Chemistry of Materials, volume 25, issue 9, pages 1607-1614

Lithium Atom and A-Site Vacancy Distributions in Lanthanum Lithium Titanate

Xiang Gao ¹

Craig A. J. Fisher ¹

Teiichi Kimura ¹

Yumi H. Ikuhara ¹

Hiroki Moriwake ¹

Akihide Kuwabara ¹

Hideki Oki ^{2, 3}

Takeshi Tojigamori ²

Rong Huang ⁴

Yuichi Ikuhara ^{1, 5}

Hide authors affiliations Show authors affiliations: 5 affiliations

Nanostructures Research Laboratory, Japan Fine Ceramics Center, Nagoya 456-8587, Japan |

Battery Materials Division, Toyota Motor Corporation, Shizuoka 410-1193, Japan |

Graduate School of Frontier Science, The University of Tokyo, Tokyo 113-0033, Japan |

⁴

Key Laboratory of Polar Materials and Devices, Ministry of Education, East China Normal University, Shanghai 200062, China |

⁵

Institute of Engineering Innovation, The University of Tokyo, Tokyo 113-8586, Japan |

Publication type: Journal Article

Publication date: 2013-04-25

American Chemical Society (ACS)

Journal: Chemistry of Materials

Quartile SCImago

Quartile WOS

Impact factor: 8.6

ISSN: 08974756, 15205002

DOI: 10.1021/cm3041357

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Materials Chemistry

General Chemistry

General Chemical Engineering

Abstract

Lanthanum lithium titanate (LLTO) is one of the most promising electrolyte materials for all-solid-state lithium-ion batteries. Despite numerous studies, the detailed crystal structure is still open to conjecture because of the difficulty of identifying precisely the positions of Li atoms and the distribution of intrinsic cation vacancies. Here we use subangstrom resolution scanning transmission electron microscopy (STEM) imaging methods and spatially resolved electron energy loss spectroscopy (EELS) analysis to examine the local atomic structure of LLTO. Direct annular bright-field (ABF) observations show Li locations on O4 window positions in Li-poor phase La0.62Li0.16TiO3 and near to A-site positions in Li-rich phase La0.56Li0.33TiO3. Local clustering of A-site vacancies results in aggregation of Li atoms, enhanced octahedral tilting and distortion, formation of O vacancies, and partial Ti4+ reduction. The results suggest local LLTO structures depend on a balance between the distribution of A-site vaca...

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Molecules	Molecules, 1, 1.08% Molecules 1 publication, 1.08%
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Elsevier	Elsevier, 29, 31.18% Elsevier 29 publications, 31.18%
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IOP Publishing	IOP Publishing, 2, 2.15% IOP Publishing 2 publications, 2.15%
Oxford University Press	Oxford University Press, 2, 2.15% Oxford University Press 2 publications, 2.15%
American Physical Society (APS)	American Physical Society (APS), 1, 1.08% American Physical Society (APS) 1 publication, 1.08%
World Scientific	World Scientific, 1, 1.08% World Scientific 1 publication, 1.08%
Japan Society of Applied Physics	Japan Society of Applied Physics, 1, 1.08% Japan Society of Applied Physics 1 publication, 1.08%
The Electrochemical Society	The Electrochemical Society, 1, 1.08% The Electrochemical Society 1 publication, 1.08%
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii	Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii, 1, 1.08% Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii 1 publication, 1.08%
	5 10 15 20 25 30

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GOST Copy

Gao X. et al. Lithium Atom and A-Site Vacancy Distributions in Lanthanum Lithium Titanate // Chemistry of Materials. 2013. Vol. 25. No. 9. pp. 1607-1614.

GOST all authors (up to 50) Copy

Gao X., Fisher C. A. J., Kimura T., Ikuhara Y. H., Moriwake H., Kuwabara A., Oki H., Tojigamori T., Huang R., Ikuhara Y. Lithium Atom and A-Site Vacancy Distributions in Lanthanum Lithium Titanate // Chemistry of Materials. 2013. Vol. 25. No. 9. pp. 1607-1614.

RIS |

Cite this

RIS Copy

TY - JOUR

DO - 10.1021/cm3041357

UR - https://doi.org/10.1021/cm3041357

TI - Lithium Atom and A-Site Vacancy Distributions in Lanthanum Lithium Titanate

T2 - Chemistry of Materials

AU - Fisher, Craig A. J.

AU - Kimura, Teiichi

AU - Ikuhara, Yumi H.

AU - Moriwake, Hiroki

AU - Kuwabara, Akihide

AU - Oki, Hideki

AU - Tojigamori, Takeshi

AU - Ikuhara, Yuichi

AU - Gao, Xiang

AU - Huang, Rong

PY - 2013

DA - 2013/04/25 00:00:00

PB - American Chemical Society (ACS)

SP - 1607-1614

IS - 9

VL - 25

SN - 0897-4756

SN - 1520-5002

ER -

BibTex |

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BibTex Copy

@article{2013_Gao,

author = {Craig A. J. Fisher and Teiichi Kimura and Yumi H. Ikuhara and Hiroki Moriwake and Akihide Kuwabara and Hideki Oki and Takeshi Tojigamori and Yuichi Ikuhara and Xiang Gao and Rong Huang},

title = {Lithium Atom and A-Site Vacancy Distributions in Lanthanum Lithium Titanate},

journal = {Chemistry of Materials},

year = {2013},

volume = {25},

publisher = {American Chemical Society (ACS)},

month = {apr},

url = {https://doi.org/10.1021/cm3041357},

number = {9},

pages = {1607--1614},

doi = {10.1021/cm3041357}

}

MLA

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MLA Copy

Gao, Xiang, et al. “Lithium Atom and A-Site Vacancy Distributions in Lanthanum Lithium Titanate.” Chemistry of Materials, vol. 25, no. 9, Apr. 2013, pp. 1607-1614. https://doi.org/10.1021/cm3041357.

Found error?

Publisher

American Chemical Society (ACS)

Journal

Chemistry of Materials

Quartile SCImago

Quartile WOS

Impact factor

8.6

ISSN

08974756 (Print)
15205002 (Electronic)