Solubility Measurement and Thermodynamic Modeling of 4-Nitrophthalimide in Twelve Pure Solvents at Elevated Temperatures Ranging from (273.15 to 323.15) K
Тип публикации: Journal Article
Дата публикации: 2016-06-24
SCImago Q2
WOS Q2
БС2
SJR: 0.467
CiteScore: 3.7
Impact factor: 2.1
ISSN: 00219568, 15205134
General Chemistry
General Chemical Engineering
Краткое описание
The solubility of 4-nitrophthalimide in different solvents are of great importance for the design of its purification process via crystallization. The work reported new solubility data for 4-nitrophthalimide in 12 pure solvents of methanol, ethanol, isopropanol, cyclohexanone, acetone, acetonitrile, ethyl acetate, 2-butanone, chloroform, 1,4-dioxane benzyl alcohol and N,N-dimethylformamide. They were determined by a high-performance liquid chromatography at T = (273.15 to 323.15) K under pressure of 0.1 MPa. The 4-nitrophthalimide solubility in the selected solvents increased with the temperature increase. At a given temperature, the solubility of 4-nitrophthalimide is largest in N,N-dimethylformamide and lowest in chloroform. The solubility data in the these solvents ranked as N,N-dimethylformamide > cyclohexanone > (1,4-dioxane, acetone, 2-butanone, benzyl alcohol) > ethyl acetate > acetonitrile > methanol > ethanol > isopropanol > chloroform. The experimental solubility data were correlated by modified...
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Han S. et al. Solubility Measurement and Thermodynamic Modeling of 4-Nitrophthalimide in Twelve Pure Solvents at Elevated Temperatures Ranging from (273.15 to 323.15) K // Journal of Chemical & Engineering Data. 2016. Vol. 61. No. 7. pp. 2525-2535.
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Han S., Long M., Du C., Xu J., Cheng C., Wang J., Zhao H. Solubility Measurement and Thermodynamic Modeling of 4-Nitrophthalimide in Twelve Pure Solvents at Elevated Temperatures Ranging from (273.15 to 323.15) K // Journal of Chemical & Engineering Data. 2016. Vol. 61. No. 7. pp. 2525-2535.
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TY - JOUR
DO - 10.1021/acs.jced.6b00230
UR - https://doi.org/10.1021/acs.jced.6b00230
TI - Solubility Measurement and Thermodynamic Modeling of 4-Nitrophthalimide in Twelve Pure Solvents at Elevated Temperatures Ranging from (273.15 to 323.15) K
T2 - Journal of Chemical & Engineering Data
AU - Han, Shuo
AU - Long, Meng
AU - Du, Cunbin
AU - Xu, Jian
AU - Cheng, Chao
AU - Wang, Jian
AU - Zhao, Hongkun
PY - 2016
DA - 2016/06/24
PB - American Chemical Society (ACS)
SP - 2525-2535
IS - 7
VL - 61
SN - 0021-9568
SN - 1520-5134
ER -
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@article{2016_Han,
author = {Shuo Han and Meng Long and Cunbin Du and Jian Xu and Chao Cheng and Jian Wang and Hongkun Zhao},
title = {Solubility Measurement and Thermodynamic Modeling of 4-Nitrophthalimide in Twelve Pure Solvents at Elevated Temperatures Ranging from (273.15 to 323.15) K},
journal = {Journal of Chemical & Engineering Data},
year = {2016},
volume = {61},
publisher = {American Chemical Society (ACS)},
month = {jun},
url = {https://doi.org/10.1021/acs.jced.6b00230},
number = {7},
pages = {2525--2535},
doi = {10.1021/acs.jced.6b00230}
}
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Han, Shuo, et al. “Solubility Measurement and Thermodynamic Modeling of 4-Nitrophthalimide in Twelve Pure Solvents at Elevated Temperatures Ranging from (273.15 to 323.15) K.” Journal of Chemical & Engineering Data, vol. 61, no. 7, Jun. 2016, pp. 2525-2535. https://doi.org/10.1021/acs.jced.6b00230.
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