Analytical Chemistry, volume 57, issue 4, pages 864-871
Determination of structural characteristics of saturates from diesel and kerosine fuels by carbon-13 nuclear magnetic resonance spectrometry
Publication type: Journal Article
Publication date: 1985-04-01
Journal:
Analytical Chemistry
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor: 7.4
ISSN: 00032700, 15206882, 21542686
Analytical Chemistry
Abstract
Two saturated hydrocarbon fractions, one mainly consisting of n-alkanes and the other containing only branched plus cyclic saturates, have been separated from each of a variety of diesel fuels (approximate boiling range 230-320/sup 0/C) and kerosene fuels (approximately 190-230/sup 0/C) using silica chromatography and urea clathration. The n-alkane fractions have been simply characterized by using conventional /sup 13/C NMR spectrometry, yielding average carbon chain lengths. The branched plus cyclic saturates fractions have been characterized by using the gated spin echo (GASPE) /sup 13/C NMR subspectra for each CH/sub n/ group type (n = 0 to 3) and allows the fractional abundances of CH/sub n/ groups to be measured. These data have been employed in devising and calculating a number of novel average structure parameters which report on the extent of branching and occurrence of ring structures in the fractions investigated. Spectral data are also used to identify some specific submolecular structures. 29 references, 7 figures, 4 tables.
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Cookson D. J., Smith B. Determination of structural characteristics of saturates from diesel and kerosine fuels by carbon-13 nuclear magnetic resonance spectrometry // Analytical Chemistry. 1985. Vol. 57. No. 4. pp. 864-871.
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Cookson D. J., Smith B. Determination of structural characteristics of saturates from diesel and kerosine fuels by carbon-13 nuclear magnetic resonance spectrometry // Analytical Chemistry. 1985. Vol. 57. No. 4. pp. 864-871.
Cite this
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TY - JOUR
DO - 10.1021/ac00281a020
UR - https://doi.org/10.1021/ac00281a020
TI - Determination of structural characteristics of saturates from diesel and kerosine fuels by carbon-13 nuclear magnetic resonance spectrometry
T2 - Analytical Chemistry
AU - Cookson, David J.
AU - Smith, Brian E.
PY - 1985
DA - 1985/04/01
PB - American Chemical Society (ACS)
SP - 864-871
IS - 4
VL - 57
SN - 0003-2700
SN - 1520-6882
SN - 2154-2686
ER -
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BibTex
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@article{1985_Cookson,
author = {David J. Cookson and Brian E. Smith},
title = {Determination of structural characteristics of saturates from diesel and kerosine fuels by carbon-13 nuclear magnetic resonance spectrometry},
journal = {Analytical Chemistry},
year = {1985},
volume = {57},
publisher = {American Chemical Society (ACS)},
month = {apr},
url = {https://doi.org/10.1021/ac00281a020},
number = {4},
pages = {864--871},
doi = {10.1021/ac00281a020}
}
Cite this
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Cookson, David J., and Brian E. Smith. “Determination of structural characteristics of saturates from diesel and kerosine fuels by carbon-13 nuclear magnetic resonance spectrometry.” Analytical Chemistry, vol. 57, no. 4, Apr. 1985, pp. 864-871. https://doi.org/10.1021/ac00281a020.