volume 57 issue 1-3 pages 307-321

Syntheses and lipophilicities of tetraarylborate ions substituted with many trifluoromethyl groups

Publication typeJournal Article
Publication date1992-04-01
scimago Q3
wos Q3
SJR0.333
CiteScore3.7
Impact factor1.9
ISSN00221139, 18733328
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Environmental Chemistry
Abstract
Syntheses were investigated using various tetraarylborate ions with a large number of trifluoromethyl groups: tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; tetrakis [3,5-bis(1-methoxy-2,2,2-trifluoro-1-(trifluoromethyl)ethyl) phenyl] borate; tetrakis[3-(1- methoxy-2,2,2-trifluoro-1-(trifluoromethyl)ethyl)-5-(trifluoromethyl)phenyl] borate; and tetrakis[3-(2,2,2- trifluoro-1-(2,2,2-trifluoroethyoxy)-1-(trifluoromethyl)ethyl)-5- (trifluoromethyl)phenyl]borate ions. The preparation of Grignard reagents and the subsequent reaction with boron trifluoride etherate are important steps for a higher yield and easier isolation of the product. Sodium- and tetramethylammonium salts of these borate ions are soluble in halocarbon solvents such as dichloromethane, chloroform and 1,2-dibromotetrafluoroethane.
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GOST Copy
Fujiki K. et al. Syntheses and lipophilicities of tetraarylborate ions substituted with many trifluoromethyl groups // Journal of Fluorine Chemistry. 1992. Vol. 57. No. 1-3. pp. 307-321.
GOST all authors (up to 50) Copy
Fujiki K., Kashiwagi M., MIYAMOTO H., Sonoda A., Ichikawa J., Kobayashi H., SONODA T. Syntheses and lipophilicities of tetraarylborate ions substituted with many trifluoromethyl groups // Journal of Fluorine Chemistry. 1992. Vol. 57. No. 1-3. pp. 307-321.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1016/s0022-1139(00)82842-0
UR - https://doi.org/10.1016/s0022-1139(00)82842-0
TI - Syntheses and lipophilicities of tetraarylborate ions substituted with many trifluoromethyl groups
T2 - Journal of Fluorine Chemistry
AU - Fujiki, Kanji
AU - Kashiwagi, Mitsuyoshi
AU - MIYAMOTO, HIDEYUKI
AU - Sonoda, Akinari
AU - Ichikawa, J.
AU - Kobayashi, Hiroshi
AU - SONODA, Takaaki
PY - 1992
DA - 1992/04/01
PB - Elsevier
SP - 307-321
IS - 1-3
VL - 57
SN - 0022-1139
SN - 1873-3328
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{1992_Fujiki,
author = {Kanji Fujiki and Mitsuyoshi Kashiwagi and HIDEYUKI MIYAMOTO and Akinari Sonoda and J. Ichikawa and Hiroshi Kobayashi and Takaaki SONODA},
title = {Syntheses and lipophilicities of tetraarylborate ions substituted with many trifluoromethyl groups},
journal = {Journal of Fluorine Chemistry},
year = {1992},
volume = {57},
publisher = {Elsevier},
month = {apr},
url = {https://doi.org/10.1016/s0022-1139(00)82842-0},
number = {1-3},
pages = {307--321},
doi = {10.1016/s0022-1139(00)82842-0}
}
MLA
Cite this
MLA Copy
Fujiki, Kanji, et al. “Syntheses and lipophilicities of tetraarylborate ions substituted with many trifluoromethyl groups.” Journal of Fluorine Chemistry, vol. 57, no. 1-3, Apr. 1992, pp. 307-321. https://doi.org/10.1016/s0022-1139(00)82842-0.