EPR observation of nitroxide free radicals during thermal decomposition of 2,4,6-trinitrotoluene and related compounds
Тип публикации: Journal Article
Дата публикации: 1986-03-01
SJR: 1.641
CiteScore: —
Impact factor: —
ISSN: 00223654, 15415740
Physical and Theoretical Chemistry
General Engineering
Краткое описание
Evidence is presented to support the observation by electron paramagnetic resonance (EPR) of nitroxide radicals formed by intermolecular coupling during the thermal decomposition of 2,4,6-trinitrotoluene (TNT) alone and during thermolysis of TNT in the presence of hexamethylbenzene (HMB) or perdeuteriohexamethylbenzene (HMB-d/sub 18/). Similar results are reported for the thermal reaction of 1,3,5-trinitrobenzene (TNB) with HMB, HMB-d/sub 18/, and TNT. A reaction mechanism is proposed. An unidentified nitroxide radical has been separated chromatographically from TNT thermolysis products. 14 references, 2 figures, 1 table.
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Mckinney T. M. et al. EPR observation of nitroxide free radicals during thermal decomposition of 2,4,6-trinitrotoluene and related compounds // The Journal of Physical Chemistry. 1986. Vol. 90. No. 6. pp. 1008-1011.
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Mckinney T. M., Warren L. F., Goldberg I. B., Swanson J. T. EPR observation of nitroxide free radicals during thermal decomposition of 2,4,6-trinitrotoluene and related compounds // The Journal of Physical Chemistry. 1986. Vol. 90. No. 6. pp. 1008-1011.
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TY - JOUR
DO - 10.1021/j100278a010
UR - https://doi.org/10.1021/j100278a010
TI - EPR observation of nitroxide free radicals during thermal decomposition of 2,4,6-trinitrotoluene and related compounds
T2 - The Journal of Physical Chemistry
AU - Mckinney, Ted M
AU - Warren, Leslie F.
AU - Goldberg, Ira B
AU - Swanson, Jon T
PY - 1986
DA - 1986/03/01
PB - American Chemical Society (ACS)
SP - 1008-1011
IS - 6
VL - 90
SN - 0022-3654
SN - 1541-5740
ER -
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@article{1986_Mckinney,
author = {Ted M Mckinney and Leslie F. Warren and Ira B Goldberg and Jon T Swanson},
title = {EPR observation of nitroxide free radicals during thermal decomposition of 2,4,6-trinitrotoluene and related compounds},
journal = {The Journal of Physical Chemistry},
year = {1986},
volume = {90},
publisher = {American Chemical Society (ACS)},
month = {mar},
url = {https://doi.org/10.1021/j100278a010},
number = {6},
pages = {1008--1011},
doi = {10.1021/j100278a010}
}
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MLA
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Mckinney, Ted M., et al. “EPR observation of nitroxide free radicals during thermal decomposition of 2,4,6-trinitrotoluene and related compounds.” The Journal of Physical Chemistry, vol. 90, no. 6, Mar. 1986, pp. 1008-1011. https://doi.org/10.1021/j100278a010.
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