ACS applied materials & interfaces, volume 11, issue 6, pages 6015-6021

Rapid and Economic Synthesis of a Li₇PS₆ Solid Electrolyte from a Liquid Approach

Dominika A Ziolkowska ¹

William Arnold

Thad Druffel

Mahendra Sunkara

Hui Wang

Hide authors affiliations Show authors affiliations: 1 affiliation

Faculty of Chemistry, University of Warsaw, 02-093 Warsaw, Poland |

Publication type: Journal Article

Publication date: 2019-01-17

American Chemical Society (ACS)

Journal: ACS applied materials & interfaces

Quartile SCImago

Quartile WOS

Impact factor: 9.5

ISSN: 19448244, 19448252

DOI: 10.1021/acsami.8b19181

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General Materials Science

Abstract

Solid electrolytes are the key to realize future solid-state batteries that show the advantages of high energy density and intrinsic safety. However, most solid electrolytes require long time and energy-consuming synthesis conditions of either extended ball milling or high-temperature solid-state reactions, impeding practical applications of solid electrolytes for large-scale systems. Here, we report a new and rapid liquid-based synthetic method for preparing a high-purity Li7PS6 solid electrolyte through the stoichemical reaction of Li3PS4 and Li2S. This method relies on facile and low-cost solution-based soft chemistry to complete chemical reaction in extensively short time (2 h). The prepared Li7PS6 solid electrolyte shows a high phase purity, an impressive ionic conductivity (0.11 mS cm-1), and a reasonable electrochemical stability with a metallic lithium anode. Our results highlight the use of an economic and nontoxic solvent to quickly synthesize a Li7PS6 solid electrolyte, which would promote the development of solid-state batteries for next-generation energy storage systems.

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Citations by journals

	1 2 3 4 5 6 7
ACS applied materials & interfaces	ACS applied materials & interfaces, 7, 9.09% ACS applied materials & interfaces 7 publications, 9.09%
Journal of Power Sources	Journal of Power Sources, 4, 5.19% Journal of Power Sources 4 publications, 5.19%
Journal of Alloys and Compounds	Journal of Alloys and Compounds, 4, 5.19% Journal of Alloys and Compounds 4 publications, 5.19%
Energy Storage Materials	Energy Storage Materials, 4, 5.19% Energy Storage Materials 4 publications, 5.19%
Journal of Materials Chemistry A	Journal of Materials Chemistry A, 4, 5.19% Journal of Materials Chemistry A 4 publications, 5.19%
ACS Applied Energy Materials	ACS Applied Energy Materials, 3, 3.9% ACS Applied Energy Materials 3 publications, 3.9%
ACS Sustainable Chemistry and Engineering	ACS Sustainable Chemistry and Engineering, 2, 2.6% ACS Sustainable Chemistry and Engineering 2 publications, 2.6%
Chemical Engineering Journal	Chemical Engineering Journal, 2, 2.6% Chemical Engineering Journal 2 publications, 2.6%
Electrochimica Acta	Electrochimica Acta, 2, 2.6% Electrochimica Acta 2 publications, 2.6%
ChemSusChem	ChemSusChem, 2, 2.6% ChemSusChem 2 publications, 2.6%
Energy Technology	Energy Technology, 2, 2.6% Energy Technology 2 publications, 2.6%
Batteries & Supercaps	Batteries & Supercaps, 2, 2.6% Batteries & Supercaps 2 publications, 2.6%
Chemistry of Materials	Chemistry of Materials, 2, 2.6% Chemistry of Materials 2 publications, 2.6%
Zeitschrift fur Physikalische Chemie	Zeitschrift fur Physikalische Chemie, 2, 2.6% Zeitschrift fur Physikalische Chemie 2 publications, 2.6%
Journal of Energy Storage	Journal of Energy Storage, 1, 1.3% Journal of Energy Storage 1 publication, 1.3%
Functional Materials Letters	Functional Materials Letters, 1, 1.3% Functional Materials Letters 1 publication, 1.3%
Chemical Research in Chinese Universities	Chemical Research in Chinese Universities, 1, 1.3% Chemical Research in Chinese Universities 1 publication, 1.3%
Electrochemical Energy Reviews	Electrochemical Energy Reviews, 1, 1.3% Electrochemical Energy Reviews 1 publication, 1.3%
Sustainable Materials and Technologies	Sustainable Materials and Technologies, 1, 1.3% Sustainable Materials and Technologies 1 publication, 1.3%
Materials Today Energy	Materials Today Energy, 1, 1.3% Materials Today Energy 1 publication, 1.3%
Solid State Ionics	Solid State Ionics, 1, 1.3% Solid State Ionics 1 publication, 1.3%
Materials Today Nano	Materials Today Nano, 1, 1.3% Materials Today Nano 1 publication, 1.3%
SSRN Electronic Journal	SSRN Electronic Journal, 1, 1.3% SSRN Electronic Journal 1 publication, 1.3%
Nano Energy	Nano Energy, 1, 1.3% Nano Energy 1 publication, 1.3%
Scripta Materialia	Scripta Materialia, 1, 1.3% Scripta Materialia 1 publication, 1.3%
Advanced Energy and Sustainability Research	Advanced Energy and Sustainability Research, 1, 1.3% Advanced Energy and Sustainability Research 1 publication, 1.3%
International Journal of Energy Research	International Journal of Energy Research, 1, 1.3% International Journal of Energy Research 1 publication, 1.3%
Inorganic Chemistry	Inorganic Chemistry, 1, 1.3% Inorganic Chemistry 1 publication, 1.3%
Journal of Physical Chemistry Letters	Journal of Physical Chemistry Letters, 1, 1.3% Journal of Physical Chemistry Letters 1 publication, 1.3%
	1 2 3 4 5 6 7

