Journal of the American Chemical Society, volume 134, issue 49, pages 20160-20168

Highly effective surface passivation of PbSe quantum dots through reaction with molecular chlorine.

Wan Ki Bae ¹

Jin Joo ²

Lazaro A. Padilha ³

Jonghan Won ³

Doh Jae Lee ³

Qianglu Lin ⁴

W.-K. Koh ³

Hongmei Luo ⁴

Victor I. Klimov ³

Jeffrey M. Pietryga ³

Hide authors affiliations Show authors affiliations: 4 affiliations

Chemistry Division, Los Alamos National Laboratory Los Alamos, New Mexico 87545 (United States) |

Department of Applied Chemistry, Kyungpook National University, Daegu 702-701, Korea |

LOS ALAMOS NATIONAL LABORATORY |

⁴

Department of Chemical Engineering, New Mexico State University, Las Cruces, New Mexico 88003, United States |

Publication type: Journal Article

Publication date: 2012-11-27

American Chemical Society (ACS)

Journal: Journal of the American Chemical Society

Quartile SCImago

Quartile WOS

Impact factor: 15

ISSN: 00027863, 15205126

DOI: 10.1021/ja309783v

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General Chemistry

Catalysis

Biochemistry

Colloid and Surface Chemistry

Abstract

PbSe nanocrystal quantum dots (NQDs) are a promising active material for a range of optoelectronic devices, including solar cells, high-sensitivity infrared (IR) photodetectors, and IR-emitting diodes and lasers. However, device realization has been constrained by these NQDs' chemical instability toward oxidation, which leads to uncontrollable changes in optical and electronic properties. Here, we present a simple method to enhance the stability of PbSe NQDs against oxidation and to improve their optical properties through reaction with molecular chlorine. The chlorine molecules preferentially etch out surface Se ions and react with Pb ions to form a thin (1-2 monolayers) PbCl(x) passivation layer which effectively prevents oxidation during long-term air exposure while passivating surface trap states to increase photoluminescence efficiency and decrease photocharging. Our method is simple, widely applicable to PbSe and PbS NQDs of a range of sizes, compatible with solution-based processes for fabricating NQD-based devices, and effective both in solution and in solid NQD films; thus, it is a practical protocol for facilitating advances over the full range of optoelectronic applications.

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Citations by journals

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RSC Advances	RSC Advances, 6, 2.74% RSC Advances 6 publications, 2.74%
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Advanced Functional Materials	Advanced Functional Materials, 4, 1.83% Advanced Functional Materials 4 publications, 1.83%
Advanced Optical Materials	Advanced Optical Materials, 4, 1.83% Advanced Optical Materials 4 publications, 1.83%
Langmuir	Langmuir, 4, 1.83% Langmuir 4 publications, 1.83%
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Small	Small, 3, 1.37% Small 3 publications, 1.37%
ACS Energy Letters	ACS Energy Letters, 3, 1.37% ACS Energy Letters 3 publications, 1.37%
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Nanomaterials	Nanomaterials, 2, 0.91% Nanomaterials 2 publications, 0.91%
NPG Asia Materials	NPG Asia Materials, 2, 0.91% NPG Asia Materials 2 publications, 0.91%
Nature	Nature, 2, 0.91% Nature 2 publications, 0.91%
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Scientific Reports	Scientific Reports, 2, 0.91% Scientific Reports 2 publications, 0.91%
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Nanotechnology	Nanotechnology, 2, 0.91% Nanotechnology 2 publications, 0.91%
Chinese Physics B	Chinese Physics B, 2, 0.91% Chinese Physics B 2 publications, 0.91%
Russian Chemical Reviews	Russian Chemical Reviews, 2, 0.91% Russian Chemical Reviews 2 publications, 0.91%
Materials Science in Semiconductor Processing	Materials Science in Semiconductor Processing, 2, 0.91% Materials Science in Semiconductor Processing 2 publications, 0.91%
Nano Energy	Nano Energy, 2, 0.91% Nano Energy 2 publications, 0.91%
	2 4 6 8 10 12 14

