volume 87 issue 1 pages 103-113

Metal-Free Annulation of 2-Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones

Publication typeJournal Article
Publication date2021-12-17
scimago Q2
wos Q1
SJR0.737
CiteScore6.1
Impact factor3.6
ISSN00223263, 15206904
Organic Chemistry
Abstract
A simple metal-free method for the synthesis of quinazolinones from commercially available 2-nitrobenzyl alcohols and tetrahydroisoquinolines is developed. The reaction conditions were tolerant of an array of functionalities such as halogen, tertiary amine, protected alcohol, and ester groups. Under nearly identical conditions, quinazolinethiones were obtained in the presence of elemental sulfur and suitable mediators.
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GOST Copy
Ly D. et al. Metal-Free Annulation of 2-Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones // Journal of Organic Chemistry. 2021. Vol. 87. No. 1. pp. 103-113.
GOST all authors (up to 50) Copy
Ly D., Nguyen T. T., Tran C. T. H., Nguyen V. P. T., Nguyen K. X., Pham P., Le N. T. H., Nguyen T. T., Phan N. T. S. Metal-Free Annulation of 2-Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones // Journal of Organic Chemistry. 2021. Vol. 87. No. 1. pp. 103-113.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1021/acs.joc.1c02017
UR - https://doi.org/10.1021/acs.joc.1c02017
TI - Metal-Free Annulation of 2-Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones
T2 - Journal of Organic Chemistry
AU - Ly, Duc
AU - Nguyen, Thao T
AU - Tran, Cam T H
AU - Nguyen, Vy P T
AU - Nguyen, Khang X
AU - Pham, Phuc
AU - Le, Nhan T H
AU - Nguyen, Tung T.
AU - Phan, Nam T. S.
PY - 2021
DA - 2021/12/17
PB - American Chemical Society (ACS)
SP - 103-113
IS - 1
VL - 87
PMID - 34918926
SN - 0022-3263
SN - 1520-6904
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2021_Ly,
author = {Duc Ly and Thao T Nguyen and Cam T H Tran and Vy P T Nguyen and Khang X Nguyen and Phuc Pham and Nhan T H Le and Tung T. Nguyen and Nam T. S. Phan},
title = {Metal-Free Annulation of 2-Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones},
journal = {Journal of Organic Chemistry},
year = {2021},
volume = {87},
publisher = {American Chemical Society (ACS)},
month = {dec},
url = {https://doi.org/10.1021/acs.joc.1c02017},
number = {1},
pages = {103--113},
doi = {10.1021/acs.joc.1c02017}
}
MLA
Cite this
MLA Copy
Ly, Duc, et al. “Metal-Free Annulation of 2-Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones.” Journal of Organic Chemistry, vol. 87, no. 1, Dec. 2021, pp. 103-113. https://doi.org/10.1021/acs.joc.1c02017.