO - 10.1016/j.tet.2007.08.108
UR - https://doi.org/10.1016/j.tet.2007.08.108
TI - Unambiguous structure elucidation of the reaction products of 3-acyl-4-methoxy-1-methylquinolinones with hydroxylamine via NMR spectroscopy
T2 - Tetrahedron
AU - Chimichi, Stefano
AU - Boccalini, Marco
AU - Matteucci, Alessandra
PY - 2007
DA - 2007/11/01
PB - Elsevier
SP - 11656-11660
IS - 47
VL - 63
SN - 0040-4020
SN - 1464-5416
ER -
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@article{2007_Chimichi,
author = {Stefano Chimichi and Marco Boccalini and Alessandra Matteucci},
title = {Unambiguous structure elucidation of the reaction products of 3-acyl-4-methoxy-1-methylquinolinones with hydroxylamine via NMR spectroscopy},
journal = {Tetrahedron},
year = {2007},
volume = {63},
publisher = {Elsevier},
month = {nov},
url = {https://doi.org/10.1016/j.tet.2007.08.108},
number = {47},
pages = {11656--11660},
doi = {10.1016/j.tet.2007.08.108}
}
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MLA
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Chimichi, Stefano, et al. “Unambiguous structure elucidation of the reaction products of 3-acyl-4-methoxy-1-methylquinolinones with hydroxylamine via NMR spectroscopy.” Tetrahedron, vol. 63, no. 47, Nov. 2007, pp. 11656-11660. https://doi.org/10.1016/j.tet.2007.08.108.