Journal of Organic Chemistry

, том 78 , издание 17 , страницы 8680-8688

2,2'-Biphenols via protecting group-free thermal or microwave-accelerated Suzuki-Miyaura coupling in water.

Тип публикации: Journal Article

Дата публикации: 2013-08-13

American Chemical Society (ACS)

Journal of Organic Chemistry

SCImago Q2

WOS Q1

БС1

SJR: 0.604

CiteScore: 5.8

Impact factor: 3.3

ISSN: 00223263, 15206904

DOI: 10.1021/jo401398n

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PubMed ID: 23899041

Organic Chemistry

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User-friendly protocols for the protecting group-free synthesis of 2,2'-biphenols via Suzuki-Miyaura coupling of o-halophenols and o-boronophenol are presented. The reactions proceed in water in the presence of simple additives such as K2CO3, KOH, KF, or TBAF and with commercially available Pd/C as precatalyst. Expensive or laboriously synthesized ligands or other additives are not required. In the case of bromophenols, efficient rate acceleration and short reaction times were accomplished by microwave irradiation.

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Schmidt B., Riemer M., Karras M. 2,2'-Biphenols via protecting group-free thermal or microwave-accelerated Suzuki-Miyaura coupling in water. // Journal of Organic Chemistry. 2013. Vol. 78. No. 17. pp. 8680-8688.

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TY - JOUR

DO - 10.1021/jo401398n

UR - https://doi.org/10.1021/jo401398n

TI - 2,2'-Biphenols via protecting group-free thermal or microwave-accelerated Suzuki-Miyaura coupling in water.

T2 - Journal of Organic Chemistry

AU - Schmidt, Bernd

AU - Riemer, Martin

AU - Karras, Manfred

PY - 2013

DA - 2013/08/13

PB - American Chemical Society (ACS)

SP - 8680-8688

IS - 17

VL - 78

PMID - 23899041

SN - 0022-3263

SN - 1520-6904

ER -

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@article{2013_Schmidt,

author = {Bernd Schmidt and Martin Riemer and Manfred Karras},

title = {2,2'-Biphenols via protecting group-free thermal or microwave-accelerated Suzuki-Miyaura coupling in water.},

journal = {Journal of Organic Chemistry},

year = {2013},

volume = {78},

publisher = {American Chemical Society (ACS)},

month = {aug},

url = {https://doi.org/10.1021/jo401398n},

number = {17},

pages = {8680--8688},

doi = {10.1021/jo401398n}

}

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Schmidt, Bernd, et al. “2,2'-Biphenols via protecting group-free thermal or microwave-accelerated Suzuki-Miyaura coupling in water..” Journal of Organic Chemistry, vol. 78, no. 17, Aug. 2013, pp. 8680-8688. https://doi.org/10.1021/jo401398n.

Издатель

American Chemical Society (ACS)

Журнал

Journal of Organic Chemistry

SCImago Q2

WOS Q1

БС1

SJR

0.604

CiteScore

5.8

Impact factor