Citations by publishers

	5 10 15 20 25
Elsevier	Elsevier, 24, 31.17% Elsevier 24 publications, 31.17%
American Chemical Society (ACS)	American Chemical Society (ACS), 21, 27.27% American Chemical Society (ACS) 21 publications, 27.27%
Wiley	Wiley, 10, 12.99% Wiley 10 publications, 12.99%
Royal Society of Chemistry (RSC)	Royal Society of Chemistry (RSC), 8, 10.39% Royal Society of Chemistry (RSC) 8 publications, 10.39%
Springer Nature	Springer Nature, 3, 3.9% Springer Nature 3 publications, 3.9%
Walter de Gruyter	Walter de Gruyter, 2, 2.6% Walter de Gruyter 2 publications, 2.6%
World Scientific	World Scientific, 1, 1.3% World Scientific 1 publication, 1.3%
Social Science Electronic Publishing	Social Science Electronic Publishing, 1, 1.3% Social Science Electronic Publishing 1 publication, 1.3%
Multidisciplinary Digital Publishing Institute (MDPI)	Multidisciplinary Digital Publishing Institute (MDPI), 1, 1.3% Multidisciplinary Digital Publishing Institute (MDPI) 1 publication, 1.3%
Proceedings of the National Academy of Sciences (PNAS)	Proceedings of the National Academy of Sciences (PNAS), 1, 1.3% Proceedings of the National Academy of Sciences (PNAS) 1 publication, 1.3%
American Association for the Advancement of Science (AAAS)	American Association for the Advancement of Science (AAAS), 1, 1.3% American Association for the Advancement of Science (AAAS) 1 publication, 1.3%
Taylor & Francis	Taylor & Francis, 1, 1.3% Taylor & Francis 1 publication, 1.3%
The Electrochemical Society	The Electrochemical Society, 1, 1.3% The Electrochemical Society 1 publication, 1.3%
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii	Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii, 1, 1.3% Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii 1 publication, 1.3%
	5 10 15 20 25

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Ziolkowska D. A. et al. Rapid and Economic Synthesis of a Li7PS6 Solid Electrolyte from a Liquid Approach // ACS applied materials & interfaces. 2019. Vol. 11. No. 6. pp. 6015-6021.

GOST all authors (up to 50) Copy

Ziolkowska D. A., Arnold W., Druffel T., Sunkara M., Wang H. Rapid and Economic Synthesis of a Li7PS6 Solid Electrolyte from a Liquid Approach // ACS applied materials & interfaces. 2019. Vol. 11. No. 6. pp. 6015-6021.

RIS |

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RIS Copy

TY - JOUR

DO - 10.1021/acsami.8b19181

UR - https://doi.org/10.1021/acsami.8b19181

TI - Rapid and Economic Synthesis of a Li7PS6 Solid Electrolyte from a Liquid Approach

T2 - ACS applied materials & interfaces

AU - Druffel, Thad

AU - Sunkara, Mahendra

AU - Wang, Hui

AU - Ziolkowska, Dominika A

AU - Arnold, William

PY - 2019

DA - 2019/01/17 00:00:00

PB - American Chemical Society (ACS)

SP - 6015-6021

IS - 6

VL - 11

SN - 1944-8244

SN - 1944-8252

ER -

BibTex |

Cite this

BibTex Copy

@article{2019_Ziolkowska,

author = {Thad Druffel and Mahendra Sunkara and Hui Wang and Dominika A Ziolkowska and William Arnold},

title = {Rapid and Economic Synthesis of a Li7PS6 Solid Electrolyte from a Liquid Approach},

journal = {ACS applied materials & interfaces},

year = {2019},

volume = {11},

publisher = {American Chemical Society (ACS)},

month = {jan},

url = {https://doi.org/10.1021/acsami.8b19181},

number = {6},

pages = {6015--6021},

doi = {10.1021/acsami.8b19181}

}

MLA

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MLA Copy

Ziolkowska, Dominika A., et al. “Rapid and Economic Synthesis of a Li7PS6 Solid Electrolyte from a Liquid Approach.” ACS applied materials & interfaces, vol. 11, no. 6, Jan. 2019, pp. 6015-6021. https://doi.org/10.1021/acsami.8b19181.

Found error?

Publisher

American Chemical Society (ACS)

Journal

ACS applied materials & interfaces

Quartile SCImago

Quartile WOS

Impact factor

9.5

ISSN

19448244 (Print)
19448252 (Electronic)