Nano Letters, volume 18, issue 10, pages 6113-6120

PVDF/Palygorskite Nanowire Composite Electrolyte for 4 V Rechargeable Lithium Batteries with High Energy Density

Jia Zhu ¹

Bin Zhu ^{1, 2}

H Zhai ¹

Xiangbiao Liao ³

Yuxiang Zhu ¹

Wei-Heng Xu ¹

Qian Cheng ¹

Charles Jayyosi ⁴

Zheng Li ⁵

Jia Zhu ²

Kristin Myers ⁴

Xi Chen ³

Yuan Yang ¹

Hide authors affiliations Show authors affiliations: 5 affiliations

Program of Materials Science and Engineering, Department of Applied Physics and Applied Mathematics, Columbia University, New York, New York 10027, United States |

College of Engineering and Applied Science, Nanjing University, Nanjing, 210093, People’s Republic of China |

Department of Earth and Environmental Engineering, Columbia University, New York, New York 10027, United States |

⁴

Department of Mechanical Engineering, Columbia University, New York, New York 10027, United States |

⁵

Jiangsu Qingtao Energy S&T Co., Ltd, Huai-an, 211700, People’s Republic of China |

Publication type: Journal Article

Publication date: 2018-08-31

American Chemical Society (ACS)

Journal: Nano Letters

Quartile SCImago

Quartile WOS

Impact factor: 10.8

ISSN: 15306984, 15306992

DOI: 10.1021/acs.nanolett.8b01421

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General Chemistry

Condensed Matter Physics

General Materials Science

Mechanical Engineering

Bioengineering

Abstract

Solid electrolytes are crucial for the development of solid state batteries. Among different types of solid electrolytes, poly(ethylene oxide) (PEO)-based polymer electrolytes have attracted extensive attention owing to their excellent flexibility and easiness for processing. However, their relatively low ionic conductivities and electrochemical instability above 4 V limit their applications in batteries with high energy density. Herein, we prepared poly(vinylidene fluoride) (PVDF) polymer electrolytes with an organic plasticizer, which possesses compatibility with 4 V cathode and high ionic conductivity (1.2 × 10-4 S/cm) at room temperature. We also revealed the importance of plasticizer content to the ionic conductivity. To address weak mechanical strength of the PVDF electrolyte with plasticizer, we introduced palygorskite ((Mg,Al)2Si4O10(OH)) nanowires as a new ceramic filler to form composite solid electrolytes (CPE), which greatly enhances both stiffness and toughness of PVDF-based polymer electrolyte. With 5 wt % of palygorskite nanowires, not only does the elastic modulus of PVDF CPE increase from 9.0 to 96 MPa but also its yield stress is enhanced by 200%. Moreover, numerical modeling uncovers that the strong nanowire-polymer interaction and cross-linking network of nanowires are responsible for such significant enhancement in mechanically robustness. The addition of 5% palygorskite nanowires also enhances transference number of Li+ from 0.21 to 0.54 due to interaction between palygorskite and ClO4- ions. We further demonstrate full cells based on Li(Ni1/3Mn1/3Co1/3)O2 (NMC111) cathode, PVDF/palygorskite CPE, and lithium anode, which can be cycled over 200 times at 0.3 C, with 97% capacity retention. Moreover, the PVDF matrix is much less flammable than PEO electrolytes. Our work illustrates that the PVDF/palygorskite CPE is a promising electrolyte for solid state batteries.

