Chemistry of Materials, volume 31, issue 4, pages 1223-1230
Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers
Dmitry Baranov
1
,
Michael J. Lynch
1
,
Anna C Curtis
1
,
Alexa R Carollo
1
,
Callum R Douglass
1
,
Alina M Mateo Tejada
1
,
David M. Jonas
1
1
Department of Chemistry, University of Colorado, 215 UCB, Boulder, Colorado 80309-0215, United States
|
Publication type: Journal Article
Publication date: 2019-02-04
Journal:
Chemistry of Materials
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor: 8.6
ISSN: 08974756, 15205002
Materials Chemistry
General Chemistry
General Chemical Engineering
Abstract
Oleylamine is widely used in nanomaterial and metal-halide perovskite synthesis. Impurities in commercially available oleylamine reagents are identified, purification procedures are explained, beneficial effects on lead chloride/oleylamine mixtures are documented, and impacts on materials synthesis are discussed. Suspensions of 0.12 mole fraction PbCl2, PbBr2, and PbI2 in purified, dried, and filtered oleylamine were found to form clear solutions upon heating to 100 °C. The infrared, Raman, and NMR spectra of oleylamine and a common trans impurity present in literature reference IR spectra are presented.
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Citations by publishers
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5
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15
20
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23 publications, 42.59%
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1 publication, 1.85%
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American Association for the Advancement of Science (AAAS)
1 publication, 1.85%
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Thieme
1 publication, 1.85%
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5
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15
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25
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- We do not take into account publications without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Baranov D. et al. Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers // Chemistry of Materials. 2019. Vol. 31. No. 4. pp. 1223-1230.
GOST all authors (up to 50)
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Baranov D., Lynch M. J., Curtis A. C., Carollo A. R., Douglass C. R., Mateo Tejada A. M., Jonas D. M. Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers // Chemistry of Materials. 2019. Vol. 31. No. 4. pp. 1223-1230.
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RIS
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TY - JOUR
DO - 10.1021/acs.chemmater.8b04198
UR - https://doi.org/10.1021/acs.chemmater.8b04198
TI - Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers
T2 - Chemistry of Materials
AU - Lynch, Michael J.
AU - Curtis, Anna C
AU - Carollo, Alexa R
AU - Douglass, Callum R
AU - Mateo Tejada, Alina M
AU - Baranov, Dmitry
AU - Jonas, David M.
PY - 2019
DA - 2019/02/04 00:00:00
PB - American Chemical Society (ACS)
SP - 1223-1230
IS - 4
VL - 31
SN - 0897-4756
SN - 1520-5002
ER -
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@article{2019_Baranov,
author = {Michael J. Lynch and Anna C Curtis and Alexa R Carollo and Callum R Douglass and Alina M Mateo Tejada and Dmitry Baranov and David M. Jonas},
title = {Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers},
journal = {Chemistry of Materials},
year = {2019},
volume = {31},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://doi.org/10.1021/acs.chemmater.8b04198},
number = {4},
pages = {1223--1230},
doi = {10.1021/acs.chemmater.8b04198}
}
Cite this
MLA
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Baranov, Dmitry, et al. “Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers.” Chemistry of Materials, vol. 31, no. 4, Feb. 2019, pp. 1223-1230. https://doi.org/10.1021/acs.chemmater.8b04198.