Synthesis of the cis diastereoisomer of 5-diethoxyphosphoryl-5-methyl-3-phenyl-1-pyrroline N-oxide (DEPMPPOc) and ESR study of its superoxide spin adduct
Тип публикации: Journal Article
Дата публикации: 2004-08-01
scimago Q3
wos Q3
БС2
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Краткое описание
The cis and trans diastereoisomers of 5-diethoxyphosphoryl-5-methyl-3-phenyl-1-pyrroline N-oxide (DEPMPPO), the C(3)-phenyl analogue of DEPMPO, were prepared in three steps from phenylacetaldehyde and used in ESR-spin trapping of various carbon-, oxygen- and sulfur-centred radicals. In the case of the cis-isomer, the presence of the phenyl group cancels the alternating line width phenomenon observed for the DEPMPO–OOR (R = H, But) spin adducts. The ESR spectra of the DEPMPPOc–OOR spin adducts exhibit more straightforward patterns and are more easily assignable.
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Nsanzumuhire C. et al. Synthesis of the cis diastereoisomer of 5-diethoxyphosphoryl-5-methyl-3-phenyl-1-pyrroline N-oxide (DEPMPPOc) and ESR study of its superoxide spin adduct // Tetrahedron Letters. 2004. Vol. 45. No. 34. pp. 6385-6389.
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Nsanzumuhire C., Clément J., Ouari O., Karoui H., Finet J., Tordo P. Synthesis of the cis diastereoisomer of 5-diethoxyphosphoryl-5-methyl-3-phenyl-1-pyrroline N-oxide (DEPMPPOc) and ESR study of its superoxide spin adduct // Tetrahedron Letters. 2004. Vol. 45. No. 34. pp. 6385-6389.
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TY - JOUR
DO - 10.1016/j.tetlet.2004.07.016
UR - https://doi.org/10.1016/j.tetlet.2004.07.016
TI - Synthesis of the cis diastereoisomer of 5-diethoxyphosphoryl-5-methyl-3-phenyl-1-pyrroline N-oxide (DEPMPPOc) and ESR study of its superoxide spin adduct
T2 - Tetrahedron Letters
AU - Nsanzumuhire, Céline
AU - Clément, Jean-Louis
AU - Ouari, Olivier
AU - Karoui, Hakim
AU - Finet, Jean-Pierre
AU - Tordo, Paul
PY - 2004
DA - 2004/08/01
PB - Elsevier
SP - 6385-6389
IS - 34
VL - 45
SN - 0040-4039
SN - 1873-3581
ER -
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@article{2004_Nsanzumuhire,
author = {Céline Nsanzumuhire and Jean-Louis Clément and Olivier Ouari and Hakim Karoui and Jean-Pierre Finet and Paul Tordo},
title = {Synthesis of the cis diastereoisomer of 5-diethoxyphosphoryl-5-methyl-3-phenyl-1-pyrroline N-oxide (DEPMPPOc) and ESR study of its superoxide spin adduct},
journal = {Tetrahedron Letters},
year = {2004},
volume = {45},
publisher = {Elsevier},
month = {aug},
url = {https://doi.org/10.1016/j.tetlet.2004.07.016},
number = {34},
pages = {6385--6389},
doi = {10.1016/j.tetlet.2004.07.016}
}
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MLA
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Nsanzumuhire, Céline, et al. “Synthesis of the cis diastereoisomer of 5-diethoxyphosphoryl-5-methyl-3-phenyl-1-pyrroline N-oxide (DEPMPPOc) and ESR study of its superoxide spin adduct.” Tetrahedron Letters, vol. 45, no. 34, Aug. 2004, pp. 6385-6389. https://doi.org/10.1016/j.tetlet.2004.07.016.