volume 27 issue 2 pages 269-275

Safety Considerations and Proposed Workflow for Laboratory-Scale Chemical Synthesis by Ball Milling

Ian Priestley 1
Claudio Battilocchio 2
Andrei V Iosub 2
Fabien Barreteau 2
Gavin W. Bluck 2
Kenneth B. Ling 3
Katharine Ingram 3
Maria Ciaccia 3
Jamie A. Leitch 4
Duncan L. Browne 4
1
 
Huddersfield Manufacturing Centre, Syngenta Ltd, Huddersfield HD2 1FF, United Kingdom
2
 
Syngenta Crop Protection AG, Schaffauserstrasse, 4332 Stein, Switzerland
3
 
Jealott’s Hill International Research Centre, Syngenta Ltd., Bracknell, Berkshire RG42 6EY, United Kingdom
Publication typeJournal Article
Publication date2023-02-03
scimago Q1
wos Q1
SJR0.865
CiteScore5.4
Impact factor3.5
ISSN10836160, 1520586X
Organic Chemistry
Physical and Theoretical Chemistry
Abstract
Chemical reactions that take place in a ball mill and in the absence of a bulk reaction solvent present different safety profiles to stirred solution reactions. Herein, we present and describe steps that a researcher may take to better ensure that they have considered some of the hazards and measures that emerge and minimize the risk to themselves and their colleagues.
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GOST |
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GOST Copy
Priestley I. et al. Safety Considerations and Proposed Workflow for Laboratory-Scale Chemical Synthesis by Ball Milling // Organic Process Research and Development. 2023. Vol. 27. No. 2. pp. 269-275.
GOST all authors (up to 50) Copy
Priestley I., Battilocchio C., Iosub A. V., Barreteau F., Bluck G. W., Ling K. B., Ingram K., Ciaccia M., Leitch J. A., Browne D. L. Safety Considerations and Proposed Workflow for Laboratory-Scale Chemical Synthesis by Ball Milling // Organic Process Research and Development. 2023. Vol. 27. No. 2. pp. 269-275.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1021/acs.oprd.2c00226
UR - https://pubs.acs.org/doi/10.1021/acs.oprd.2c00226
TI - Safety Considerations and Proposed Workflow for Laboratory-Scale Chemical Synthesis by Ball Milling
T2 - Organic Process Research and Development
AU - Priestley, Ian
AU - Battilocchio, Claudio
AU - Iosub, Andrei V
AU - Barreteau, Fabien
AU - Bluck, Gavin W.
AU - Ling, Kenneth B.
AU - Ingram, Katharine
AU - Ciaccia, Maria
AU - Leitch, Jamie A.
AU - Browne, Duncan L.
PY - 2023
DA - 2023/02/03
PB - American Chemical Society (ACS)
SP - 269-275
IS - 2
VL - 27
SN - 1083-6160
SN - 1520-586X
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2023_Priestley,
author = {Ian Priestley and Claudio Battilocchio and Andrei V Iosub and Fabien Barreteau and Gavin W. Bluck and Kenneth B. Ling and Katharine Ingram and Maria Ciaccia and Jamie A. Leitch and Duncan L. Browne},
title = {Safety Considerations and Proposed Workflow for Laboratory-Scale Chemical Synthesis by Ball Milling},
journal = {Organic Process Research and Development},
year = {2023},
volume = {27},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://pubs.acs.org/doi/10.1021/acs.oprd.2c00226},
number = {2},
pages = {269--275},
doi = {10.1021/acs.oprd.2c00226}
}
MLA
Cite this
MLA Copy
Priestley, Ian, et al. “Safety Considerations and Proposed Workflow for Laboratory-Scale Chemical Synthesis by Ball Milling.” Organic Process Research and Development, vol. 27, no. 2, Feb. 2023, pp. 269-275. https://pubs.acs.org/doi/10.1021/acs.oprd.2c00226.