Journal of Organic Chemistry

, том 85 , издание 23 , страницы 15760-15766

Mechanochemical Synthesis of 1,2,6-Thiadiazine 1-Oxides from Sulfonimidamides and the Fluorescence Properties of the Products

Тип публикации: Journal Article

Дата публикации: 2020-11-23

American Chemical Society (ACS)

Journal of Organic Chemistry

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SJR: 0.737

CiteScore: 6.1

Impact factor: 3.6

ISSN: 00223263, 15206904

DOI: 10.1021/acs.joc.0c02599

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PubMed ID: 33225705

Organic Chemistry

Краткое описание

A solvent-free mechanochemical synthesis for 1,2,6-thiadiazine 1-oxides starting from NH-sulfonimidamides and propargyl ketones has been developed. Lewis acids affect these one-pot aza-Michael-addition/cyclization/dehydration reaction sequences. The photophysical properties of the resulting heterocyclic sulfonimidamide derivatives were characterized.

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Schöbel J. et al. Mechanochemical Synthesis of 1,2,6-Thiadiazine 1-Oxides from Sulfonimidamides and the Fluorescence Properties of the Products // Journal of Organic Chemistry. 2020. Vol. 85. No. 23. pp. 15760-15766.

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Schöbel J., Liang W., Wöll D., Bolm C. Mechanochemical Synthesis of 1,2,6-Thiadiazine 1-Oxides from Sulfonimidamides and the Fluorescence Properties of the Products // Journal of Organic Chemistry. 2020. Vol. 85. No. 23. pp. 15760-15766.

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TY - JOUR

DO - 10.1021/acs.joc.0c02599

UR - https://pubs.acs.org/doi/10.1021/acs.joc.0c02599

TI - Mechanochemical Synthesis of 1,2,6-Thiadiazine 1-Oxides from Sulfonimidamides and the Fluorescence Properties of the Products

T2 - Journal of Organic Chemistry

AU - Schöbel, Jan-Hendrik

AU - Liang, Wenjing

AU - Wöll, Dominik

AU - Bolm, Carsten

PY - 2020

DA - 2020/11/23

PB - American Chemical Society (ACS)

SP - 15760-15766

IS - 23

VL - 85

PMID - 33225705

SN - 0022-3263

SN - 1520-6904

ER -

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@article{2020_Schöbel,

author = {Jan-Hendrik Schöbel and Wenjing Liang and Dominik Wöll and Carsten Bolm},

title = {Mechanochemical Synthesis of 1,2,6-Thiadiazine 1-Oxides from Sulfonimidamides and the Fluorescence Properties of the Products},

journal = {Journal of Organic Chemistry},

year = {2020},

volume = {85},

publisher = {American Chemical Society (ACS)},

month = {nov},

url = {https://pubs.acs.org/doi/10.1021/acs.joc.0c02599},

number = {23},

pages = {15760--15766},

doi = {10.1021/acs.joc.0c02599}

}

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Schöbel, Jan-Hendrik, et al. “Mechanochemical Synthesis of 1,2,6-Thiadiazine 1-Oxides from Sulfonimidamides and the Fluorescence Properties of the Products.” Journal of Organic Chemistry, vol. 85, no. 23, Nov. 2020, pp. 15760-15766. https://pubs.acs.org/doi/10.1021/acs.joc.0c02599.