Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4 VO(PO4 )2
Publication type: Journal Article
Publication date: 2004-02-10
scimago Q1
wos Q1
SJR: 2.065
CiteScore: 12.0
Impact factor: 7.0
ISSN: 08974756, 15205002
Materials Chemistry
General Chemistry
General Chemical Engineering
Abstract
The new vanadyl phosphate Na4VO(PO4)2 was synthesized and investigated by X-ray powder and single-crystal diffraction, high-temperature X-ray diffraction, electron diffraction, high-resolution electron microscopy, thermal analysis, magnetic susceptibility, and conductivity measurements. The compound undergoes a reversible phase transition at about 200 °C. The crystal structure of low-temperature β-Na4VO(PO4)2 was solved using X-ray single-crystal data. This phase has an orthorhombic unit cell with lattice parameters a = 16.0068(12) A, b = 14.5129(8) A, c = 7.0231(5) A, S.G. Pbca, and Z = 8. The crystal structure of β-Na4VO(PO4)2 is built by isolated chains formed by corner-shared V4+O6 octahedra linked additionally via corners by two PO4 tetrahedra. All chains in the structure are equivalent. Na cations are located between the chains in an ordered manner. High-temperature α-Na4VO(PO4)2 also has an orthorhombic cell with lattice parameters a = 15.595(1) A, b = 14.651(2) A, c = 7.0262(6) A, S.G. Ibam, and Z...
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Total citations:
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Panin R. V. et al. Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2 // Chemistry of Materials. 2004. Vol. 16. No. 6. pp. 1048-1055.
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Hadermann J., Kaul E. E., Geibel C. Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2 // Chemistry of Materials. 2004. Vol. 16. No. 6. pp. 1048-1055.
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RIS
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TY - JOUR
DO - 10.1021/cm0351543
UR - https://pubs.acs.org/doi/10.1021/cm0351543
TI - Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2
T2 - Chemistry of Materials
AU - Hadermann, Joke
AU - Kaul, Enrique E.
AU - Geibel, C.
PY - 2004
DA - 2004/02/10
PB - American Chemical Society (ACS)
SP - 1048-1055
IS - 6
VL - 16
SN - 0897-4756
SN - 1520-5002
ER -
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BibTex (up to 50 authors)
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@article{2004_Panin,
author = {Joke Hadermann and Enrique E. Kaul and C. Geibel},
title = {Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2},
journal = {Chemistry of Materials},
year = {2004},
volume = {16},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://pubs.acs.org/doi/10.1021/cm0351543},
number = {6},
pages = {1048--1055},
doi = {10.1021/cm0351543}
}
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MLA
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Panin, Rodion V., et al. “Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2.” Chemistry of Materials, vol. 16, no. 6, Feb. 2004, pp. 1048-1055. https://pubs.acs.org/doi/10.1021/cm0351543.
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