Synthesis of alpha-hydrazino ketones via regio- and stereoselective electrophilic amination of manganese enolates and enamines.
Тип публикации: Journal Article
Дата публикации: 2004-11-01
SCImago Q2
WOS Q1
БС1
SJR: 0.604
CiteScore: 5.8
Impact factor: 3.3
ISSN: 00223263, 15206904
PubMed ID:
15549836
Organic Chemistry
Краткое описание
A straightforward procedure for the regio- and stereoselective synthesis of alpha-hydrazino ketones is described. Manganese enolates and manganese enamines derived from ketones and from the corresponding N-sulfinylimines react with azodicarboxylate esters (DTBAD and DEAD) in a regioselective fashion to afford in good to excellent yields the kinetic alpha-hydrazino ketones as sole or highly prevalent products. When enantiopure N-sulfinyl manganese enamines were used the stereoselectivity of these reactions ranged from 40% to 68% ee.
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Dessole G. et al. Synthesis of alpha-hydrazino ketones via regio- and stereoselective electrophilic amination of manganese enolates and enamines. // Journal of Organic Chemistry. 2004. Vol. 69. No. 24. pp. 8525-8528.
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Dessole G., Bernardi L., Bonini B. F., Capitò E., Fochi M., Herrera R. P., Ricci A., Cahiez G. Synthesis of alpha-hydrazino ketones via regio- and stereoselective electrophilic amination of manganese enolates and enamines. // Journal of Organic Chemistry. 2004. Vol. 69. No. 24. pp. 8525-8528.
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TY - JOUR
DO - 10.1021/jo049152t
UR - https://doi.org/10.1021/jo049152t
TI - Synthesis of alpha-hydrazino ketones via regio- and stereoselective electrophilic amination of manganese enolates and enamines.
T2 - Journal of Organic Chemistry
AU - Dessole, Gabriella
AU - Bernardi, Luca
AU - Bonini, Bianca F.
AU - Capitò, Elena
AU - Fochi, Mariafrancesca
AU - Herrera, Raquel P
AU - Ricci, Alfredo
AU - Cahiez, Gerard
PY - 2004
DA - 2004/11/01
PB - American Chemical Society (ACS)
SP - 8525-8528
IS - 24
VL - 69
PMID - 15549836
SN - 0022-3263
SN - 1520-6904
ER -
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@article{2004_Dessole,
author = {Gabriella Dessole and Luca Bernardi and Bianca F. Bonini and Elena Capitò and Mariafrancesca Fochi and Raquel P Herrera and Alfredo Ricci and Gerard Cahiez},
title = {Synthesis of alpha-hydrazino ketones via regio- and stereoselective electrophilic amination of manganese enolates and enamines.},
journal = {Journal of Organic Chemistry},
year = {2004},
volume = {69},
publisher = {American Chemical Society (ACS)},
month = {nov},
url = {https://doi.org/10.1021/jo049152t},
number = {24},
pages = {8525--8528},
doi = {10.1021/jo049152t}
}
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MLA
Скопировать
Dessole, Gabriella, et al. “Synthesis of alpha-hydrazino ketones via regio- and stereoselective electrophilic amination of manganese enolates and enamines..” Journal of Organic Chemistry, vol. 69, no. 24, Nov. 2004, pp. 8525-8528. https://doi.org/10.1021/jo049152t.
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