Defect and Surface Area Control in Hydrothermally Synthesized LiMn0.8Fe0.2PO4 Using a Phosphate Based Structure Directing Agent
J. Schoiber
1
,
Gerold Tippelt
1
,
Günther Redhammer
1
,
Chihiro Yada
2
,
Oleksandr Dolotko
3
,
R. J. F. Berger
1
,
N. Hüsing
1
3
Maier-Leibnitz Zentrum MLZ Forschungsreaktor München FRM-II, Lichtenbergstrasse 1, 85747 Garching, Germany
|
Тип публикации: Journal Article
Дата публикации: 2015-08-24
scimago Q2
wos Q1
БС1
SJR: 0.633
CiteScore: 5.6
Impact factor: 3.4
ISSN: 15287483, 15287505
General Chemistry
Condensed Matter Physics
General Materials Science
Краткое описание
As confirmed by ion coupled plasma-optical emission spectroscopy and powder X-ray diffraction, stoichiometrically pure samples of olivine type LiFe0.2Mn0.8PO4 in the presence of a phosphoric acid ester based structure directing agent have been prepared. A Rietveld analysis of X-ray and n0 diffraction data suggests that the solids are largely free of defect occupation of Fe at the lithium sites. This is confirmed by 57Fe-Mosbauer spectroscopic investigations. The use of the structure directing surfactant results in significantly higher specific surface areas (SSA) and smaller particle sizes as compared to samples prepared without using a surfactant.
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Schoiber J. et al. Defect and Surface Area Control in Hydrothermally Synthesized LiMn0.8Fe0.2PO4 Using a Phosphate Based Structure Directing Agent // Crystal Growth and Design. 2015. Vol. 15. No. 9. pp. 4213-4218.
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Schoiber J., Tippelt G., Redhammer G., Yada C., Dolotko O., Berger R. J. F., Hüsing N. Defect and Surface Area Control in Hydrothermally Synthesized LiMn0.8Fe0.2PO4 Using a Phosphate Based Structure Directing Agent // Crystal Growth and Design. 2015. Vol. 15. No. 9. pp. 4213-4218.
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TY - JOUR
DO - 10.1021/acs.cgd.5b00324
UR - https://doi.org/10.1021/acs.cgd.5b00324
TI - Defect and Surface Area Control in Hydrothermally Synthesized LiMn0.8Fe0.2PO4 Using a Phosphate Based Structure Directing Agent
T2 - Crystal Growth and Design
AU - Schoiber, J.
AU - Tippelt, Gerold
AU - Redhammer, Günther
AU - Yada, Chihiro
AU - Dolotko, Oleksandr
AU - Berger, R. J. F.
AU - Hüsing, N.
PY - 2015
DA - 2015/08/24
PB - American Chemical Society (ACS)
SP - 4213-4218
IS - 9
VL - 15
SN - 1528-7483
SN - 1528-7505
ER -
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@article{2015_Schoiber,
author = {J. Schoiber and Gerold Tippelt and Günther Redhammer and Chihiro Yada and Oleksandr Dolotko and R. J. F. Berger and N. Hüsing},
title = {Defect and Surface Area Control in Hydrothermally Synthesized LiMn0.8Fe0.2PO4 Using a Phosphate Based Structure Directing Agent},
journal = {Crystal Growth and Design},
year = {2015},
volume = {15},
publisher = {American Chemical Society (ACS)},
month = {aug},
url = {https://doi.org/10.1021/acs.cgd.5b00324},
number = {9},
pages = {4213--4218},
doi = {10.1021/acs.cgd.5b00324}
}
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MLA
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Schoiber, J., et al. “Defect and Surface Area Control in Hydrothermally Synthesized LiMn0.8Fe0.2PO4 Using a Phosphate Based Structure Directing Agent.” Crystal Growth and Design, vol. 15, no. 9, Aug. 2015, pp. 4213-4218. https://doi.org/10.1021/acs.cgd.5b00324.