volume 123 issue 29 pages 18095-18102

Trapping of Gd(III) Ions by Keplerate Polyanionic Nanocapsules in Water: A 1H Fast Field Cycling NMR Relaxometry Study

Silvia Pizzanelli 1
Rustem Zairov 2, 3
Marco Carlo Mascherpa 1
Bulat Akhmadeev 3
Asiya Mustafina 2
Publication typeJournal Article
Publication date2019-07-02
scimago Q1
wos Q3
SJR0.914
CiteScore6.2
Impact factor3.2
ISSN19327447, 19327455
Surfaces, Coatings and Films
Electronic, Optical and Magnetic Materials
Physical and Theoretical Chemistry
General Energy
Abstract
Polyoxomolybdates of the type [{MoVIMoVI5O21(H2O)6}12{MoV2O4(L)}30](12+30n)–, also referred to as keplerates (Kps), are polyanionic nanocapsules bearing 20 {Mo9O9} pores connected to a central cavity by 20 channels. In solution, they can entrap cations in different sites of their porous structure (in the internal cavity, in the pores, or on the capsule surface) in equilibrium with cations free in solution. The porosity of Kps was previously exploited to prepare nanostructured potential contrast agents through the self-assembly of KpOAc or KpHPO4 (i.e., Kp with L = acetate or hydrogen phosphate) macroanions and Gd(III) cations in water, accompanied by stabilization with F-127 Pluronics. The strongly enhanced water proton relaxivity observed at 20 MHz was postulated to derive from the trapping of Gd(III) aqua ions by the nanocapsules. In the present work, 1H fast field cycling NMR relaxometry allowed this hypothesis to be verified on aqueous suspensions containing either KpOAc or KpHPO4 and Gd(III) in diffe...
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Pizzanelli S. et al. Trapping of Gd(III) Ions by Keplerate Polyanionic Nanocapsules in Water: A 1H Fast Field Cycling NMR Relaxometry Study // Journal of Physical Chemistry C. 2019. Vol. 123. No. 29. pp. 18095-18102.
GOST all authors (up to 50) Copy
Pizzanelli S., Zairov R., Sokolov M., Mascherpa M. C., Akhmadeev B. S., Akhmadeev B., Mustafina A. R., Mustafina A., Calucci L. Trapping of Gd(III) Ions by Keplerate Polyanionic Nanocapsules in Water: A 1H Fast Field Cycling NMR Relaxometry Study // Journal of Physical Chemistry C. 2019. Vol. 123. No. 29. pp. 18095-18102.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1021/acs.jpcc.9b05044
UR - https://pubs.acs.org/doi/10.1021/acs.jpcc.9b05044
TI - Trapping of Gd(III) Ions by Keplerate Polyanionic Nanocapsules in Water: A 1H Fast Field Cycling NMR Relaxometry Study
T2 - Journal of Physical Chemistry C
AU - Pizzanelli, Silvia
AU - Zairov, Rustem
AU - Sokolov, Maxim
AU - Mascherpa, Marco Carlo
AU - Akhmadeev, Bulat S.
AU - Akhmadeev, Bulat
AU - Mustafina, Asiya R.
AU - Mustafina, Asiya
AU - Calucci, Lucia
PY - 2019
DA - 2019/07/02
PB - American Chemical Society (ACS)
SP - 18095-18102
IS - 29
VL - 123
SN - 1932-7447
SN - 1932-7455
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2019_Pizzanelli,
author = {Silvia Pizzanelli and Rustem Zairov and Maxim Sokolov and Marco Carlo Mascherpa and Bulat S. Akhmadeev and Bulat Akhmadeev and Asiya R. Mustafina and Asiya Mustafina and Lucia Calucci},
title = {Trapping of Gd(III) Ions by Keplerate Polyanionic Nanocapsules in Water: A 1H Fast Field Cycling NMR Relaxometry Study},
journal = {Journal of Physical Chemistry C},
year = {2019},
volume = {123},
publisher = {American Chemical Society (ACS)},
month = {jul},
url = {https://pubs.acs.org/doi/10.1021/acs.jpcc.9b05044},
number = {29},
pages = {18095--18102},
doi = {10.1021/acs.jpcc.9b05044}
}
MLA
Cite this
MLA Copy
Pizzanelli, Silvia, et al. “Trapping of Gd(III) Ions by Keplerate Polyanionic Nanocapsules in Water: A 1H Fast Field Cycling NMR Relaxometry Study.” Journal of Physical Chemistry C, vol. 123, no. 29, Jul. 2019, pp. 18095-18102. https://pubs.acs.org/doi/10.1021/acs.jpcc.9b05044.