Crystal Growth and Design, volume 18, issue 2, pages 879-882

Exploring the Peculiarities of LiFePO4 Hydrothermal Synthesis Using in Situ Calvet Calorimetry

Publication typeJournal Article
Publication date2017-12-29
Quartile SCImago
Q2
Quartile WOS
Q1
Impact factor3.8
ISSN15287483, 15287505
General Chemistry
Condensed Matter Physics
General Materials Science
Abstract
Peculiarities of the hydrothermal synthesis of the lithium iron phosphate cathode material are studied using in situ Calvet calorimetry. Staging and temperature intervals of the phase formation process are determined as a function of the concentration of the initial reagents. Obtained results revealed a clear correlation between observed heat absorption behavior and lattice parameters, morphology, and electrochemical performance of the obtained LiFePO4 materials. Lowering temperature of the precursor dehydration leads to better Li/Fe ordering, smaller particle size of LiFePO4 samples, and the highest charge–discharge capacity measured in the Li-ion cell.

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GOST Copy
Sharikov F. Yu. et al. Exploring the Peculiarities of LiFePO4 Hydrothermal Synthesis Using in Situ Calvet Calorimetry // Crystal Growth and Design. 2017. Vol. 18. No. 2. pp. 879-882.
GOST all authors (up to 50) Copy
Sharikov F. Yu., Drozhzhin O. A., Sumanov V. D., Baranov A. N., Abakumov A. M., Antipov E. V. Exploring the Peculiarities of LiFePO4 Hydrothermal Synthesis Using in Situ Calvet Calorimetry // Crystal Growth and Design. 2017. Vol. 18. No. 2. pp. 879-882.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1021/ACS.CGD.7B01366
UR - https://doi.org/10.1021%2FACS.CGD.7B01366
TI - Exploring the Peculiarities of LiFePO4 Hydrothermal Synthesis Using in Situ Calvet Calorimetry
T2 - Crystal Growth and Design
AU - Sharikov, Felix Yu
AU - Sumanov, Vasiliy D.
AU - Baranov, Andrey N.
AU - Drozhzhin, Oleg A.
AU - Abakumov, Artem M.
AU - Antipov, Evgeny V.
PY - 2017
DA - 2017/12/29 00:00:00
PB - American Chemical Society (ACS)
SP - 879-882
IS - 2
VL - 18
SN - 1528-7483
SN - 1528-7505
ER -
BibTex |
Cite this
BibTex Copy
@article{2017_Sharikov,
author = {Felix Yu Sharikov and Vasiliy D. Sumanov and Andrey N. Baranov and Oleg A. Drozhzhin and Artem M. Abakumov and Evgeny V. Antipov},
title = {Exploring the Peculiarities of LiFePO4 Hydrothermal Synthesis Using in Situ Calvet Calorimetry},
journal = {Crystal Growth and Design},
year = {2017},
volume = {18},
publisher = {American Chemical Society (ACS)},
month = {dec},
url = {https://doi.org/10.1021%2FACS.CGD.7B01366},
number = {2},
pages = {879--882},
doi = {10.1021/ACS.CGD.7B01366}
}
MLA
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MLA Copy
Sharikov, Felix Yu., et al. “Exploring the Peculiarities of LiFePO4 Hydrothermal Synthesis Using in Situ Calvet Calorimetry.” Crystal Growth and Design, vol. 18, no. 2, Dec. 2017, pp. 879-882. https://doi.org/10.1021%2FACS.CGD.7B01366.
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