A new facile synthesis of steroid dimers containing 17,17′-dicarboxamide spacers
Rui M. B. Carrilho
1, 2
,
Mariette M. Pereira
3
,
Maria José S. M. Moreno
4
,
Attila Takács
2
,
László Kollár
2
Publication type: Journal Article
Publication date: 2013-05-01
scimago Q3
wos Q3
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
A set of new steroid dimers linked through ring D–ring D were synthesized via catalytic diaminocarbonylation of 17-iodo-5α-androst-16-ene, in the presence of palladium–phosphine in situ catalysts and aliphatic or aromatic diamines as N -nucleophiles. The dimeric steroidal compounds containing 17,17′-dicarboxamide spacers were obtained through highly chemoselective reactions in good isolated yields and completely characterized by spectroscopic techniques.
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Carrilho R. M. B. et al. A new facile synthesis of steroid dimers containing 17,17′-dicarboxamide spacers // Tetrahedron Letters. 2013. Vol. 54. No. 22. pp. 2763-2765.
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Carrilho R. M. B., Pereira M. M., Moreno M. J. S. M., Takács A., Kollár L. A new facile synthesis of steroid dimers containing 17,17′-dicarboxamide spacers // Tetrahedron Letters. 2013. Vol. 54. No. 22. pp. 2763-2765.
Cite this
RIS
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TY - JOUR
DO - 10.1016/j.tetlet.2013.02.108
UR - https://doi.org/10.1016/j.tetlet.2013.02.108
TI - A new facile synthesis of steroid dimers containing 17,17′-dicarboxamide spacers
T2 - Tetrahedron Letters
AU - Carrilho, Rui M. B.
AU - Pereira, Mariette M.
AU - Moreno, Maria José S. M.
AU - Takács, Attila
AU - Kollár, László
PY - 2013
DA - 2013/05/01
PB - Elsevier
SP - 2763-2765
IS - 22
VL - 54
SN - 0040-4039
SN - 1873-3581
ER -
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BibTex (up to 50 authors)
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@article{2013_Carrilho,
author = {Rui M. B. Carrilho and Mariette M. Pereira and Maria José S. M. Moreno and Attila Takács and László Kollár},
title = {A new facile synthesis of steroid dimers containing 17,17′-dicarboxamide spacers},
journal = {Tetrahedron Letters},
year = {2013},
volume = {54},
publisher = {Elsevier},
month = {may},
url = {https://doi.org/10.1016/j.tetlet.2013.02.108},
number = {22},
pages = {2763--2765},
doi = {10.1016/j.tetlet.2013.02.108}
}
Cite this
MLA
Copy
Carrilho, Rui M. B., et al. “A new facile synthesis of steroid dimers containing 17,17′-dicarboxamide spacers.” Tetrahedron Letters, vol. 54, no. 22, May. 2013, pp. 2763-2765. https://doi.org/10.1016/j.tetlet.2013.02.108.