Ruthenium-Catalyzed Silylation of 1,3-Butadienes with Vinylsilanes
Justyna Szudkowska Frątczak
1
,
Bogdan Marciniec
1, 2
,
Grzegorz Hreczycho
1
,
M. Kubicki
1
,
Piotr Pawluć
1
Publication type: Journal Article
Publication date: 2015-04-27
scimago Q1
wos Q1
SJR: 1.235
CiteScore: 8.7
Impact factor: 5.0
ISSN: 15237060, 15237052
PubMed ID:
25914959
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
A novel method for the synthesis of 1-silyl-substituted 1,3-butadienes, based on [RuHCl(CO)(PCy3)2]-catalyzed silylative coupling of terminal (E)-1,3-dienes with vinylsilanes, is reported. The reaction provides a facile and straightforward access to (E,E)-dienylsilanes in a highly stereoselective fashion (especially for aryl-substituted dienes) and opens a valuable and general synthetic route for the direct catalytic silylation of conjugated dienes with elimination of ethylene as a single byproduct. Preliminary results on synthetic application of the synthesized silylated 1,3-butadienes in desilylation reactions are described.
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GOST
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Szudkowska Frątczak J. et al. Ruthenium-Catalyzed Silylation of 1,3-Butadienes with Vinylsilanes // Organic Letters. 2015. Vol. 17. No. 10. pp. 2366-2369.
GOST all authors (up to 50)
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Szudkowska Frątczak J., Marciniec B., Hreczycho G., Kubicki M., Pawluć P. Ruthenium-Catalyzed Silylation of 1,3-Butadienes with Vinylsilanes // Organic Letters. 2015. Vol. 17. No. 10. pp. 2366-2369.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1021/acs.orglett.5b00865
UR - https://doi.org/10.1021/acs.orglett.5b00865
TI - Ruthenium-Catalyzed Silylation of 1,3-Butadienes with Vinylsilanes
T2 - Organic Letters
AU - Szudkowska Frątczak, Justyna
AU - Marciniec, Bogdan
AU - Hreczycho, Grzegorz
AU - Kubicki, M.
AU - Pawluć, Piotr
PY - 2015
DA - 2015/04/27
PB - American Chemical Society (ACS)
SP - 2366-2369
IS - 10
VL - 17
PMID - 25914959
SN - 1523-7060
SN - 1523-7052
ER -
Cite this
BibTex (up to 50 authors)
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@article{2015_Szudkowska Frątczak,
author = {Justyna Szudkowska Frątczak and Bogdan Marciniec and Grzegorz Hreczycho and M. Kubicki and Piotr Pawluć},
title = {Ruthenium-Catalyzed Silylation of 1,3-Butadienes with Vinylsilanes},
journal = {Organic Letters},
year = {2015},
volume = {17},
publisher = {American Chemical Society (ACS)},
month = {apr},
url = {https://doi.org/10.1021/acs.orglett.5b00865},
number = {10},
pages = {2366--2369},
doi = {10.1021/acs.orglett.5b00865}
}
Cite this
MLA
Copy
Szudkowska Frątczak, Justyna, et al. “Ruthenium-Catalyzed Silylation of 1,3-Butadienes with Vinylsilanes.” Organic Letters, vol. 17, no. 10, Apr. 2015, pp. 2366-2369. https://doi.org/10.1021/acs.orglett.5b00865.