Development of Second Generation Gold-Supported Palladium Material with Low-Leaching and Recyclable Characteristics in Aromatic Amination
Mohammad Al Amin
1
,
Satoshi Arai
2
,
Naoyoki Hoshiya
1, 2
,
Tetsuo Honma
3
,
Yusuke Tamenori
3
,
Takatoshi Sato
1
,
Mami Yokoyama
4
,
A. Ishii
4
,
Masashi Takeuchi
2
,
Tomohiro Maruko
2
,
Satoshi Shuto
1
,
Mitsuhiro Arisawa
1
2
Furuya Metal Company, Ltd., Minami-otsuka 2-37-5, Toshima-ku, Tokyo 170-0005,
Japan
|
Publication type: Journal Article
Publication date: 2013-07-17
scimago Q2
wos Q1
SJR: 0.737
CiteScore: 6.1
Impact factor: 3.6
ISSN: 00223263, 15206904
PubMed ID:
23862612
Organic Chemistry
Abstract
An improved process for the preparation of sulfur-modified gold-supported palladium material [SAPd, second generation] is presented. The developed preparation method is safer and generates less heat (aqueous Na2S2O8 and H2SO4) for sulfur fixation on a gold surface, and it is superior to the previous method of preparing SAPd (first generation), which requires the use of the more heat-generating and dangerous piranha solution (concentrated H2SO4 and 35% H2O2) in the sulfur fixation step. This safer and improved preparation method is particularly important for the mass production of SAPd (second generation) for which the catalytic activity was examined in ligand-free Buchwald-Hartwig cross-coupling reactions. The catalytic activities were the same between the first and second generation SAPds in aromatic aminations, but the lower palladium leaching properties and safer preparative method of second generation SAPd are a significant improvement over the first generation SAPd.
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Total citations:
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Citations from 2024:
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(3.7%)
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GOST
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Al Amin M. et al. Development of Second Generation Gold-Supported Palladium Material with Low-Leaching and Recyclable Characteristics in Aromatic Amination // Journal of Organic Chemistry. 2013. Vol. 78. No. 15. pp. 7575-7581.
GOST all authors (up to 50)
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Al Amin M., Arai S., Hoshiya N., Honma T., Tamenori Y., Sato T., Yokoyama M., Ishii A., Takeuchi M., Maruko T., Shuto S., Arisawa M. Development of Second Generation Gold-Supported Palladium Material with Low-Leaching and Recyclable Characteristics in Aromatic Amination // Journal of Organic Chemistry. 2013. Vol. 78. No. 15. pp. 7575-7581.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1021/jo4011415
UR - https://doi.org/10.1021/jo4011415
TI - Development of Second Generation Gold-Supported Palladium Material with Low-Leaching and Recyclable Characteristics in Aromatic Amination
T2 - Journal of Organic Chemistry
AU - Al Amin, Mohammad
AU - Arai, Satoshi
AU - Hoshiya, Naoyoki
AU - Honma, Tetsuo
AU - Tamenori, Yusuke
AU - Sato, Takatoshi
AU - Yokoyama, Mami
AU - Ishii, A.
AU - Takeuchi, Masashi
AU - Maruko, Tomohiro
AU - Shuto, Satoshi
AU - Arisawa, Mitsuhiro
PY - 2013
DA - 2013/07/17
PB - American Chemical Society (ACS)
SP - 7575-7581
IS - 15
VL - 78
PMID - 23862612
SN - 0022-3263
SN - 1520-6904
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2013_Al Amin,
author = {Mohammad Al Amin and Satoshi Arai and Naoyoki Hoshiya and Tetsuo Honma and Yusuke Tamenori and Takatoshi Sato and Mami Yokoyama and A. Ishii and Masashi Takeuchi and Tomohiro Maruko and Satoshi Shuto and Mitsuhiro Arisawa},
title = {Development of Second Generation Gold-Supported Palladium Material with Low-Leaching and Recyclable Characteristics in Aromatic Amination},
journal = {Journal of Organic Chemistry},
year = {2013},
volume = {78},
publisher = {American Chemical Society (ACS)},
month = {jul},
url = {https://doi.org/10.1021/jo4011415},
number = {15},
pages = {7575--7581},
doi = {10.1021/jo4011415}
}
Cite this
MLA
Copy
Al Amin, Mohammad, et al. “Development of Second Generation Gold-Supported Palladium Material with Low-Leaching and Recyclable Characteristics in Aromatic Amination.” Journal of Organic Chemistry, vol. 78, no. 15, Jul. 2013, pp. 7575-7581. https://doi.org/10.1021/jo4011415.