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Citations by journals

	2 4 6 8 10 12 14
Energy Storage Materials	Energy Storage Materials, 13, 5.46% Energy Storage Materials 13 publications, 5.46%
Journal of Materials Chemistry A	Journal of Materials Chemistry A, 13, 5.46% Journal of Materials Chemistry A 13 publications, 5.46%
Advanced Functional Materials	Advanced Functional Materials, 12, 5.04% Advanced Functional Materials 12 publications, 5.04%
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ACS applied materials & interfaces	ACS applied materials & interfaces, 10, 4.2% ACS applied materials & interfaces 10 publications, 4.2%
Advanced Energy Materials	Advanced Energy Materials, 8, 3.36% Advanced Energy Materials 8 publications, 3.36%
Advanced Materials	Advanced Materials, 7, 2.94% Advanced Materials 7 publications, 2.94%
Journal of Energy Chemistry	Journal of Energy Chemistry, 6, 2.52% Journal of Energy Chemistry 6 publications, 2.52%
Chemical Engineering Journal	Chemical Engineering Journal, 6, 2.52% Chemical Engineering Journal 6 publications, 2.52%
Energy & Fuels	Energy & Fuels, 6, 2.52% Energy & Fuels 6 publications, 2.52%
Small	Small, 5, 2.1% Small 5 publications, 2.1%
Journal of Colloid and Interface Science	Journal of Colloid and Interface Science, 5, 2.1% Journal of Colloid and Interface Science 5 publications, 2.1%
ACS Applied Energy Materials	ACS Applied Energy Materials, 5, 2.1% ACS Applied Energy Materials 5 publications, 2.1%
Nano Energy	Nano Energy, 4, 1.68% Nano Energy 4 publications, 1.68%
Journal of Membrane Science	Journal of Membrane Science, 3, 1.26% Journal of Membrane Science 3 publications, 1.26%
Ceramics International	Ceramics International, 3, 1.26% Ceramics International 3 publications, 1.26%
Solid State Ionics	Solid State Ionics, 3, 1.26% Solid State Ionics 3 publications, 1.26%
Angewandte Chemie - International Edition	Angewandte Chemie - International Edition, 3, 1.26% Angewandte Chemie - International Edition 3 publications, 1.26%
Angewandte Chemie	Angewandte Chemie, 3, 1.26% Angewandte Chemie 3 publications, 1.26%
ACS Energy Letters	ACS Energy Letters, 3, 1.26% ACS Energy Letters 3 publications, 1.26%
ACS Applied Nano Materials	ACS Applied Nano Materials, 3, 1.26% ACS Applied Nano Materials 3 publications, 1.26%
Materials Chemistry Frontiers	Materials Chemistry Frontiers, 3, 1.26% Materials Chemistry Frontiers 3 publications, 1.26%
InfoMat	InfoMat, 2, 0.84% InfoMat 2 publications, 0.84%
Materials	Materials, 2, 0.84% Materials 2 publications, 0.84%
Nature Reviews Materials	Nature Reviews Materials, 2, 0.84% Nature Reviews Materials 2 publications, 0.84%
Science China Materials	Science China Materials, 2, 0.84% Science China Materials 2 publications, 0.84%
Nano Research	Nano Research, 2, 0.84% Nano Research 2 publications, 0.84%
Nano-Micro Letters	Nano-Micro Letters, 2, 0.84% Nano-Micro Letters 2 publications, 0.84%
Journal of Electroanalytical Chemistry	Journal of Electroanalytical Chemistry, 2, 0.84% Journal of Electroanalytical Chemistry 2 publications, 0.84%
	2 4 6 8 10 12 14

Citations by publishers

	10 20 30 40 50 60 70 80 90
Elsevier	Elsevier, 82, 34.45% Elsevier 82 publications, 34.45%
Wiley	Wiley, 59, 24.79% Wiley 59 publications, 24.79%
American Chemical Society (ACS)	American Chemical Society (ACS), 38, 15.97% American Chemical Society (ACS) 38 publications, 15.97%
Royal Society of Chemistry (RSC)	Royal Society of Chemistry (RSC), 23, 9.66% Royal Society of Chemistry (RSC) 23 publications, 9.66%
Springer Nature	Springer Nature, 18, 7.56% Springer Nature 18 publications, 7.56%
Multidisciplinary Digital Publishing Institute (MDPI)	Multidisciplinary Digital Publishing Institute (MDPI), 4, 1.68% Multidisciplinary Digital Publishing Institute (MDPI) 4 publications, 1.68%
IOP Publishing	IOP Publishing, 2, 0.84% IOP Publishing 2 publications, 0.84%
Emerald	Emerald, 1, 0.42% Emerald 1 publication, 0.42%
The Electrochemical Society	The Electrochemical Society, 1, 0.42% The Electrochemical Society 1 publication, 0.42%
Chemical Industry Press	Chemical Industry Press, 1, 0.42% Chemical Industry Press 1 publication, 0.42%
Electrochemical Science Group, University of Belgrade	Electrochemical Science Group, University of Belgrade, 1, 0.42% Electrochemical Science Group, University of Belgrade 1 publication, 0.42%
Chinese Physical Society	Chinese Physical Society, 1, 0.42% Chinese Physical Society 1 publication, 0.42%
Shanghai Institute of Ceramics	Shanghai Institute of Ceramics, 1, 0.42% Shanghai Institute of Ceramics 1 publication, 0.42%
Proceedings of the National Academy of Sciences (PNAS)	Proceedings of the National Academy of Sciences (PNAS), 1, 0.42% Proceedings of the National Academy of Sciences (PNAS) 1 publication, 0.42%
ITMO University	ITMO University, 1, 0.42% ITMO University 1 publication, 0.42%
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii	Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii, 1, 0.42% Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii 1 publication, 0.42%
	10 20 30 40 50 60 70 80 90

