Chemistry of Materials, volume 31, issue 4, pages 1223-1230
Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers
Dmitry Baranov
1
,
Michael J. Lynch
1
,
Anna C Curtis
1
,
Alexa R Carollo
1
,
Callum R Douglass
1
,
Alina M Mateo Tejada
1
,
David M. Jonas
1
Publication type: Journal Article
Publication date: 2019-02-04
Journal:
Chemistry of Materials
Q1
Q1
SJR: 2.421
CiteScore: 14.1
Impact factor: 7.2
ISSN: 08974756, 15205002
Materials Chemistry
General Chemistry
General Chemical Engineering
Abstract
Oleylamine is widely used in nanomaterial and metal-halide perovskite synthesis. Impurities in commercially available oleylamine reagents are identified, purification procedures are explained, beneficial effects on lead chloride/oleylamine mixtures are documented, and impacts on materials synthesis are discussed. Suspensions of 0.12 mole fraction PbCl2, PbBr2, and PbI2 in purified, dried, and filtered oleylamine were found to form clear solutions upon heating to 100 °C. The infrared, Raman, and NMR spectra of oleylamine and a common trans impurity present in literature reference IR spectra are presented.
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GOST
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Baranov D. et al. Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers // Chemistry of Materials. 2019. Vol. 31. No. 4. pp. 1223-1230.
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Baranov D., Lynch M. J., Curtis A. C., Carollo A. R., Douglass C. R., Mateo Tejada A. M., Jonas D. M. Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers // Chemistry of Materials. 2019. Vol. 31. No. 4. pp. 1223-1230.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1021/acs.chemmater.8b04198
UR - https://doi.org/10.1021/acs.chemmater.8b04198
TI - Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers
T2 - Chemistry of Materials
AU - Baranov, Dmitry
AU - Lynch, Michael J.
AU - Curtis, Anna C
AU - Carollo, Alexa R
AU - Douglass, Callum R
AU - Mateo Tejada, Alina M
AU - Jonas, David M.
PY - 2019
DA - 2019/02/04
PB - American Chemical Society (ACS)
SP - 1223-1230
IS - 4
VL - 31
SN - 0897-4756
SN - 1520-5002
ER -
Cite this
BibTex (up to 50 authors)
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@article{2019_Baranov,
author = {Dmitry Baranov and Michael J. Lynch and Anna C Curtis and Alexa R Carollo and Callum R Douglass and Alina M Mateo Tejada and David M. Jonas},
title = {Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers},
journal = {Chemistry of Materials},
year = {2019},
volume = {31},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://doi.org/10.1021/acs.chemmater.8b04198},
number = {4},
pages = {1223--1230},
doi = {10.1021/acs.chemmater.8b04198}
}
Cite this
MLA
Copy
Baranov, Dmitry, et al. “Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers.” Chemistry of Materials, vol. 31, no. 4, Feb. 2019, pp. 1223-1230. https://doi.org/10.1021/acs.chemmater.8b04198.