Chemistry of Materials, volume 16, issue 6, pages 1048-1055
Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4 VO(PO4 )2
Panin Rodion V
,
Shpanchenko Roman V.
,
Mironov Andrei V.
,
Velikodny Yuri A.
,
Hadermann Joke
1
,
Tarnopolsky Vasily A.
,
Kaul Enrique E.
2
,
2
Max Planck Institute for Chemical Physics of Solids, Max Planck Society
3
Christoph Geibel, Physics of Quantum Materials, Max Planck Institute for Chemical Physics of Solids, Max Planck Society
Publication type: Journal Article
Publication date: 2004-02-10
Journal:
Chemistry of Materials
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor: 8.6
ISSN: 08974756, 15205002
Materials Chemistry
General Chemistry
General Chemical Engineering
Abstract
The new vanadyl phosphate Na4VO(PO4)2 was synthesized and investigated by X-ray powder and single-crystal diffraction, high-temperature X-ray diffraction, electron diffraction, high-resolution electron microscopy, thermal analysis, magnetic susceptibility, and conductivity measurements. The compound undergoes a reversible phase transition at about 200 °C. The crystal structure of low-temperature β-Na4VO(PO4)2 was solved using X-ray single-crystal data. This phase has an orthorhombic unit cell with lattice parameters a = 16.0068(12) A, b = 14.5129(8) A, c = 7.0231(5) A, S.G. Pbca, and Z = 8. The crystal structure of β-Na4VO(PO4)2 is built by isolated chains formed by corner-shared V4+O6 octahedra linked additionally via corners by two PO4 tetrahedra. All chains in the structure are equivalent. Na cations are located between the chains in an ordered manner. High-temperature α-Na4VO(PO4)2 also has an orthorhombic cell with lattice parameters a = 15.595(1) A, b = 14.651(2) A, c = 7.0262(6) A, S.G. Ibam, and Z...
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Panin R. V. et al. Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2 // Chemistry of Materials. 2004. Vol. 16. No. 6. pp. 1048-1055.
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Panin R. V., Shpanchenko R. V., Mironov A. V., Velikodny Y. A., Antipov E. V., Hadermann J., Tarnopolsky V. A., Yaroslavtsev A. B., Kaul E. E., Geibel C. Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2 // Chemistry of Materials. 2004. Vol. 16. No. 6. pp. 1048-1055.
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TY - JOUR
DO - 10.1021/cm0351543
UR - https://doi.org/10.1021%2Fcm0351543
TI - Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2
T2 - Chemistry of Materials
AU - Panin, Rodion V
AU - Shpanchenko, Roman V.
AU - Mironov, Andrei V.
AU - Velikodny, Yuri A.
AU - Tarnopolsky, Vasily A.
AU - Yaroslavtsev, Andrei B.
AU - Kaul, Enrique E.
AU - Antipov, Evgeny V.
AU - Hadermann, Joke
AU - Geibel, C.
PY - 2004
DA - 2004/02/10 00:00:00
PB - American Chemical Society (ACS)
SP - 1048-1055
IS - 6
VL - 16
SN - 0897-4756
SN - 1520-5002
ER -
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@article{2004_Panin
author = {Rodion V Panin and Roman V. Shpanchenko and Andrei V. Mironov and Yuri A. Velikodny and Vasily A. Tarnopolsky and Andrei B. Yaroslavtsev and Enrique E. Kaul and Evgeny V. Antipov and Joke Hadermann and C. Geibel},
title = {Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2},
journal = {Chemistry of Materials},
year = {2004},
volume = {16},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://doi.org/10.1021%2Fcm0351543},
number = {6},
pages = {1048--1055},
doi = {10.1021/cm0351543}
}
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Panin, Rodion V., et al. “Crystal Structure, Polymorphism, and Properties of the New Vanadyl Phosphate Na4VO(PO4)2.” Chemistry of Materials, vol. 16, no. 6, Feb. 2004, pp. 1048-1055. https://doi.org/10.1021%2Fcm0351543.
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