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Zhu J. et al. PVDF/Palygorskite Nanowire Composite Electrolyte for 4 V Rechargeable Lithium Batteries with High Energy Density // Nano Letters. 2018. Vol. 18. No. 10. pp. 6113-6120.

GOST all authors (up to 50) Copy

Zhu J., Zhu B., Zhai H., Liao X., Zhu Y., Xu W., Cheng Q., Jayyosi C., Li Z., Zhu J., Myers K., Chen X., Yang Y. PVDF/Palygorskite Nanowire Composite Electrolyte for 4 V Rechargeable Lithium Batteries with High Energy Density // Nano Letters. 2018. Vol. 18. No. 10. pp. 6113-6120.

RIS |

Cite this

RIS Copy

TY - JOUR

DO - 10.1021/acs.nanolett.8b01421

UR - https://doi.org/10.1021/acs.nanolett.8b01421

TI - PVDF/Palygorskite Nanowire Composite Electrolyte for 4 V Rechargeable Lithium Batteries with High Energy Density

T2 - Nano Letters

AU - Jayyosi, Charles

AU - Zhu, Jia

AU - Zhai, H

AU - Liao, Xiangbiao

AU - Cheng, Qian

AU - Zhu, Jia

AU - Yang, Yuan

AU - Zhu, Bin

AU - Zhu, Yuxiang

AU - Xu, Wei-Heng

AU - Li, Zheng

AU - Myers, Kristin

AU - Chen, Xi

PY - 2018

DA - 2018/08/31 00:00:00

PB - American Chemical Society (ACS)

SP - 6113-6120

IS - 10

VL - 18

SN - 1530-6984

SN - 1530-6992

ER -

BibTex |

Cite this

BibTex Copy

@article{2018_Zhu,

author = {Charles Jayyosi and Jia Zhu and H Zhai and Xiangbiao Liao and Qian Cheng and Jia Zhu and Yuan Yang and Bin Zhu and Yuxiang Zhu and Wei-Heng Xu and Zheng Li and Kristin Myers and Xi Chen},

title = {PVDF/Palygorskite Nanowire Composite Electrolyte for 4 V Rechargeable Lithium Batteries with High Energy Density},

journal = {Nano Letters},

year = {2018},

volume = {18},

publisher = {American Chemical Society (ACS)},

month = {aug},

url = {https://doi.org/10.1021/acs.nanolett.8b01421},

number = {10},

pages = {6113--6120},

doi = {10.1021/acs.nanolett.8b01421}

}

MLA

Cite this

MLA Copy

Zhu, Jia, et al. “PVDF/Palygorskite Nanowire Composite Electrolyte for 4 V Rechargeable Lithium Batteries with High Energy Density.” Nano Letters, vol. 18, no. 10, Aug. 2018, pp. 6113-6120. https://doi.org/10.1021/acs.nanolett.8b01421.

Found error?

Publisher

American Chemical Society (ACS)

Journal

Nano Letters

Quartile SCImago

Quartile WOS

Impact factor

10.8

ISSN

15306984 (Print)
15306992 (Electronic)