Optimized Syntheses of Cyclopentadienyl Nickel Chloride Compounds Containing N-Heterocyclic Carbene Ligands for Short Laboratory Periods
Publication type: Journal Article
Publication date: 2010-11-08
scimago Q2
wos Q1
SJR: 0.596
CiteScore: 4.7
Impact factor: 2.9
ISSN: 00219584, 19381328
General Chemistry
Education
Abstract
Experiments are described for the preparation of imidazolium chloride precursors to N-heterocyclic carbenes and their cyclopentadienyl nickel chloride derivatives. The syntheses have been optimized for second- and third-year undergraduate laboratories that have a maximum programmed length of three hours per week. The experiments are flexible and are readily adapted to a variety of laboratory schedules and student skill levels. The compounds can be characterized by 1H and 13C NMR spectroscopy, and the interesting challenges presented by the NMR spectroscopy of the 2,6-diisopropylphenyl substituted imidazole ring are illustrated.
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31
Total citations:
31
Citations from 2025:
1
(3.23%)
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MLA
Cite this
GOST
Copy
Cooke J., Lightbody O. C. Optimized Syntheses of Cyclopentadienyl Nickel Chloride Compounds Containing N-Heterocyclic Carbene Ligands for Short Laboratory Periods // Journal of Chemical Education. 2010. Vol. 88. No. 1. pp. 88-91.
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Cooke J., Lightbody O. C. Optimized Syntheses of Cyclopentadienyl Nickel Chloride Compounds Containing N-Heterocyclic Carbene Ligands for Short Laboratory Periods // Journal of Chemical Education. 2010. Vol. 88. No. 1. pp. 88-91.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1021/ed100478c
UR - https://doi.org/10.1021/ed100478c
TI - Optimized Syntheses of Cyclopentadienyl Nickel Chloride Compounds Containing N-Heterocyclic Carbene Ligands for Short Laboratory Periods
T2 - Journal of Chemical Education
AU - Cooke, Jason
AU - Lightbody, Owen C
PY - 2010
DA - 2010/11/08
PB - American Chemical Society (ACS)
SP - 88-91
IS - 1
VL - 88
SN - 0021-9584
SN - 1938-1328
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2010_Cooke,
author = {Jason Cooke and Owen C Lightbody},
title = {Optimized Syntheses of Cyclopentadienyl Nickel Chloride Compounds Containing N-Heterocyclic Carbene Ligands for Short Laboratory Periods},
journal = {Journal of Chemical Education},
year = {2010},
volume = {88},
publisher = {American Chemical Society (ACS)},
month = {nov},
url = {https://doi.org/10.1021/ed100478c},
number = {1},
pages = {88--91},
doi = {10.1021/ed100478c}
}
Cite this
MLA
Copy
Cooke, Jason, and Owen C Lightbody. “Optimized Syntheses of Cyclopentadienyl Nickel Chloride Compounds Containing N-Heterocyclic Carbene Ligands for Short Laboratory Periods.” Journal of Chemical Education, vol. 88, no. 1, Nov. 2010, pp. 88-91. https://doi.org/10.1021/ed100478c.