Tributylphosphine catalyzed addition of diphenylphosphine oxide to unsubstituted and substituted electron-deficient alkenes
Тип публикации: Journal Article
Дата публикации: 2018-04-01
scimago Q3
wos Q3
БС2
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Краткое описание
The PBu3-catalyzed conjugate addition of diphenylphosphine oxide to unsubstituted and substituted electron-deficient alkenes is reported. β-Substituted α,β-unsaturated esters, trans-methyl crotonate and trans-methyl cinnamate, known for their reluctance to participate in phosphine-catalyzed transformations, also react well under the developed conditions. Mild reaction conditions, simple work-up and the ease of catalyst recovery make the proposed methodology useful for the preparation of functionalized tertiary phosphine oxides. The utility of this method was demonstrated by the gram-scale reactions of diphenylphosphine oxide with electron-deficient alkenes.
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Salin A. V. et al. Tributylphosphine catalyzed addition of diphenylphosphine oxide to unsubstituted and substituted electron-deficient alkenes // Tetrahedron Letters. 2018. Vol. 59. No. 17. pp. 1630-1634.
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Salin A. V., Ilin A. V., Faskhutdinov R. I., Galkin V. I., R. Islamov D., Kataeva O. Tributylphosphine catalyzed addition of diphenylphosphine oxide to unsubstituted and substituted electron-deficient alkenes // Tetrahedron Letters. 2018. Vol. 59. No. 17. pp. 1630-1634.
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TY - JOUR
DO - 10.1016/j.tetlet.2018.03.040
UR - https://doi.org/10.1016/j.tetlet.2018.03.040
TI - Tributylphosphine catalyzed addition of diphenylphosphine oxide to unsubstituted and substituted electron-deficient alkenes
T2 - Tetrahedron Letters
AU - Salin, Alexey V.
AU - Ilin, Anton V
AU - Faskhutdinov, Rustem I
AU - Galkin, Vladimir I.
AU - R. Islamov, Daut
AU - Kataeva, O.N.
PY - 2018
DA - 2018/04/01
PB - Elsevier
SP - 1630-1634
IS - 17
VL - 59
SN - 0040-4039
SN - 1873-3581
ER -
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@article{2018_Salin,
author = {Alexey V. Salin and Anton V Ilin and Rustem I Faskhutdinov and Vladimir I. Galkin and Daut R. Islamov and O.N. Kataeva},
title = {Tributylphosphine catalyzed addition of diphenylphosphine oxide to unsubstituted and substituted electron-deficient alkenes},
journal = {Tetrahedron Letters},
year = {2018},
volume = {59},
publisher = {Elsevier},
month = {apr},
url = {https://doi.org/10.1016/j.tetlet.2018.03.040},
number = {17},
pages = {1630--1634},
doi = {10.1016/j.tetlet.2018.03.040}
}
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Salin, Alexey V., et al. “Tributylphosphine catalyzed addition of diphenylphosphine oxide to unsubstituted and substituted electron-deficient alkenes.” Tetrahedron Letters, vol. 59, no. 17, Apr. 2018, pp. 1630-1634. https://doi.org/10.1016/j.tetlet.2018.03.040.
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