Silver(I) Ethynide Coordination Networks and Clusters Assembled with tert-Butylphosphonic Acid
Publication type: Journal Article
Publication date: 2012-07-31
scimago Q1
wos Q1
SJR: 0.958
CiteScore: 7.4
Impact factor: 4.7
ISSN: 00201669, 1520510X
PubMed ID:
22849630
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Variation of the reaction conditions with AgC≡CR (R = Ph, C(6)H(4)OCH(3)-4, (t)Bu), (t)BuPO(3)H(2), and AgX (X = NO(3), BF(4)) as starting materials afforded four new silver(I) ethynide complexes incorporating the tert-butylphosphonate ligand, namely, 3AgC≡CPh·Ag(2)(t)BuPO(3)·Ag(t)BuPO(3)H·2AgNO(3) (1), 2AgC≡CC(6)H(4)OCH(3)-4·Ag(2)(t)BuPO(3)·2AgNO(3) (2), [{Ag(5)(NO(3)@Ag(18))Ag(5)}((t)BuC≡C)(16)((t)BuPO(3))(4)(H(2)O)(3)][{Ag(5)(NO(3)@Ag(18))Ag(5)} ((t)BuC≡C)(16)((t)BuPO(3))(4)(H(2)O)(4)]·3SiF(6)·4.5H(2)O·3.5MeOH (3), and [{Ag(8)(Cl@Ag(14))}((t)BuC≡C)(14)((t)BuPO(3))(2)F(2)(H(2)O)(2)]BF(4)·3.5H(2)O (4). Single-crystal X-ray analysis revealed that complexes 1 and 2 display different layer-type coordination networks, while 3 and 4 contain high-nuclearity silver(I) composite clusters enclosing nitrate and chloride template ions, respectively, that are supported by (t)BuPO(3)(2-) ligands.
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Xie Y., Mak T. C. W. Silver(I) Ethynide Coordination Networks and Clusters Assembled with tert-Butylphosphonic Acid // Inorganic Chemistry. 2012. Vol. 51. No. 16. pp. 8640-8642.
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Xie Y., Mak T. C. W. Silver(I) Ethynide Coordination Networks and Clusters Assembled with tert-Butylphosphonic Acid // Inorganic Chemistry. 2012. Vol. 51. No. 16. pp. 8640-8642.
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TY - JOUR
DO - 10.1021/ic300913u
UR - https://doi.org/10.1021/ic300913u
TI - Silver(I) Ethynide Coordination Networks and Clusters Assembled with tert-Butylphosphonic Acid
T2 - Inorganic Chemistry
AU - Xie, Yun-Peng
AU - Mak, Thomas C. W.
PY - 2012
DA - 2012/07/31
PB - American Chemical Society (ACS)
SP - 8640-8642
IS - 16
VL - 51
PMID - 22849630
SN - 0020-1669
SN - 1520-510X
ER -
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BibTex (up to 50 authors)
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@article{2012_Xie,
author = {Yun-Peng Xie and Thomas C. W. Mak},
title = {Silver(I) Ethynide Coordination Networks and Clusters Assembled with tert-Butylphosphonic Acid},
journal = {Inorganic Chemistry},
year = {2012},
volume = {51},
publisher = {American Chemical Society (ACS)},
month = {jul},
url = {https://doi.org/10.1021/ic300913u},
number = {16},
pages = {8640--8642},
doi = {10.1021/ic300913u}
}
Cite this
MLA
Copy
Xie, Yun-Peng, and Thomas C. W. Mak. “Silver(I) Ethynide Coordination Networks and Clusters Assembled with tert-Butylphosphonic Acid.” Inorganic Chemistry, vol. 51, no. 16, Jul. 2012, pp. 8640-8642. https://doi.org/10.1021/ic300913u.