2,2'-Biphenols via protecting group-free thermal or microwave-accelerated Suzuki-Miyaura coupling in water.
1
Institut fuer Chemie (Organische Synthesechemie), Universitaet Potsdam, Karl-Liebknecht-Strasse 24-25,
D-14476 Potsdam-Golm, Germany
|
Publication type: Journal Article
Publication date: 2013-08-13
scimago Q2
wos Q1
SJR: 0.737
CiteScore: 6.1
Impact factor: 3.6
ISSN: 00223263, 15206904
PubMed ID:
23899041
Organic Chemistry
Abstract
User-friendly protocols for the protecting group-free synthesis of 2,2'-biphenols via Suzuki-Miyaura coupling of o-halophenols and o-boronophenol are presented. The reactions proceed in water in the presence of simple additives such as K2CO3, KOH, KF, or TBAF and with commercially available Pd/C as precatalyst. Expensive or laboriously synthesized ligands or other additives are not required. In the case of bromophenols, efficient rate acceleration and short reaction times were accomplished by microwave irradiation.
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Citations from 2024:
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(8%)
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GOST
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Schmidt B., Riemer M., Karras M. 2,2'-Biphenols via protecting group-free thermal or microwave-accelerated Suzuki-Miyaura coupling in water. // Journal of Organic Chemistry. 2013. Vol. 78. No. 17. pp. 8680-8688.
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Schmidt B., Riemer M., Karras M. 2,2'-Biphenols via protecting group-free thermal or microwave-accelerated Suzuki-Miyaura coupling in water. // Journal of Organic Chemistry. 2013. Vol. 78. No. 17. pp. 8680-8688.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1021/jo401398n
UR - https://doi.org/10.1021/jo401398n
TI - 2,2'-Biphenols via protecting group-free thermal or microwave-accelerated Suzuki-Miyaura coupling in water.
T2 - Journal of Organic Chemistry
AU - Schmidt, Bernd
AU - Riemer, Martin
AU - Karras, Manfred
PY - 2013
DA - 2013/08/13
PB - American Chemical Society (ACS)
SP - 8680-8688
IS - 17
VL - 78
PMID - 23899041
SN - 0022-3263
SN - 1520-6904
ER -
Cite this
BibTex (up to 50 authors)
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@article{2013_Schmidt,
author = {Bernd Schmidt and Martin Riemer and Manfred Karras},
title = {2,2'-Biphenols via protecting group-free thermal or microwave-accelerated Suzuki-Miyaura coupling in water.},
journal = {Journal of Organic Chemistry},
year = {2013},
volume = {78},
publisher = {American Chemical Society (ACS)},
month = {aug},
url = {https://doi.org/10.1021/jo401398n},
number = {17},
pages = {8680--8688},
doi = {10.1021/jo401398n}
}
Cite this
MLA
Copy
Schmidt, Bernd, et al. “2,2'-Biphenols via protecting group-free thermal or microwave-accelerated Suzuki-Miyaura coupling in water..” Journal of Organic Chemistry, vol. 78, no. 17, Aug. 2013, pp. 8680-8688. https://doi.org/10.1021/jo401398n.