Solubility and Speciation of Ketoprofen and Aspirin in Supercritical CO2 by Infrared Spectroscopy
Тип публикации: Journal Article
Дата публикации: 2016-01-07
SCImago Q2
WOS Q3
БС2
SJR: 0.467
CiteScore: 3.7
Impact factor: 2.4
ISSN: 00219568, 15205134
General Chemistry
General Chemical Engineering
Краткое описание
The solubility of ketoprofen and aspirin in subcritical and supercritical CO2 was measured using FTIR absorption spectroscopy in the large range of temperature of 298.2–353.2 K and pressure of 5–35 MPa. The evolution of the solubility of both active pharmaceutical ingredients (APIs) was fitted using the Chrastil’s equation. In addition, the speciation of both APIs in monomeric and dimeric forms was explored by analyzing the characteristic carbonyl stretching vibrations of the carboxylic acid functions assigned to the dimers and monomers, respectively. Moreover, the evolution of the dimerization constant K of the two drugs as a function of the temperature and the pressure of scCO2 has been reported.
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ГОСТ
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Champeau M. et al. Solubility and Speciation of Ketoprofen and Aspirin in Supercritical CO2 by Infrared Spectroscopy // Journal of Chemical & Engineering Data. 2016. Vol. 61. No. 2. pp. 968-978.
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Champeau M., Thomassin J. M., Jérôme C., Tassaing T. Solubility and Speciation of Ketoprofen and Aspirin in Supercritical CO2 by Infrared Spectroscopy // Journal of Chemical & Engineering Data. 2016. Vol. 61. No. 2. pp. 968-978.
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TY - JOUR
DO - 10.1021/acs.jced.5b00812
UR - https://doi.org/10.1021/acs.jced.5b00812
TI - Solubility and Speciation of Ketoprofen and Aspirin in Supercritical CO2 by Infrared Spectroscopy
T2 - Journal of Chemical & Engineering Data
AU - Champeau, Mathilde
AU - Thomassin, Jean Michel
AU - Jérôme, Christine
AU - Tassaing, Thierry
PY - 2016
DA - 2016/01/07
PB - American Chemical Society (ACS)
SP - 968-978
IS - 2
VL - 61
SN - 0021-9568
SN - 1520-5134
ER -
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@article{2016_Champeau,
author = {Mathilde Champeau and Jean Michel Thomassin and Christine Jérôme and Thierry Tassaing},
title = {Solubility and Speciation of Ketoprofen and Aspirin in Supercritical CO2 by Infrared Spectroscopy},
journal = {Journal of Chemical & Engineering Data},
year = {2016},
volume = {61},
publisher = {American Chemical Society (ACS)},
month = {jan},
url = {https://doi.org/10.1021/acs.jced.5b00812},
number = {2},
pages = {968--978},
doi = {10.1021/acs.jced.5b00812}
}
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MLA
Скопировать
Champeau, Mathilde, et al. “Solubility and Speciation of Ketoprofen and Aspirin in Supercritical CO2 by Infrared Spectroscopy.” Journal of Chemical & Engineering Data, vol. 61, no. 2, Jan. 2016, pp. 968-978. https://doi.org/10.1021/acs.jced.5b00812.
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