Experimental and Theoretical Approach to the Understanding of TiCl4 Interacting with Arenes. Isolation of a d0-Metal-Arene Complex and Cyclotrimerization of But-2-yne Promoted by TiCl4
Тип публикации: Journal Article
Дата публикации: 1994-04-01
scimago Q1
wos Q1
БС1
SJR: 0.928
CiteScore: 7.6
Impact factor: 4.7
ISSN: 00201669, 1520510X
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
The reaction of TiCl 4 with C 6 Me 6 in CH 2 Cl 2 or 1,2-C 6 H 4 Cl 2 led to a do-arene complex [(η 6 -C 6 Me 6 )TiCl 3 ] + °STi 2 Cl 9 ]-(2), which was structurally characterized by an X-ray analysis. The structure consists of a three-leg piano-stool metallic fragment (TiCl 3 ) + η 6 binding the arene moiety. The 1 H NMR spectrum of the reaction solution indicated the presence of a charge transfer intermediate. The high stability of 2 is evidenced by the TiCL-promoted stoichiometric cyclotrimerization of but-2-yne
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Solari E. et al. Experimental and Theoretical Approach to the Understanding of TiCl4 Interacting with Arenes. Isolation of a d0-Metal-Arene Complex and Cyclotrimerization of But-2-yne Promoted by TiCl4 // Inorganic Chemistry. 1994. Vol. 33. No. 9. pp. 2018-2028.
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Solari E., Floriani C., Schenk K., CHIESI-VILLA A., Rizzoli C., Rosi M., Sgamellotti A. Experimental and Theoretical Approach to the Understanding of TiCl4 Interacting with Arenes. Isolation of a d0-Metal-Arene Complex and Cyclotrimerization of But-2-yne Promoted by TiCl4 // Inorganic Chemistry. 1994. Vol. 33. No. 9. pp. 2018-2028.
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TY - JOUR
DO - 10.1021/ic00087a044
UR - https://doi.org/10.1021/ic00087a044
TI - Experimental and Theoretical Approach to the Understanding of TiCl4 Interacting with Arenes. Isolation of a d0-Metal-Arene Complex and Cyclotrimerization of But-2-yne Promoted by TiCl4
T2 - Inorganic Chemistry
AU - Solari, Euro
AU - Floriani, Carlo
AU - Schenk, Kurt
AU - CHIESI-VILLA, ANGIOLA
AU - Rizzoli, Corrado
AU - Rosi, Marzio
AU - Sgamellotti, Antonio
PY - 1994
DA - 1994/04/01
PB - American Chemical Society (ACS)
SP - 2018-2028
IS - 9
VL - 33
SN - 0020-1669
SN - 1520-510X
ER -
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@article{1994_Solari,
author = {Euro Solari and Carlo Floriani and Kurt Schenk and ANGIOLA CHIESI-VILLA and Corrado Rizzoli and Marzio Rosi and Antonio Sgamellotti},
title = {Experimental and Theoretical Approach to the Understanding of TiCl4 Interacting with Arenes. Isolation of a d0-Metal-Arene Complex and Cyclotrimerization of But-2-yne Promoted by TiCl4},
journal = {Inorganic Chemistry},
year = {1994},
volume = {33},
publisher = {American Chemical Society (ACS)},
month = {apr},
url = {https://doi.org/10.1021/ic00087a044},
number = {9},
pages = {2018--2028},
doi = {10.1021/ic00087a044}
}
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MLA
Скопировать
Solari, Euro, et al. “Experimental and Theoretical Approach to the Understanding of TiCl4 Interacting with Arenes. Isolation of a d0-Metal-Arene Complex and Cyclotrimerization of But-2-yne Promoted by TiCl4.” Inorganic Chemistry, vol. 33, no. 9, Apr. 1994, pp. 2018-2028. https://doi.org/10.1021/ic00087a044.