Synthesis and Structural Characterization of Aluminum Iminophosphonamide Complexes
Тип публикации: Journal Article
Дата публикации: 2009-09-09
scimago Q1
wos Q1
БС1
SJR: 0.928
CiteScore: 7.6
Impact factor: 4.7
ISSN: 00201669, 1520510X
PubMed ID:
19739632
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
Monoanionic iminophosphonamide ligands have a N-P-N linkage and undergo four-membered ring N,N-ligand formation when treated with aluminum compounds. The reaction of LLi (L = [Ph(2)P(NSiMe(3))(2)]) with equivalent amounts of AlCl(3) and AlMeCl(2) in toluene afforded LAlCl(2) (3) and LAlClMe (4), respectively. L(2)AlH (5), LAlEt(2) (6), and LAl(NMe(2))(2) (7) respectively were prepared by the reaction of LH with AlH(3) x NMe(3), AlEt(3), and Al(NMe(2))(3) in n-hexane. Subsequently compounds 3-7 were characterized by elemental analysis, (1)H, (13)C, and (31)P NMR spectroscopy and X-ray crystallographic studies (for 3, 4, 5, and 7).
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Nekoueishahraki B. et al. Synthesis and Structural Characterization of Aluminum Iminophosphonamide Complexes // Inorganic Chemistry. 2009. Vol. 48. No. 19. pp. 9174-9179.
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Nekoueishahraki B., Roesky H. W., Schwab G., Stern D., Stalke D. Synthesis and Structural Characterization of Aluminum Iminophosphonamide Complexes // Inorganic Chemistry. 2009. Vol. 48. No. 19. pp. 9174-9179.
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TY - JOUR
DO - 10.1021/ic9011179
UR - https://doi.org/10.1021/ic9011179
TI - Synthesis and Structural Characterization of Aluminum Iminophosphonamide Complexes
T2 - Inorganic Chemistry
AU - Nekoueishahraki, Bijan
AU - Roesky, Herbert W.
AU - Schwab, Gerald
AU - Stern, Daniel
AU - Stalke, Dietmar
PY - 2009
DA - 2009/09/09
PB - American Chemical Society (ACS)
SP - 9174-9179
IS - 19
VL - 48
PMID - 19739632
SN - 0020-1669
SN - 1520-510X
ER -
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@article{2009_Nekoueishahraki,
author = {Bijan Nekoueishahraki and Herbert W. Roesky and Gerald Schwab and Daniel Stern and Dietmar Stalke},
title = {Synthesis and Structural Characterization of Aluminum Iminophosphonamide Complexes},
journal = {Inorganic Chemistry},
year = {2009},
volume = {48},
publisher = {American Chemical Society (ACS)},
month = {sep},
url = {https://doi.org/10.1021/ic9011179},
number = {19},
pages = {9174--9179},
doi = {10.1021/ic9011179}
}
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MLA
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Nekoueishahraki, Bijan, et al. “Synthesis and Structural Characterization of Aluminum Iminophosphonamide Complexes.” Inorganic Chemistry, vol. 48, no. 19, Sep. 2009, pp. 9174-9179. https://doi.org/10.1021/ic9011179.