volume 35 issue 6 pages 2549-2558

Chemically Understanding the Liquid-Phase Synthesis of Argyrodite Solid Electrolyte Li6PS5Cl with the Highest Ionic Conductivity for All-Solid-State Batteries

Radian Febi Indrawan 1
Hirotada GAMO 1
Atsushi Nagai 1, 2
Atsunori Matsuda 1
Publication typeJournal Article
Publication date2023-03-10
scimago Q1
wos Q1
SJR2.065
CiteScore12.0
Impact factor7.0
ISSN08974756, 15205002
Materials Chemistry
General Chemistry
General Chemical Engineering
Abstract
Solid electrolytes (SEs), which essentially act as both the electron separator and ion conductor, play an important role in all-solid-state lithium-ion batteries. Liquid-phase synthesis is one of the promising methods as the synthesis of SEs is easily scalable and consumes lower energy. However, due to the complexity of the SEs prepared by liquid-phase synthesis, many problems such as impurities arise, making the liquid electrolytes irreplaceable. This study examines and solves the question why Li3PO4 is produced as an impurity upon preparing Li6PS5Cl argyrodite by approaching the chemical factors. This is accomplished by replacing the hydroxide-based solvent with a thiol-based solvent through liquid-phase synthesis. As a result, the absence of Li3PO4 from the Li6PS5Cl SEs in this study resulted in Li6PS5Cl attaining the highest ionic conductivity value (>2 mS·cm–1) ever obtained through liquid-phase synthesis. Furthermore, the absence of Li3PO4 in the argyrodite SE could magnificently increase the cell's capacity with remarkable stability.
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GOST Copy
Indrawan R. F. et al. Chemically Understanding the Liquid-Phase Synthesis of Argyrodite Solid Electrolyte Li6PS5Cl with the Highest Ionic Conductivity for All-Solid-State Batteries // Chemistry of Materials. 2023. Vol. 35. No. 6. pp. 2549-2558.
GOST all authors (up to 50) Copy
Indrawan R. F., GAMO H., Nagai A., Matsuda A. Chemically Understanding the Liquid-Phase Synthesis of Argyrodite Solid Electrolyte Li6PS5Cl with the Highest Ionic Conductivity for All-Solid-State Batteries // Chemistry of Materials. 2023. Vol. 35. No. 6. pp. 2549-2558.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1021/acs.chemmater.2c03818
UR - https://pubs.acs.org/doi/10.1021/acs.chemmater.2c03818
TI - Chemically Understanding the Liquid-Phase Synthesis of Argyrodite Solid Electrolyte Li6PS5Cl with the Highest Ionic Conductivity for All-Solid-State Batteries
T2 - Chemistry of Materials
AU - Indrawan, Radian Febi
AU - GAMO, Hirotada
AU - Nagai, Atsushi
AU - Matsuda, Atsunori
PY - 2023
DA - 2023/03/10
PB - American Chemical Society (ACS)
SP - 2549-2558
IS - 6
VL - 35
SN - 0897-4756
SN - 1520-5002
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2023_Indrawan,
author = {Radian Febi Indrawan and Hirotada GAMO and Atsushi Nagai and Atsunori Matsuda},
title = {Chemically Understanding the Liquid-Phase Synthesis of Argyrodite Solid Electrolyte Li6PS5Cl with the Highest Ionic Conductivity for All-Solid-State Batteries},
journal = {Chemistry of Materials},
year = {2023},
volume = {35},
publisher = {American Chemical Society (ACS)},
month = {mar},
url = {https://pubs.acs.org/doi/10.1021/acs.chemmater.2c03818},
number = {6},
pages = {2549--2558},
doi = {10.1021/acs.chemmater.2c03818}
}
MLA
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MLA Copy
Indrawan, Radian Febi, et al. “Chemically Understanding the Liquid-Phase Synthesis of Argyrodite Solid Electrolyte Li6PS5Cl with the Highest Ionic Conductivity for All-Solid-State Batteries.” Chemistry of Materials, vol. 35, no. 6, Mar. 2023, pp. 2549-2558. https://pubs.acs.org/doi/10.1021/acs.chemmater.2c03818.