Cesium hydroperoxostannate: First complete structural characterization of a homoleptic hydroperoxocomplex
Тип публикации: Journal Article
Дата публикации: 2010-05-11
scimago Q1
wos Q1
БС1
SJR: 0.958
CiteScore: 7.4
Impact factor: 4.7
ISSN: 00201669, 1520510X
PubMed ID:
20459061
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
The crystal structure of cesium hexahydroperoxostannate Cs(2)Sn(OOH)(6) is presented. The compound was characterized by single crystal and by powder X-ray diffraction, FTIR, (119)Sn MAS NMR, and TG-DTA. Cs(2)Sn(OOH)(6) crystallizes in the trigonal space group P3, a = 7.5575(4), c = 5.1050(6) A, V = 252.51(4) A(3), Z = 1, R(1) = 0.0120 (I > 2sigma(I)), wR(2) = 0.0293 (all data), and comprises cesium cations and slightly distorted octahedral [Sn(OOH)(6)](2-) anions lying on the threefold axis. The [Sn(OOH)(6)](2-) unit forms 12 interanion hydrogen bonds resulting in anionic chains spread along the c-axis. All six hydroperoxo ligands are crystallographically equivalent; O-O distances are 1.482(2), only slightly longer than the O-O distance in hydrogen peroxide. FTIR and (119)Sn MAS NMR reveal the similarity between all alkali hydroperoxostannates.
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Churakov A. V. et al. Cesium hydroperoxostannate: First complete structural characterization of a homoleptic hydroperoxocomplex // Inorganic Chemistry. 2010. Vol. 49. No. 11. pp. 4762-4764.
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Churakov A. V., Sladkevich S., Lev O., Tripolskaya T. A., Prikhodchenko P. V. Cesium hydroperoxostannate: First complete structural characterization of a homoleptic hydroperoxocomplex // Inorganic Chemistry. 2010. Vol. 49. No. 11. pp. 4762-4764.
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TY - JOUR
DO - 10.1021/ic100554u
UR - https://pubs.acs.org/doi/10.1021/ic100554u
TI - Cesium hydroperoxostannate: First complete structural characterization of a homoleptic hydroperoxocomplex
T2 - Inorganic Chemistry
AU - Churakov, Andrei V.
AU - Sladkevich, Sergey
AU - Lev, Ovadia
AU - Tripolskaya, Tatiana A
AU - Prikhodchenko, Petr V.
PY - 2010
DA - 2010/05/11
PB - American Chemical Society (ACS)
SP - 4762-4764
IS - 11
VL - 49
PMID - 20459061
SN - 0020-1669
SN - 1520-510X
ER -
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@article{2010_Churakov,
author = {Andrei V. Churakov and Sergey Sladkevich and Ovadia Lev and Tatiana A Tripolskaya and Petr V. Prikhodchenko},
title = {Cesium hydroperoxostannate: First complete structural characterization of a homoleptic hydroperoxocomplex},
journal = {Inorganic Chemistry},
year = {2010},
volume = {49},
publisher = {American Chemical Society (ACS)},
month = {may},
url = {https://pubs.acs.org/doi/10.1021/ic100554u},
number = {11},
pages = {4762--4764},
doi = {10.1021/ic100554u}
}
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MLA
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Churakov, Andrei V., et al. “Cesium hydroperoxostannate: First complete structural characterization of a homoleptic hydroperoxocomplex.” Inorganic Chemistry, vol. 49, no. 11, May. 2010, pp. 4762-4764. https://pubs.acs.org/doi/10.1021/ic100554u.