PCl 3 - and organometallic-free synthesis of tris(2-picolyl)phosphine oxide from elemental phosphorus and 2-(chloromethyl)pyridine hydrochloride
Publication type: Journal Article
Publication date: 2018-02-01
scimago Q3
wos Q3
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
In the superbase KOH/H2O/toluene/phase-transfer catalyst system, 2-picolyl chloride, generated in situ from 2-(chloromethyl)pyridine hydrochloride, reacts with elemental phosphorus at 65–95 °C for 3 h to afford tris(2-picolyl)phosphine oxide in 50% yield. Single crystal X-ray analysis of the latter revealed one polymorph form of this tertiary phosphine oxide.
Found
Nothing found, try to update filter.
Found
Nothing found, try to update filter.
Top-30
Journals
|
1
2
3
|
|
|
ChemistrySelect
3 publications, 16.67%
|
|
|
Russian Journal of General Chemistry
2 publications, 11.11%
|
|
|
International Journal of Molecular Sciences
1 publication, 5.56%
|
|
|
Catalysts
1 publication, 5.56%
|
|
|
Bioorganic Chemistry
1 publication, 5.56%
|
|
|
Russian Chemical Reviews
1 publication, 5.56%
|
|
|
European Journal of Organic Chemistry
1 publication, 5.56%
|
|
|
Organic and Biomolecular Chemistry
1 publication, 5.56%
|
|
|
Journal of Materials Chemistry C
1 publication, 5.56%
|
|
|
Green Chemistry
1 publication, 5.56%
|
|
|
Russian Journal of Organic Chemistry
1 publication, 5.56%
|
|
|
Molecules
1 publication, 5.56%
|
|
|
Mendeleev Communications
1 publication, 5.56%
|
|
|
Angewandte Chemie - International Edition
1 publication, 5.56%
|
|
|
Angewandte Chemie
1 publication, 5.56%
|
|
|
1
2
3
|
Publishers
|
1
2
3
4
5
6
|
|
|
Wiley
6 publications, 33.33%
|
|
|
MDPI
3 publications, 16.67%
|
|
|
Royal Society of Chemistry (RSC)
3 publications, 16.67%
|
|
|
Pleiades Publishing
3 publications, 16.67%
|
|
|
Elsevier
1 publication, 5.56%
|
|
|
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii
1 publication, 5.56%
|
|
|
OOO Zhurnal "Mendeleevskie Soobshcheniya"
1 publication, 5.56%
|
|
|
1
2
3
4
5
6
|
- We do not take into account publications without a DOI.
- Statistics recalculated weekly.
Are you a researcher?
Create a profile to get free access to personal recommendations for colleagues and new articles.
Metrics
18
Total citations:
18
Citations from 2025:
2
(11.11%)
Cite this
GOST |
RIS |
BibTex |
MLA
Cite this
GOST
Copy
Malysheva S. A. et al. PCl 3 - and organometallic-free synthesis of tris(2-picolyl)phosphine oxide from elemental phosphorus and 2-(chloromethyl)pyridine hydrochloride // Tetrahedron Letters. 2018. Vol. 59. No. 8. pp. 723-726.
GOST all authors (up to 50)
Copy
Malysheva S. A., Belogorlova N. A., Kuimov V. A., Litvintsev Y. I., Sterkhova I., Albanov A. I., Gusarova N. K., Trofimov B. A. PCl 3 - and organometallic-free synthesis of tris(2-picolyl)phosphine oxide from elemental phosphorus and 2-(chloromethyl)pyridine hydrochloride // Tetrahedron Letters. 2018. Vol. 59. No. 8. pp. 723-726.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1016/j.tetlet.2018.01.021
UR - https://doi.org/10.1016/j.tetlet.2018.01.021
TI - PCl 3 - and organometallic-free synthesis of tris(2-picolyl)phosphine oxide from elemental phosphorus and 2-(chloromethyl)pyridine hydrochloride
T2 - Tetrahedron Letters
AU - Malysheva, Svetlana A.
AU - Belogorlova, Nataliya A.
AU - Kuimov, Vladimir A
AU - Litvintsev, Yurii I
AU - Sterkhova, Irina
AU - Albanov, Alexander I
AU - Gusarova, Nina K.
AU - Trofimov, B. A.
PY - 2018
DA - 2018/02/01
PB - Elsevier
SP - 723-726
IS - 8
VL - 59
SN - 0040-4039
SN - 1873-3581
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2018_Malysheva,
author = {Svetlana A. Malysheva and Nataliya A. Belogorlova and Vladimir A Kuimov and Yurii I Litvintsev and Irina Sterkhova and Alexander I Albanov and Nina K. Gusarova and B. A. Trofimov},
title = {PCl 3 - and organometallic-free synthesis of tris(2-picolyl)phosphine oxide from elemental phosphorus and 2-(chloromethyl)pyridine hydrochloride},
journal = {Tetrahedron Letters},
year = {2018},
volume = {59},
publisher = {Elsevier},
month = {feb},
url = {https://doi.org/10.1016/j.tetlet.2018.01.021},
number = {8},
pages = {723--726},
doi = {10.1016/j.tetlet.2018.01.021}
}
Cite this
MLA
Copy
Malysheva, Svetlana A., et al. “PCl 3 - and organometallic-free synthesis of tris(2-picolyl)phosphine oxide from elemental phosphorus and 2-(chloromethyl)pyridine hydrochloride.” Tetrahedron Letters, vol. 59, no. 8, Feb. 2018, pp. 723-726. https://doi.org/10.1016/j.tetlet.2018.01.021.