N-Vinylation of Aromatic Sulfonamides Using Calcium Carbide as a Concise Solid Alkyne Source
Publication type: Journal Article
Publication date: 2023-04-01
scimago Q3
wos Q3
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
An efficient method for N-vinylation of aromatic sulfonamides using calcium carbide as a concise solid alkyne source is described. A series of N-vinyl aromatic sulfonamides are easily synthesized by this strategy. Notable features of this protocol are the use of an inexpensive and easy-to-handle solid alkyne source instead of flammable and explosive gaseous acetylene, transition metal-free catalysts, good functional group tolerance, and simple workup procedures. The synthesis of representative product can also be extended to gram scale.
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Liao H., Zheng L. N-Vinylation of Aromatic Sulfonamides Using Calcium Carbide as a Concise Solid Alkyne Source // Tetrahedron Letters. 2023. Vol. 120. p. 154445.
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Liao H., Zheng L. N-Vinylation of Aromatic Sulfonamides Using Calcium Carbide as a Concise Solid Alkyne Source // Tetrahedron Letters. 2023. Vol. 120. p. 154445.
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TY - JOUR
DO - 10.1016/j.tetlet.2023.154445
UR - https://doi.org/10.1016/j.tetlet.2023.154445
TI - N-Vinylation of Aromatic Sulfonamides Using Calcium Carbide as a Concise Solid Alkyne Source
T2 - Tetrahedron Letters
AU - Liao, Haiyan
AU - Zheng, Lei
PY - 2023
DA - 2023/04/01
PB - Elsevier
SP - 154445
VL - 120
SN - 0040-4039
SN - 1873-3581
ER -
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BibTex (up to 50 authors)
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@article{2023_Liao,
author = {Haiyan Liao and Lei Zheng},
title = {N-Vinylation of Aromatic Sulfonamides Using Calcium Carbide as a Concise Solid Alkyne Source},
journal = {Tetrahedron Letters},
year = {2023},
volume = {120},
publisher = {Elsevier},
month = {apr},
url = {https://doi.org/10.1016/j.tetlet.2023.154445},
pages = {154445},
doi = {10.1016/j.tetlet.2023.154445}
}