Journal of Organic Chemistry, volume 84, issue 16, pages 9937-9945
Copper/B2pin2-Catalyzed Difluoroalkylation of Methylenecyclopropanes with Bromodifluorinated Acetates and Acetamides: One-Pot Synthesis of CF2-Containing Dihydronaphthalene Derivatives
1
School of Chemistry and Materials Science, Liaoning Shihua University, Fushun 113001, P. R. China
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Publication type: Journal Article
Publication date: 2019-07-26
Journal:
Journal of Organic Chemistry
Q2
Q1
SJR: 0.724
CiteScore: 6.2
Impact factor: 3.3
ISSN: 00223263, 15206904
Organic Chemistry
Abstract
Novel copper/B2pin2-catalyzed difluoroalkylation of methylenecyclopropanes with bromodifluorinated acetates and acetamides via a tandem radical process involving ring-opening/intramolecular cyclization has been reported. This protocol is not only tolerated to a diverse range of substrates but also applicable to the synthesis of useful difluoromethylated compounds. Moreover, the reaction could be performed on a gram scale with a high yield, which opens up the possibility for practical applications.
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Liu C. et al. Copper/B2pin2-Catalyzed Difluoroalkylation of Methylenecyclopropanes with Bromodifluorinated Acetates and Acetamides: One-Pot Synthesis of CF2-Containing Dihydronaphthalene Derivatives // Journal of Organic Chemistry. 2019. Vol. 84. No. 16. pp. 9937-9945.
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Liu C., Yang Y., Dong J., Zhou M., Li L., Wang H. Copper/B2pin2-Catalyzed Difluoroalkylation of Methylenecyclopropanes with Bromodifluorinated Acetates and Acetamides: One-Pot Synthesis of CF2-Containing Dihydronaphthalene Derivatives // Journal of Organic Chemistry. 2019. Vol. 84. No. 16. pp. 9937-9945.
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TY - JOUR
DO - 10.1021/acs.joc.9b01106
UR - https://doi.org/10.1021/acs.joc.9b01106
TI - Copper/B2pin2-Catalyzed Difluoroalkylation of Methylenecyclopropanes with Bromodifluorinated Acetates and Acetamides: One-Pot Synthesis of CF2-Containing Dihydronaphthalene Derivatives
T2 - Journal of Organic Chemistry
AU - Liu, Chuang
AU - Yang, Yan-Jie
AU - Dong, Jun-Ying
AU - Zhou, Mingdong
AU - Li, Lei
AU - Wang, He
PY - 2019
DA - 2019/07/26
PB - American Chemical Society (ACS)
SP - 9937-9945
IS - 16
VL - 84
SN - 0022-3263
SN - 1520-6904
ER -
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@article{2019_Liu,
author = {Chuang Liu and Yan-Jie Yang and Jun-Ying Dong and Mingdong Zhou and Lei Li and He Wang},
title = {Copper/B2pin2-Catalyzed Difluoroalkylation of Methylenecyclopropanes with Bromodifluorinated Acetates and Acetamides: One-Pot Synthesis of CF2-Containing Dihydronaphthalene Derivatives},
journal = {Journal of Organic Chemistry},
year = {2019},
volume = {84},
publisher = {American Chemical Society (ACS)},
month = {jul},
url = {https://doi.org/10.1021/acs.joc.9b01106},
number = {16},
pages = {9937--9945},
doi = {10.1021/acs.joc.9b01106}
}
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Liu, Chuang, et al. “Copper/B2pin2-Catalyzed Difluoroalkylation of Methylenecyclopropanes with Bromodifluorinated Acetates and Acetamides: One-Pot Synthesis of CF2-Containing Dihydronaphthalene Derivatives.” Journal of Organic Chemistry, vol. 84, no. 16, Jul. 2019, pp. 9937-9945. https://doi.org/10.1021/acs.joc.9b01106.