Syntheses and Structures of a Series of Acyclic Diaminocarbene Palladium(II) Complexes Derived from 3,4-Diaryl-1H-pyrrol-2,5-diimines and Bisisocyanide Palladium(II) Complexes
Dina V Boyarskaya
1
,
Evgeny Bulatov
2
,
Irina A Boyarskaya
1
,
Tatiana Chulkova
1
,
Valentin A Rassadin
1
,
Publication type: Journal Article
Publication date: 2018-12-26
scimago Q2
wos Q1
SJR: 0.676
CiteScore: 5.1
Impact factor: 2.9
ISSN: 02767333, 15206041
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Reactions of 3,4-diaryl-1H-pyrrol-2,5-diimines with various bisisocyanide palladium(II) complexes were studied. The coupling proceeds with one isocyanide ligand to accomplish the acyclic diaminocarbene complexes. The structure of generated diaminocarbene complexes depends on bulkiness of isocyanide ligand in the bisisocyanide complexes of palladium(II). The imino-group of 3,4-diaryl-1H-pyrrol-2,5-diimine reacts with one isocyanide ligand of cis-[PdCl2(CN–R)2] (R = i-Pr, Cy, t-Bu, Bn), and the nitrogen atom of the pyrrole ring is coordinated to the palladium center as the second isocyanide ligand remains intact. In the case of cis-[PdCl2(CN–R)2] (R = 2-acyloxyphenyl, 2-sulfonyloxyphenyl), one isocyanide ligand is displaced from the coordination sphere. Structural features of the prepared diaminocarbene complexes have been studied by molecular spectroscopy techniques, cyclic voltammetry, single-crystal X-ray diffraction, and DFT calculations. The photophysical properties of the obtained acyclic diaminocarbe...
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Boyarskaya D. V. et al. Syntheses and Structures of a Series of Acyclic Diaminocarbene Palladium(II) Complexes Derived from 3,4-Diaryl-1H-pyrrol-2,5-diimines and Bisisocyanide Palladium(II) Complexes // Organometallics. 2018. Vol. 38. No. 2. pp. 300-309.
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Boyarskaya D. V., Bulatov E., Boyarskaya I. A., Chulkova T., Rassadin V. A., Tolstopjatova E. G., Kolesnikov I. E., Avdontceva M. S., Panikorovskii T. L., Suslonov V. V., Haukka M. Syntheses and Structures of a Series of Acyclic Diaminocarbene Palladium(II) Complexes Derived from 3,4-Diaryl-1H-pyrrol-2,5-diimines and Bisisocyanide Palladium(II) Complexes // Organometallics. 2018. Vol. 38. No. 2. pp. 300-309.
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TY - JOUR
DO - 10.1021/acs.organomet.8b00725
UR - https://doi.org/10.1021/acs.organomet.8b00725
TI - Syntheses and Structures of a Series of Acyclic Diaminocarbene Palladium(II) Complexes Derived from 3,4-Diaryl-1H-pyrrol-2,5-diimines and Bisisocyanide Palladium(II) Complexes
T2 - Organometallics
AU - Boyarskaya, Dina V
AU - Bulatov, Evgeny
AU - Boyarskaya, Irina A
AU - Chulkova, Tatiana
AU - Rassadin, Valentin A
AU - Tolstopjatova, Elena G
AU - Kolesnikov, Ilya E.
AU - Avdontceva, Margarita S.
AU - Panikorovskii, T. L.
AU - Suslonov, Vitalii V
AU - Haukka, Matti
PY - 2018
DA - 2018/12/26
PB - American Chemical Society (ACS)
SP - 300-309
IS - 2
VL - 38
SN - 0276-7333
SN - 1520-6041
ER -
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@article{2018_Boyarskaya,
author = {Dina V Boyarskaya and Evgeny Bulatov and Irina A Boyarskaya and Tatiana Chulkova and Valentin A Rassadin and Elena G Tolstopjatova and Ilya E. Kolesnikov and Margarita S. Avdontceva and T. L. Panikorovskii and Vitalii V Suslonov and Matti Haukka},
title = {Syntheses and Structures of a Series of Acyclic Diaminocarbene Palladium(II) Complexes Derived from 3,4-Diaryl-1H-pyrrol-2,5-diimines and Bisisocyanide Palladium(II) Complexes},
journal = {Organometallics},
year = {2018},
volume = {38},
publisher = {American Chemical Society (ACS)},
month = {dec},
url = {https://doi.org/10.1021/acs.organomet.8b00725},
number = {2},
pages = {300--309},
doi = {10.1021/acs.organomet.8b00725}
}
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Boyarskaya, Dina V., et al. “Syntheses and Structures of a Series of Acyclic Diaminocarbene Palladium(II) Complexes Derived from 3,4-Diaryl-1H-pyrrol-2,5-diimines and Bisisocyanide Palladium(II) Complexes.” Organometallics, vol. 38, no. 2, Dec. 2018, pp. 300-309. https://doi.org/10.1021/acs.organomet.8b00725.