Platinum Acetate Blue: Synthesis and Characterization
Dmitry I Kochubey
2, 3
,
Vladislav V Kanazhevskiy
2, 3
,
Vladimir I Zaikovskii
2, 4
,
V. V. Ivanov
1
,
Alla P Klyagina
1
,
Zhanna V Dobrokhotova
1, 5
,
Natalia Yu. Kozitsyna
1, 5
,
Igor B Baranovsky
1, 5
,
Olga G Ellert
1, 5
,
Nikolai N. Efimov
1, 5
,
Sergei E Nefedov
1, 5
,
Vladimir M. Novotortsev
1, 5
,
Michael N Vargaftik
5
,
Publication type: Journal Article
Publication date: 2014-08-07
scimago Q1
wos Q1
SJR: 0.958
CiteScore: 7.4
Impact factor: 4.7
ISSN: 00201669, 1520510X
PubMed ID:
25102316
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Platinum acetate blue (PAB) of the empirical formula Pt(OOCMe)2.5±0.25, a byproduct in the synthesis of crystalline platinum(II) acetate Pt4(OOCMe)8, is an X-ray amorphous substance containing platinum in the oxidation state between (II) and (III). Typical PAB samples were studied with X-ray diffraction, differential thermal analysis-thermogravimetric, extended X-ray absorption fine structure, scanning electron microscopy, transmission electron microscopy, magnetochemistry, and combined quantum chemical density functional theory-molecular mechanics modeling to reveal the main structural features of the PAB molecular building blocks. The applicability of PAB to the synthesis of platinum complexes was demonstrated by the preparation of the new homo- and heteronuclear complexes Pt(II)(dipy)(OOCMe)2 (1), Pt(II)(μ-OOCMe)4Co(II)(OH2) (2), and Pt(III)2(OOCMe)4(O3SPhMe)2 (3) with the use of PAB as starting material.
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Total citations:
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GOST
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Cherkashina N. V. et al. Platinum Acetate Blue: Synthesis and Characterization // Inorganic Chemistry. 2014. Vol. 53. No. 16. pp. 8397-8406.
GOST all authors (up to 50)
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Cherkashina N. V., Kochubey D. I., Kanazhevskiy V. V., Zaikovskii V. I., Ivanov V. V., Ivanov V. K., Markov A. A., Klyagina A. P., Dobrokhotova Z. V., Kozitsyna N. Y., Baranovsky I. B., Ellert O. G., Efimov N. N., Nefedov S. E., Novotortsev V. M., Vargaftik M., Vargaftik M. N., Moiseev I. I. Platinum Acetate Blue: Synthesis and Characterization // Inorganic Chemistry. 2014. Vol. 53. No. 16. pp. 8397-8406.
Cite this
RIS
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TY - JOUR
DO - 10.1021/ic500940a
UR - https://pubs.acs.org/doi/10.1021/ic500940a
TI - Platinum Acetate Blue: Synthesis and Characterization
T2 - Inorganic Chemistry
AU - Cherkashina, Natalia V.
AU - Kochubey, Dmitry I
AU - Kanazhevskiy, Vladislav V
AU - Zaikovskii, Vladimir I
AU - Ivanov, V. V.
AU - Ivanov, Vladimir K.
AU - Markov, Alexander A
AU - Klyagina, Alla P
AU - Dobrokhotova, Zhanna V
AU - Kozitsyna, Natalia Yu.
AU - Baranovsky, Igor B
AU - Ellert, Olga G
AU - Efimov, Nikolai N.
AU - Nefedov, Sergei E
AU - Novotortsev, Vladimir M.
AU - Vargaftik, Michael
AU - Vargaftik, Michael N
AU - Moiseev, Ilya I
PY - 2014
DA - 2014/08/07
PB - American Chemical Society (ACS)
SP - 8397-8406
IS - 16
VL - 53
PMID - 25102316
SN - 0020-1669
SN - 1520-510X
ER -
Cite this
BibTex (up to 50 authors)
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@article{2014_Cherkashina,
author = {Natalia V. Cherkashina and Dmitry I Kochubey and Vladislav V Kanazhevskiy and Vladimir I Zaikovskii and V. V. Ivanov and Vladimir K. Ivanov and Alexander A Markov and Alla P Klyagina and Zhanna V Dobrokhotova and Natalia Yu. Kozitsyna and Igor B Baranovsky and Olga G Ellert and Nikolai N. Efimov and Sergei E Nefedov and Vladimir M. Novotortsev and Michael Vargaftik and Michael N Vargaftik and Ilya I Moiseev},
title = {Platinum Acetate Blue: Synthesis and Characterization},
journal = {Inorganic Chemistry},
year = {2014},
volume = {53},
publisher = {American Chemical Society (ACS)},
month = {aug},
url = {https://pubs.acs.org/doi/10.1021/ic500940a},
number = {16},
pages = {8397--8406},
doi = {10.1021/ic500940a}
}
Cite this
MLA
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Cherkashina, Natalia V., et al. “Platinum Acetate Blue: Synthesis and Characterization.” Inorganic Chemistry, vol. 53, no. 16, Aug. 2014, pp. 8397-8406. https://pubs.acs.org/doi/10.1021/ic500940a.