Citations by publishers

	10 20 30 40 50 60 70 80
American Chemical Society (ACS)	American Chemical Society (ACS), 74, 33.79% American Chemical Society (ACS) 74 publications, 33.79%
Wiley	Wiley, 38, 17.35% Wiley 38 publications, 17.35%
Elsevier	Elsevier, 27, 12.33% Elsevier 27 publications, 12.33%
Royal Society of Chemistry (RSC)	Royal Society of Chemistry (RSC), 25, 11.42% Royal Society of Chemistry (RSC) 25 publications, 11.42%
Springer Nature	Springer Nature, 21, 9.59% Springer Nature 21 publications, 9.59%
IOP Publishing	IOP Publishing, 7, 3.2% IOP Publishing 7 publications, 3.2%
American Institute of Physics (AIP)	American Institute of Physics (AIP), 5, 2.28% American Institute of Physics (AIP) 5 publications, 2.28%
Multidisciplinary Digital Publishing Institute (MDPI)	Multidisciplinary Digital Publishing Institute (MDPI), 4, 1.83% Multidisciplinary Digital Publishing Institute (MDPI) 4 publications, 1.83%
Walter de Gruyter	Walter de Gruyter, 4, 1.83% Walter de Gruyter 4 publications, 1.83%
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii	Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii, 2, 0.91% Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii 2 publications, 0.91%
Taylor & Francis	Taylor & Francis, 2, 0.91% Taylor & Francis 2 publications, 0.91%
Optical Society of America	Optical Society of America, 2, 0.91% Optical Society of America 2 publications, 0.91%
Materials Research Society	Materials Research Society, 1, 0.46% Materials Research Society 1 publication, 0.46%
Annual Reviews	Annual Reviews, 1, 0.46% Annual Reviews 1 publication, 0.46%
American Vacuum Society	American Vacuum Society, 1, 0.46% American Vacuum Society 1 publication, 0.46%
	10 20 30 40 50 60 70 80

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Bae W. K. et al. Highly effective surface passivation of PbSe quantum dots through reaction with molecular chlorine. // Journal of the American Chemical Society. 2012. Vol. 134. No. 49. pp. 20160-20168.

GOST all authors (up to 50) Copy

Bae W. K., Joo J., Padilha L. A., Won J., Lee D. J., Lin Q., Koh W., Luo H., Klimov V. I., Pietryga J. M. Highly effective surface passivation of PbSe quantum dots through reaction with molecular chlorine. // Journal of the American Chemical Society. 2012. Vol. 134. No. 49. pp. 20160-20168.

RIS |

Cite this

RIS Copy

TY - JOUR

DO - 10.1021/ja309783v

UR - https://doi.org/10.1021/ja309783v

TI - Highly effective surface passivation of PbSe quantum dots through reaction with molecular chlorine.

T2 - Journal of the American Chemical Society

AU - Won, Jonghan

AU - Lin, Qianglu

AU - Bae, Wan Ki

AU - Joo, Jin

AU - Padilha, Lazaro A.

AU - Lee, Doh Jae

AU - Koh, W.-K.

AU - Luo, Hongmei

AU - Klimov, Victor I.

AU - Pietryga, Jeffrey M.

PY - 2012

DA - 2012/11/27 00:00:00

PB - American Chemical Society (ACS)

SP - 20160-20168

IS - 49

VL - 134

SN - 0002-7863

SN - 1520-5126

ER -

BibTex |

Cite this

BibTex Copy

@article{2012_Bae,

author = {Jonghan Won and Qianglu Lin and Wan Ki Bae and Jin Joo and Lazaro A. Padilha and Doh Jae Lee and W.-K. Koh and Hongmei Luo and Victor I. Klimov and Jeffrey M. Pietryga},

title = {Highly effective surface passivation of PbSe quantum dots through reaction with molecular chlorine.},

journal = {Journal of the American Chemical Society},

year = {2012},

volume = {134},

publisher = {American Chemical Society (ACS)},

month = {nov},

url = {https://doi.org/10.1021/ja309783v},

number = {49},

pages = {20160--20168},

doi = {10.1021/ja309783v}

}

MLA

Cite this

MLA Copy

Bae, Wan Ki, et al. “Highly effective surface passivation of PbSe quantum dots through reaction with molecular chlorine..” Journal of the American Chemical Society, vol. 134, no. 49, Nov. 2012, pp. 20160-20168. https://doi.org/10.1021/ja309783v.

Found error?

Publisher

American Chemical Society (ACS)

Journal

Journal of the American Chemical Society

Quartile SCImago

Quartile WOS

Impact factor

ISSN

00027863 (Print)
15205126 (Electronic)