Biferrocene-Based Diphosphine Ligands: Synthesis and Application of Walphos Analogues in Asymmetric Hydrogenations
Тип публикации: Journal Article
Дата публикации: 2013-02-11
SCImago Q2
WOS Q2
БС1
SJR: 0.55
CiteScore: 4.6
Impact factor: 2.4
ISSN: 02767333, 15206041
PubMed ID:
23457421
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
A total of four biferrocene-based Walphos-type ligands have been synthesized, structurally characterized, and tested in the rhodium-, ruthenium- and iridium-catalyzed hydrogenation of alkenes and ketones. Negishi coupling conditions allowed the biferrocene backbone of these diphosphine ligands to be built up diastereoselectively from the two nonidentical and nonracemic ferrocene fragments (R)-1-(N,N-dimethylamino)ethylferrocene and (SFc)-2-bromoiodoferrocene. The molecular structures of (SFc)-2-bromoiodoferrocene, the coupling product, two ligands, and the two complexes ([PdCl2(L)] and [RuCl(p-cymene)(L)]PF6) were determined by X-ray diffraction. The structural features of complexes and the catalysis results obtained with the newly synthesized biferrocene-based ligands were compared with those of the corresponding Walphos ligands.
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ГОСТ
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Zirakzadeh A. et al. Biferrocene-Based Diphosphine Ligands: Synthesis and Application of Walphos Analogues in Asymmetric Hydrogenations // Organometallics. 2013. Vol. 32. No. 4. pp. 1075-1084.
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Zirakzadeh A., Gross M. A., Wang Y., Mereiter K., Spindler F., Weissensteiner W. Biferrocene-Based Diphosphine Ligands: Synthesis and Application of Walphos Analogues in Asymmetric Hydrogenations // Organometallics. 2013. Vol. 32. No. 4. pp. 1075-1084.
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TY - JOUR
DO - 10.1021/om3012147
UR - https://doi.org/10.1021/om3012147
TI - Biferrocene-Based Diphosphine Ligands: Synthesis and Application of Walphos Analogues in Asymmetric Hydrogenations
T2 - Organometallics
AU - Zirakzadeh, Afrooz
AU - Gross, Manuela A
AU - Wang, Yaping
AU - Mereiter, K.
AU - Spindler, Felix
AU - Weissensteiner, Walter
PY - 2013
DA - 2013/02/11
PB - American Chemical Society (ACS)
SP - 1075-1084
IS - 4
VL - 32
PMID - 23457421
SN - 0276-7333
SN - 1520-6041
ER -
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@article{2013_Zirakzadeh,
author = {Afrooz Zirakzadeh and Manuela A Gross and Yaping Wang and K. Mereiter and Felix Spindler and Walter Weissensteiner},
title = {Biferrocene-Based Diphosphine Ligands: Synthesis and Application of Walphos Analogues in Asymmetric Hydrogenations},
journal = {Organometallics},
year = {2013},
volume = {32},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://doi.org/10.1021/om3012147},
number = {4},
pages = {1075--1084},
doi = {10.1021/om3012147}
}
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MLA
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Zirakzadeh, Afrooz, et al. “Biferrocene-Based Diphosphine Ligands: Synthesis and Application of Walphos Analogues in Asymmetric Hydrogenations.” Organometallics, vol. 32, no. 4, Feb. 2013, pp. 1075-1084. https://doi.org/10.1021/om3012147.
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