Chemistry of Materials

, том 16 , издание 6 , страницы 1048-1055

Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2

Тип публикации: Journal Article

Дата публикации: 2004-02-10

American Chemical Society (ACS)

Chemistry of Materials

scimago Q1

wos Q1

БС1

SJR: 2.065

CiteScore: 12.0

Impact factor: 7.0

ISSN: 08974756, 15205002

DOI: 10.1021/cm0351543

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Materials Chemistry

General Chemistry

General Chemical Engineering

Краткое описание

The new vanadyl phosphate Na4VO(PO4)2 was synthesized and investigated by X-ray powder and single-crystal diffraction, high-temperature X-ray diffraction, electron diffraction, high-resolution electron microscopy, thermal analysis, magnetic susceptibility, and conductivity measurements. The compound undergoes a reversible phase transition at about 200 °C. The crystal structure of low-temperature β-Na4VO(PO4)2 was solved using X-ray single-crystal data. This phase has an orthorhombic unit cell with lattice parameters a = 16.0068(12) A, b = 14.5129(8) A, c = 7.0231(5) A, S.G. Pbca, and Z = 8. The crystal structure of β-Na4VO(PO4)2 is built by isolated chains formed by corner-shared V4+O6 octahedra linked additionally via corners by two PO4 tetrahedra. All chains in the structure are equivalent. Na cations are located between the chains in an ordered manner. High-temperature α-Na4VO(PO4)2 also has an orthorhombic cell with lattice parameters a = 15.595(1) A, b = 14.651(2) A, c = 7.0262(6) A, S.G. Ibam, and Z...

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Антипов Евгений

д.х.н., проф., академик, Российская академия наук

466 публикаций, 10 708 цитирований, 29 рецензий

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Московский государственный университет имени М.В. Ломоносова

Сколковский институт науки и технологий

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Journal of Solid State Chemistry	Journal of Solid State Chemistry, 2, 8.7% Journal of Solid State Chemistry 2 публикации, 8.7%
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Panin R. V. et al. Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2 // Chemistry of Materials. 2004. Vol. 16. No. 6. pp. 1048-1055.

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Hadermann J., Kaul E. E., Geibel C. Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2 // Chemistry of Materials. 2004. Vol. 16. No. 6. pp. 1048-1055.

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TY - JOUR

DO - 10.1021/cm0351543

UR - https://pubs.acs.org/doi/10.1021/cm0351543

TI - Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2

T2 - Chemistry of Materials

AU - Hadermann, Joke

AU - Kaul, Enrique E.

AU - Geibel, C.

PY - 2004

DA - 2004/02/10

PB - American Chemical Society (ACS)

SP - 1048-1055

IS - 6

VL - 16

SN - 0897-4756

SN - 1520-5002

ER -

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@article{2004_Panin,

author = {Joke Hadermann and Enrique E. Kaul and C. Geibel},

title = {Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2},

journal = {Chemistry of Materials},

year = {2004},

volume = {16},

publisher = {American Chemical Society (ACS)},

month = {feb},

url = {https://pubs.acs.org/doi/10.1021/cm0351543},

number = {6},

pages = {1048--1055},

doi = {10.1021/cm0351543}

}

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Panin, Rodion V., et al. “Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2.” Chemistry of Materials, vol. 16, no. 6, Feb. 2004, pp. 1048-1055. https://pubs.acs.org/doi/10.1021/cm0351543.