Inorganic Chemistry

, том 41 , издание 25 , страницы 6892-6904

Synthesis and Properties of Stereoregular Cyclic Polysilanols: cis-[PhSi(O)OH]4, cis-[PhSi(O)OH]6, and Tris-cis-tris-trans-[PhSi(O)OH]12

Тип публикации: Journal Article

Дата публикации: 2002-11-19

American Chemical Society (ACS)

Inorganic Chemistry

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wos Q1

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SJR: 0.928

CiteScore: 7.6

Impact factor: 4.7

ISSN: 00201669, 1520510X

DOI: 10.1021/ic020546h

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PubMed ID: 12470088

Inorganic Chemistry

Physical and Theoretical Chemistry

Краткое описание

New stereoregular cyclic polysilanols of the general formula [PhSi(O)OH]n (n = 6 and 12) have been selectively obtained in high yields by the reaction of cagelike oligophenylmetallasiloxanes with dilute solutions of hydrochloric acid at low temperatures. An alternative method was used to prepare cis-[PhSi(O)OH](4) from sodium phenylsiloxanolate, cis-[(Na(+))(4)[PhSi(O)O(-)](4)].(1-butanol)(x). All compounds were fully characterized by NMR and IR spectroscopy and molecular weight determinations. The structure of cis-[PhSi(O)OH](6) was confirmed by single-crystal X-ray analysis. Furthermore, a series of stereoregular cyclosiloxanes containing triorganylsiloxy groups at each silicon atom was prepared by the reactions of the cyclic polysilanols with triorganylchlorosilanes Me(3)SiCl, Me(2)ViSiCl, and Me(2)(CH(2)Cl)SiCl.

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Shchegolikhina O. I. et al. Synthesis and Properties of Stereoregular Cyclic Polysilanols: cis-[PhSi(O)OH]4, cis-[PhSi(O)OH]6, and Tris-cis-tris-trans-[PhSi(O)OH]12 // Inorganic Chemistry. 2002. Vol. 41. No. 25. pp. 6892-6904.

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Shchegolikhina O. I., Pozdnyakova Y. A., Molodtsova Y. A., Korkin S. D., Bukalov S. S., Leites L. A., Lyssenko K. A., Peregudov A. S., Auner N., Katsoulis D. Synthesis and Properties of Stereoregular Cyclic Polysilanols: cis-[PhSi(O)OH]4, cis-[PhSi(O)OH]6, and Tris-cis-tris-trans-[PhSi(O)OH]12 // Inorganic Chemistry. 2002. Vol. 41. No. 25. pp. 6892-6904.

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TY - JOUR

DO - 10.1021/ic020546h

UR - https://doi.org/10.1021/ic020546h

TI - Synthesis and Properties of Stereoregular Cyclic Polysilanols: cis-[PhSi(O)OH]4, cis-[PhSi(O)OH]6, and Tris-cis-tris-trans-[PhSi(O)OH]12

T2 - Inorganic Chemistry

AU - Shchegolikhina, Olga I.

AU - Pozdnyakova, Yulia A

AU - Molodtsova, Yulia A

AU - Korkin, Sergey D

AU - Bukalov, S. S.

AU - Leites, Larissa A.

AU - Lyssenko, Konstantin A.

AU - Peregudov, Alexandr S

AU - Auner, Norbert

AU - Katsoulis, D.E

PY - 2002

DA - 2002/11/19

PB - American Chemical Society (ACS)

SP - 6892-6904

IS - 25

VL - 41

PMID - 12470088

SN - 0020-1669

SN - 1520-510X

ER -

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@article{2002_Shchegolikhina,

author = {Olga I. Shchegolikhina and Yulia A Pozdnyakova and Yulia A Molodtsova and Sergey D Korkin and S. S. Bukalov and Larissa A. Leites and Konstantin A. Lyssenko and Alexandr S Peregudov and Norbert Auner and D.E Katsoulis},

title = {Synthesis and Properties of Stereoregular Cyclic Polysilanols: cis-[PhSi(O)OH]4, cis-[PhSi(O)OH]6, and Tris-cis-tris-trans-[PhSi(O)OH]12},

journal = {Inorganic Chemistry},

year = {2002},

volume = {41},

publisher = {American Chemical Society (ACS)},

month = {nov},

url = {https://doi.org/10.1021/ic020546h},

number = {25},

pages = {6892--6904},

doi = {10.1021/ic020546h}

}

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Shchegolikhina, Olga I., et al. “Synthesis and Properties of Stereoregular Cyclic Polysilanols: cis-[PhSi(O)OH]4, cis-[PhSi(O)OH]6, and Tris-cis-tris-trans-[PhSi(O)OH]12.” Inorganic Chemistry, vol. 41, no. 25, Nov. 2002, pp. 6892-6904. https://doi.org/10.1021/ic020546h.