A convenient method for the synthesis of N2,N2-dimethylguanosine by reductive carbon-sulfur bond cleavage with tributyltin hydride
Publication type: Journal Article
Publication date: 1991-02-01
scimago Q2
wos Q1
SJR: 0.737
CiteScore: 6.1
Impact factor: 3.6
ISSN: 00223263, 15206904
Organic Chemistry
Abstract
A new method for the N-methylation of guanosine is described. The 1,3-benzodithiol-2-yl group was introduced into the 2-amino group of 2',3',5'-tri-O-acetylguanosine (3) and then converted into a methyl group by reductive C-S bond cleavage with tributyltin hydride. This method was also applied to the synthesis of N 2 ,N 2 -dimethylguanosine. A similar reductive conversion of a (p-tolylthio) methyl group into a methyl group was studied
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Sekine M., Satoh T. A convenient method for the synthesis of N2,N2-dimethylguanosine by reductive carbon-sulfur bond cleavage with tributyltin hydride // Journal of Organic Chemistry. 1991. Vol. 56. No. 3. pp. 1224-1227.
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Sekine M., Satoh T. A convenient method for the synthesis of N2,N2-dimethylguanosine by reductive carbon-sulfur bond cleavage with tributyltin hydride // Journal of Organic Chemistry. 1991. Vol. 56. No. 3. pp. 1224-1227.
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RIS
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TY - JOUR
DO - 10.1021/jo00003a052
UR - https://doi.org/10.1021/jo00003a052
TI - A convenient method for the synthesis of N2,N2-dimethylguanosine by reductive carbon-sulfur bond cleavage with tributyltin hydride
T2 - Journal of Organic Chemistry
AU - Sekine, Mitsuo
AU - Satoh, Takahiko
PY - 1991
DA - 1991/02/01
PB - American Chemical Society (ACS)
SP - 1224-1227
IS - 3
VL - 56
SN - 0022-3263
SN - 1520-6904
ER -
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BibTex (up to 50 authors)
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@article{1991_Sekine,
author = {Mitsuo Sekine and Takahiko Satoh},
title = {A convenient method for the synthesis of N2,N2-dimethylguanosine by reductive carbon-sulfur bond cleavage with tributyltin hydride},
journal = {Journal of Organic Chemistry},
year = {1991},
volume = {56},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://doi.org/10.1021/jo00003a052},
number = {3},
pages = {1224--1227},
doi = {10.1021/jo00003a052}
}
Cite this
MLA
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Sekine, Mitsuo, and Takahiko Satoh. “A convenient method for the synthesis of N2,N2-dimethylguanosine by reductive carbon-sulfur bond cleavage with tributyltin hydride.” Journal of Organic Chemistry, vol. 56, no. 3, Feb. 1991, pp. 1224-1227. https://doi.org/10.1021/jo00003a052.