ACS applied materials & interfaces, volume 4, issue 5, pages 2561-2569
One-Pot Noninjection Route to CdS Quantum Dots via Hydrothermal Synthesis
Abdelhay Aboulaich
1, 2
,
Denis Billaud
2
,
Mouhammad Abyan
2
,
Lavinia Balan
3
,
J.J Gaumet
4
,
Ghouti Medjadhi
2
,
Jaafar Ghanbaja
2
,
R. Schneider
1
3
Institut de Science des Matériaux de Mulhouse (IS2M), LRC 7228, 15
rue Jean Starcky, 68093 Mulhouse, France
|
Publication type: Journal Article
Publication date: 2012-04-30
Journal:
ACS applied materials & interfaces
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor: 9.5
ISSN: 19448244, 19448252
General Materials Science
Abstract
Water-dispersible CdS quantum dots (QDs) emitting from 510 to 650 nm were synthesized in a simple one-pot noninjection hydrothermal route using cadmium chloride, thiourea, and 3-mercaptopropionic acid (MPA) as starting materials. All these chemicals were loaded at room temperature in a Teflon sealed tube and the reaction mixture heated at 100 °C. The effects of CdCl(2)/thiourea/MPA feed molar ratios, pH, and concentrations of precursors affecting the growth of the CdS QDs, was monitored via the temporal evolution of the optical properties of the CdS nanocrystals. High concentration of precursors and high MPA/Cd feed molar ratios were found to lead to an increase in the diameter of the resulting CdS nanocrystals and of the trap state emission of the dots. The combination of moderate pH value, low concentration of precursors and slow growth rate plays the crucial role in the good optical properties of the obtained CdS nanocrystals. The highest photoluminescence achieved for CdS@MPA QDs of average size 3.5 nm was 20%. As prepared colloids show rather narrow particle size distribution, although all reactants were mixed at room temperature. CdS@MPA QDs were characterized by UV-vis and photoluminescence spectroscopy, powder X-ray diffraction, transmission electron microscopy, energy-dispersive X-ray spectrometry and MALDI TOF mass spectrometry. This noninjection one-pot approach features easy handling and large-scale production with excellent synthetic reproducibility. Surface passivation of CdS@MPA cores by a wider bandgap material, ZnS, led to enhanced luminescence intensity. CdS@MPA and CdS/ZnS@MPA QDs exhibit high photochemical stability and hold a good potential to be applied in optoelectronic devices and biological applications.
Top-30
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2 publications, 1.47%
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1 publication, 0.74%
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1 publication, 0.74%
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1 publication, 0.74%
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1 publication, 0.74%
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Citations by publishers
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5
10
15
20
25
30
35
40
45
50
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Elsevier
48 publications, 35.29%
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Springer Nature
25 publications, 18.38%
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Royal Society of Chemistry (RSC)
20 publications, 14.71%
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American Chemical Society (ACS)
13 publications, 9.56%
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IOP Publishing
6 publications, 4.41%
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Wiley
5 publications, 3.68%
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Multidisciplinary Digital Publishing Institute (MDPI)
4 publications, 2.94%
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Pleiades Publishing
2 publications, 1.47%
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Taylor & Francis
2 publications, 1.47%
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Beilstein-Institut
1 publication, 0.74%
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Institution of Engineering and Technology (IET)
1 publication, 0.74%
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The Korean Fiber Society
1 publication, 0.74%
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KeAi Communications Co.
1 publication, 0.74%
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Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii
1 publication, 0.74%
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American Institute of Physics (AIP)
1 publication, 0.74%
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5
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15
20
25
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- We do not take into account publications without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Aboulaich A. et al. One-Pot Noninjection Route to CdS Quantum Dots via Hydrothermal Synthesis // ACS applied materials & interfaces. 2012. Vol. 4. No. 5. pp. 2561-2569.
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Aboulaich A., Billaud D., Abyan M., Balan L., Gaumet J., Medjadhi G., Ghanbaja J., Schneider R. One-Pot Noninjection Route to CdS Quantum Dots via Hydrothermal Synthesis // ACS applied materials & interfaces. 2012. Vol. 4. No. 5. pp. 2561-2569.
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TY - JOUR
DO - 10.1021/am300232z
UR - https://doi.org/10.1021/am300232z
TI - One-Pot Noninjection Route to CdS Quantum Dots via Hydrothermal Synthesis
T2 - ACS applied materials & interfaces
AU - Aboulaich, Abdelhay
AU - Billaud, Denis
AU - Abyan, Mouhammad
AU - Balan, Lavinia
AU - Medjadhi, Ghouti
AU - Gaumet, J.J
AU - Ghanbaja, Jaafar
AU - Schneider, R.
PY - 2012
DA - 2012/04/30 00:00:00
PB - American Chemical Society (ACS)
SP - 2561-2569
IS - 5
VL - 4
SN - 1944-8244
SN - 1944-8252
ER -
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@article{2012_Aboulaich,
author = {Abdelhay Aboulaich and Denis Billaud and Mouhammad Abyan and Lavinia Balan and Ghouti Medjadhi and J.J Gaumet and Jaafar Ghanbaja and R. Schneider},
title = {One-Pot Noninjection Route to CdS Quantum Dots via Hydrothermal Synthesis},
journal = {ACS applied materials & interfaces},
year = {2012},
volume = {4},
publisher = {American Chemical Society (ACS)},
month = {apr},
url = {https://doi.org/10.1021/am300232z},
number = {5},
pages = {2561--2569},
doi = {10.1021/am300232z}
}
Cite this
MLA
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Aboulaich, Abdelhay, et al. “One-Pot Noninjection Route to CdS Quantum Dots via Hydrothermal Synthesis.” ACS applied materials & interfaces, vol. 4, no. 5, Apr. 2012, pp. 2561-2569. https://doi.org/10.1021/am300232z.