Metal-Free Annulation of 2-Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones
Тип публикации: Journal Article
Дата публикации: 2021-12-17
SCImago Q2
WOS Q1
БС1
SJR: 0.604
CiteScore: 5.8
Impact factor: 3.3
ISSN: 00223263, 15206904
PubMed ID:
34918926
Organic Chemistry
Краткое описание
A simple metal-free method for the synthesis of quinazolinones from commercially available 2-nitrobenzyl alcohols and tetrahydroisoquinolines is developed. The reaction conditions were tolerant of an array of functionalities such as halogen, tertiary amine, protected alcohol, and ester groups. Under nearly identical conditions, quinazolinethiones were obtained in the presence of elemental sulfur and suitable mediators.
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ГОСТ
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Ly D. et al. Metal-Free Annulation of 2-Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones // Journal of Organic Chemistry. 2021. Vol. 87. No. 1. pp. 103-113.
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Ly D., Nguyen T. T., Tran C. T. H., Nguyen V. P. T., Nguyen K. X., Pham P., Le N. T. H., Nguyen T. T., Phan N. T. S. Metal-Free Annulation of 2-Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones // Journal of Organic Chemistry. 2021. Vol. 87. No. 1. pp. 103-113.
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TY - JOUR
DO - 10.1021/acs.joc.1c02017
UR - https://doi.org/10.1021/acs.joc.1c02017
TI - Metal-Free Annulation of 2-Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones
T2 - Journal of Organic Chemistry
AU - Ly, Duc
AU - Nguyen, Thao T
AU - Tran, Cam T H
AU - Nguyen, Vy P T
AU - Nguyen, Khang X
AU - Pham, Phuc
AU - Le, Nhan T H
AU - Nguyen, Tung T.
AU - Phan, Nam T. S.
PY - 2021
DA - 2021/12/17
PB - American Chemical Society (ACS)
SP - 103-113
IS - 1
VL - 87
PMID - 34918926
SN - 0022-3263
SN - 1520-6904
ER -
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@article{2021_Ly,
author = {Duc Ly and Thao T Nguyen and Cam T H Tran and Vy P T Nguyen and Khang X Nguyen and Phuc Pham and Nhan T H Le and Tung T. Nguyen and Nam T. S. Phan},
title = {Metal-Free Annulation of 2-Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones},
journal = {Journal of Organic Chemistry},
year = {2021},
volume = {87},
publisher = {American Chemical Society (ACS)},
month = {dec},
url = {https://doi.org/10.1021/acs.joc.1c02017},
number = {1},
pages = {103--113},
doi = {10.1021/acs.joc.1c02017}
}
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MLA
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Ly, Duc, et al. “Metal-Free Annulation of 2-Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones.” Journal of Organic Chemistry, vol. 87, no. 1, Dec. 2021, pp. 103-113. https://doi.org/10.1021/acs.joc.1c02017.
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