Energy & Fuels

, том 29 , издание 8 , страницы 4768-4773

Catalytic Aquathermolysis of Heavy Oil with Iron Tris(acetylacetonate): Changes of Heavy Oil Composition and in Situ Formation of Magnetic Nanoparticles

Andrey Galukhin ¹

Anton A Erokhin ¹

Yuri N. Osin ¹

Danis K Nurgaliev ¹

Скрыть аффилиации авторов Показать аффилиации авторов: 1 аффилиация

Kazan Federal University, 18 Kremlevskaya Street, Kazan 420008, Russia |

Тип публикации: Journal Article

Дата публикации: 2015-07-16

American Chemical Society (ACS)

Energy & Fuels

scimago Q1

wos Q1

БС1

SJR: 1.124

CiteScore: 9.5

Impact factor: 5.3

ISSN: 08870624, 15205029

DOI: 10.1021/acs.energyfuels.5b00587

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General Chemical Engineering

Energy Engineering and Power Technology

Fuel Technology

Краткое описание

We investigated the influence of catalytic aquathermolysis on the composition changes of Ashal’cha heavy oil. The synergetic effect of organic solvent and an oil-soluble catalyst leads to deep conversion of resins into light components. Composition changes of resins and asphaltenes before and after aquathermolysis were investigated by proton nuclear magnetic resonance (1H NMR), Fourier transform infrared spectroscopy (FTIR), matrix-assisted laser desorption/ionization mass spectrometry (MALDI MS), and elemental analysis. It was shown that iron(III) tris(acetylacetonate) forms magnetic nanoparticles (MNPs) during aquathermolysis of heavy oil without any addition of surfactants. Composition of MNPs was determined as a mixture of hematite, magnetite, and maghemite. It turns out that obtained MNPs possess superparamagnetic properties of single-domain nanoparticles.

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Galukhin A. et al. Catalytic Aquathermolysis of Heavy Oil with Iron Tris(acetylacetonate): Changes of Heavy Oil Composition and in Situ Formation of Magnetic Nanoparticles // Energy & Fuels. 2015. Vol. 29. No. 8. pp. 4768-4773.

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Galukhin A., Erokhin A. A., Osin Y. N., Nurgaliev D. K. Catalytic Aquathermolysis of Heavy Oil with Iron Tris(acetylacetonate): Changes of Heavy Oil Composition and in Situ Formation of Magnetic Nanoparticles // Energy & Fuels. 2015. Vol. 29. No. 8. pp. 4768-4773.

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TY - JOUR

DO - 10.1021/acs.energyfuels.5b00587

UR - https://doi.org/10.1021/acs.energyfuels.5b00587

TI - Catalytic Aquathermolysis of Heavy Oil with Iron Tris(acetylacetonate): Changes of Heavy Oil Composition and in Situ Formation of Magnetic Nanoparticles

T2 - Energy & Fuels

AU - Galukhin, Andrey

AU - Erokhin, Anton A

AU - Osin, Yuri N.

AU - Nurgaliev, Danis K

PY - 2015

DA - 2015/07/16

PB - American Chemical Society (ACS)

SP - 4768-4773

IS - 8

VL - 29

SN - 0887-0624

SN - 1520-5029

ER -

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@article{2015_Galukhin,

author = {Andrey Galukhin and Anton A Erokhin and Yuri N. Osin and Danis K Nurgaliev},

title = {Catalytic Aquathermolysis of Heavy Oil with Iron Tris(acetylacetonate): Changes of Heavy Oil Composition and in Situ Formation of Magnetic Nanoparticles},

journal = {Energy & Fuels},

year = {2015},

volume = {29},

publisher = {American Chemical Society (ACS)},

month = {jul},

url = {https://doi.org/10.1021/acs.energyfuels.5b00587},

number = {8},

pages = {4768--4773},

doi = {10.1021/acs.energyfuels.5b00587}

}

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Galukhin, Andrey, et al. “Catalytic Aquathermolysis of Heavy Oil with Iron Tris(acetylacetonate): Changes of Heavy Oil Composition and in Situ Formation of Magnetic Nanoparticles.” Energy & Fuels, vol. 29, no. 8, Jul. 2015, pp. 4768-4773. https://doi.org/10.1021/acs.energyfuels.5b00587.